Rapid Heating of Silicon Carbide Fibers under Radio Frequency Fields and Application in Curing Preceramic Polymer Composites

2019 ◽  
Vol 11 (49) ◽  
pp. 46132-46139 ◽  
Author(s):  
Nutan Patil ◽  
Xiaofei Zhao ◽  
Naveen K. Mishra ◽  
Mohammad A. Saed ◽  
Miladin Radovic ◽  
...  
Author(s):  
L. A. Giannuzzi ◽  
C. A. Lewinsohn ◽  
C. E. Bakis ◽  
R. E. Tressler

The SCS-6 SiC fiber is a 142 μm diameter fiber consisting of four distinct regions of βSiC. These SiC regions vary in excess carbon content ranging from 10 a/o down to 5 a/o in the SiC1 through SiC3 region. The SiC4 region is stoichiometric. The SiC sub-grains in all regions grow radially outward from the carbon core of the fiber during the chemical vapor deposition processing of these fibers. In general, the sub-grain width changes from 50nm to 250nm while maintaining an aspect ratio of ~10:1 from the SiC1 through the SiC4 regions. In addition, the SiC shows a <110> texture, i.e., the {111} planes lie ±15° along the fiber axes. Previous has shown that the SCS-6 fiber (as well as the SCS-9 and the developmental SCS-50 μm fiber) undergoes primary creep (i.e., the creep rate constantly decreases as a function of time) throughout the lifetime of the creep test.


2017 ◽  
Vol 37 (6) ◽  
pp. 547-557 ◽  
Author(s):  
Sekaran Sathees Kumar ◽  
Ganesan Kanagaraj

Abstract In this paper, the combined effect of different weight percentages of silicon carbide (SiC) and graphite (Gr) reinforcement on the mechanical properties of polyamide (PA6) composite is studied. Test specimens of pure PA6, 85 wt% PA6+10 wt% SiC+5 wt% Gr and 85 wt% PA6+5 wt% SiC+10 wt% Gr are prepared using an injection molding machine. The tensile, impact, hardness, morphology and thermal properties of the injection molded composites were investigated. The obtained results showed that mechanical properties, such as tensile and impact strength and modulus of the PA6 composites, were significantly higher than the pure PA6, and hybridization with silicon carbide and graphite further enhanced the performance properties, as well as the thermal resistance of the composites. The tensile fracture morphology and the characterization of PA6 polymer composites were observed by scanning electron microscope (SEM) and Fourier transform infrared spectroscopic methods. SEM observation of the fracture surfaces showed the fine dispersion of SiC and Gr for strong interfacial adhesion between fibers and matrix. The individual and combined reinforcing effects of silicon carbide and graphite on the mechanical properties of PA6 hybrid composites were compared and interpreted in this study. Improved mechanical properties were observed by the addition of small amount of SiC and Gr concurrently reinforced with the pure PA6. Finally, thermogravimetric analysis showed that the heat resistance of the composites tended to increase with increasing silicon carbide and graphite content simultaneously.


2018 ◽  
Vol 38 (1) ◽  
pp. 67-74 ◽  
Author(s):  
Bo Tang ◽  
Mingchao Wang ◽  
Ruiming Liu ◽  
Jiachen Liu ◽  
Haiyan Du ◽  
...  

2010 ◽  
Vol 93 (1) ◽  
pp. 89-95 ◽  
Author(s):  
Xiaojun Chen ◽  
Zhiming Su ◽  
Li Zhang ◽  
Ming Tang ◽  
Yuxi Yu ◽  
...  

2018 ◽  
Vol 912 ◽  
pp. 141-146 ◽  
Author(s):  
Glauson Aparecido Ferreira Machado ◽  
Rosa Maria Rocha ◽  
Ana Helena Almeida Bressiani

Alumina-mullite composites with low shrinkage can be made by reaction bond using mixtures of alumina, aluminum and silicon carbide. In this work, an alternative route is used to produce alumina composites with low shrinkage. Here alumina samples containing additions of 10 and 20 wt% of a preceramic polymer were warm-pressed and treated in the range of 900 -1500°C to produce alumina based composites. The obtained composites were analyzed by linear shrinkage and compared to pure alumina samples sintered at the same temperature range. It were also evaluated the density variation and crystalline phases formed during heat treatment of alumina composites. Results showed that alumina-silicon oxycarbide and alumina-mullite composites were obtained with lower shrinkage than pure alumina samples.


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