One-Pot Synthesis of a Double-Network Hydrogel Electrolyte with Extraordinarily Excellent Mechanical Properties for a Highly Compressible and Bendable Flexible Supercapacitor

2018 ◽  
Vol 10 (35) ◽  
pp. 29684-29693 ◽  
Author(s):  
Tingrui Lin ◽  
Mengni Shi ◽  
Furong Huang ◽  
Jing Peng ◽  
Qingwen Bai ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
One Pot ◽  
Double Network ◽  
Flexible Supercapacitor ◽  
One Pot Synthesis

A Robust, One-Pot Synthesis of Highly Mechanical and Recoverable Double Network Hydrogels Using Thermoreversible Sol-Gel Polysaccharide

2013 ◽  
Vol 25 (30) ◽  
pp. 4171-4176 ◽  
Author(s):  
Qiang Chen ◽  
Lin Zhu ◽  
Chao Zhao ◽  
Qiuming Wang ◽  
Jie Zheng
Keyword(s):  
Sol Gel ◽  
One Pot ◽  
Double Network ◽  
One Pot Synthesis

One-pot synthesis of bimodal silica nanospheres and their effects on the rheological and thermal–mechanical properties of silica–epoxy composites

RSC Advances ◽  
2015 ◽  
Vol 5 (62) ◽  
pp. 50073-50081 ◽  
Author(s):  
Qian Guo ◽  
Pengli Zhu ◽  
Gang Li ◽  
Liang Huang ◽  
Yu Zhang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Epoxy Resins ◽  
Epoxy Composites ◽  
Silica Nanospheres ◽  
One Pot ◽  
One Pot Synthesis ◽  
Thermal Mechanical Properties ◽  
Modify Epoxy

Bimodal silica nanospheres were prepared in one pot and were used as reinforcement fillers to modify epoxy resins.

One-pot synthesis of poly(lactic acid) with terminal methacrylate groups for the adjustment of mechanical properties of biomaterials

2017 ◽  
Vol 27 (6) ◽  
pp. 574-576 ◽  
Author(s):  
Ilia V. Averianov ◽  
Viktor A. Korzhikov-Vlakh ◽  
Yulia E. Moskalenko ◽  
Valentina E. Smirnova ◽  
Tatiana B. Tennikova
Keyword(s):  
Mechanical Properties ◽  
Lactic Acid ◽  
Poly Lactic Acid ◽  
One Pot ◽  
One Pot Synthesis

scholarly journals High Mechanical Performance Based on Physically Linked Double Network (DN) Hydrogels

Materials ◽  
2019 ◽  
Vol 12 (20) ◽  
pp. 3333 ◽  
Author(s):  
Niu ◽  
Zhang ◽  
Shen ◽  
Sheng ◽  
Fu ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Mechanical Performance ◽  
Design Strategy ◽  
Hydroxyethyl Cellulose ◽  
One Pot ◽  
Double Network ◽  
Polyhydroxy Compounds ◽  
Potential Applications ◽  
Cellulose Composite ◽  
Biomedical Fields

A new design strategy was proposed to improve the mechanical performance of double network (DN) hydrogels by introducing polyhydroxy compounds into the DN structure and form a physically linked double network through the interaction of hydrogen bonding. Herein, agar/poly(acrylic acid)/hydroxyethyl cellulose composite hydrogels could be prepared by a simple one-pot method. The resulting hydrogels exhibit highly mechanical properties and excellent recoverability, which have potential applications in biomedical fields.

Flexible superhydrophobic polysiloxane aerogels for oil–water separation via one-pot synthesis in supercritical CO2

RSC Advances ◽  
2015 ◽  
Vol 5 (93) ◽  
pp. 76346-76351 ◽  
Author(s):  
Fangxin Zou ◽  
Li Peng ◽  
Wenxin Fu ◽  
Jianling Zhang ◽  
Zhibo Li
Keyword(s):  
Mechanical Properties ◽  
Robust Stability ◽  
Supercritical Co2 ◽  
One Pot ◽  
Water Separation ◽  
One Pot Synthesis ◽  
Oil Water Separation ◽  
Oil Water

A flexible polysiloxane aerogel synthesized using a green, one-pot method possesses extraordinary mechanical properties and robust stability, and exhibits great potential in oil–water separation.

scholarly journals Swelling and Mechanical Properties of Polyacrylamide-derivative Dual-Crosslink Hydrogels Having Metal–Ligand Coordination Bonds as Transient Crosslinks

Gels ◽  
2021 ◽  
Vol 7 (2) ◽  
pp. 72
Author(s):  
Louis Debertrand ◽  
Jingwen Zhao ◽  
Costantino Creton ◽  
Tetsuharu Narita
Keyword(s):  
Mechanical Properties ◽  
Model Systems ◽  
Diffusion Method ◽  
Swelling Ratio ◽  
One Pot ◽  
Swelling Properties ◽  
One Pot Synthesis ◽  
Ligand Coordination ◽  
Coordination Bonds ◽  
Metal Ligand

Hydrogels that have both permanent chemical crosslinks and transient physical crosslinks are good model systems to represent tough gels. Such “dual-crosslink” hydrogels can be prepared either by simultaneous polymerization and dual crosslinking (one-pot synthesis) or by diffusion/complexation of the physical crosslinks to the chemical network (diffusion method). To study the effects of the preparation methods and of the crosslinking ratio on the mechanical properties, the equilibrium swelling of the dual-crosslink gels need to be examined. Since most of these gels are polyelectrolytes, their swelling properties are complex, so no systematic study has been reported. In this work, we synthesized model dual-crosslink gels with metal–ligand coordination bonds as physical crosslinks by both methods, and we proposed a simple way of adding salt to control the swelling ratio prepared by ion diffusion. Tensile and linear rheological tests of the gels at the same swelling ratio showed that during the one-pot synthesis, free radical polymerization was affected by the transition metal ions used as physical crosslinkers, while the presence of electrostatic interactions did not affect the role of the metal complexes on the mechanical properties.

One Pot Synthesis of Multifunctional Aramid Aerogels

2012 ◽  
Vol 1403 ◽  
Author(s):  
Chakkaravarthy Chidambareswarapattar ◽  
Dhairyashil P. Mohite ◽  
Zachary J. Larimore ◽  
Hongbing Lu ◽  
Chariklia Sotiriou-Leventis ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Three Dimensional ◽  
Cross Linking ◽  
One Pot ◽  
High Mechanical Strength ◽  
Electrically Conducting ◽  
New Class ◽  
One Pot Synthesis ◽  
Surface Areas ◽  
High Specific Energy

ABSTRACTAerogels are quasi-stable, low-density, three-dimensional assemblies of nanoparticles, but they are commonly associated with poor mechanical properties. The most successful efforts to improve their mechanical properties involve cross-linking of the skeletal nanoparticles with polymers. However, post gelation cross-linking is time-consuming. Hence, it is reasonable to seek robust all-polymer aerogels among polymers known for their high mechanical strength. As a result, here we report the facile one-pot synthesis of a new class of Kevlar-like aerogels based on the rather underutilized reaction of multifunctional isocyanates and carboxylic acids. The resulting materials are up to 84% v/v porous with surface areas as high as 380 m2 g-1. The ultimate compressive strength per unit density is within 10% equal to that of Kevlar 49. The high specific energy absorption (37 J g-1) and Styrofoam-like thermal conductivity (0.028 W m-1 K-1) combined with thermal stability up to 350 °C render aramid aerogels multifunctional materials suitable for defense, civil and transportation related applications. Upon pyrolysis at 800 °C they can be converted to 80% (v/v) porous, electrically conducting carbons with surface areas as high as 474 m2 g-1.

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