NMR Crystallography of Aluminum Carbide: Impurities in the Reagent and Improved 27Al NMR Tensors

2020 ◽  
Vol 124 (13) ◽  
pp. 7238-7243 ◽  
Author(s):  
Robert M. Marti ◽  
Vincent Sarou-Kanian ◽  
Colton M. Moran ◽  
Krista S. Walton ◽  
Sophia E. Hayes
Keyword(s):  
Aluminum Carbide ◽  
27Al Nmr ◽  
Nmr Tensors ◽  
Nmr Crystallography

High temperature 27Al NMR time resolved study. Application to the CaO-Al2O3 binary system

1995 ◽  
Vol 92 ◽  
pp. 1871-1876 ◽  
Author(s):  
B Touzo ◽  
D Trumeau ◽  
D Massiot ◽  
I Farnan ◽  
JP Coutures
Keyword(s):  
High Temperature ◽  
Binary System ◽  
27Al Nmr ◽  
Time Resolved ◽  
Study Application

27Al NMR Study in UNiAl

2000 ◽  
Vol 18 (1-4) ◽  
pp. 53-58 ◽  
Author(s):  
Bogdan Nowak ◽  
Robert Troć
Keyword(s):  
27Al Nmr ◽  
Nmr Study

A Study of Silver Species on Silver-Exchanged ETS-10 and Mordenite by XRD, SEM and Solid-State 109Ag, 29Si and 27Al NMR Spectroscopy

2012 ◽  
Vol 12 (8) ◽  
pp. 6420-6427 ◽  
Author(s):  
Yan Liu ◽  
Fu Chen ◽  
Roderick E. Wasylishen ◽  
Zhenghe Xu ◽  
James Sawada ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
27Al Nmr ◽  
27Al Nmr Spectroscopy

Design and Use of Background-Reduced 27Al NMR Probes for the Study of Dilute Samples from the Environment

1995 ◽  
Vol 49 (2) ◽  
pp. 156-162 ◽  
Author(s):  
Janet S. MacFall ◽  
Anthony A. Ribeiro ◽  
Gary P. Cofer ◽  
Ko-Hsiu G. Dai ◽  
William Labiosa ◽  
...  
Keyword(s):  
Environmental Samples ◽  
Natural Waters ◽  
Background Signal ◽  
27Al Nmr ◽  
Sample Container ◽  
Al Content ◽  
Free Sample ◽  
External Reference ◽  
Soil Solutions ◽  
Colorimetric Assays

Development of methods for the detection and measurement of aluminum (Al) is crucial for our understanding of Al(III) chemistry and toxicity in natural waters, soil solutions, and environmental samples. Traditional colorimetric assays, by their very nature, alter solution Al(III) chemistry, potentially biasing measurements. Methods based on 27Al NMR spectroscopy have the advantage of being nondestructive and of not altering the chemistry of the solution. Standard commercial NMR probes and sample tubes, unfortunately, are constructed from aluminum-containing components. These materials give substantial background signal, which is detected as a large, broad hump, overwhelming signals from dilute samples. We describe here the construction of two novel NMR probes and a sample container built from a variety of materials with low Al content. The designs feature the use of transversely mounted solenoid coils with aluminum-free sample holders. The sample container features a second chamber which can be filled with an external reference solution. These novel 27Al NMR probes are being used for the NMR spectroscopic investigation and quantitation of natural, dilute (10−6 M) Al(III) samples from the environment.

Mechanochemical synthesis of γ-LiAlO2 studied by 6Li and 27Al NMR and synchrotron X-Ray diffraction

2011 ◽  
Vol 47 (7) ◽  
pp. 763-767 ◽  
Author(s):  
V. P. Isupov ◽  
O. A. Kharlamova ◽  
L. E. Chupakhina ◽  
M. R. Sharafutdinov ◽  
D. F. Khabibulin ◽  
...  
Keyword(s):  
Mechanochemical Synthesis ◽  
X Ray Diffraction ◽  
27Al Nmr ◽  
X Ray

Crystal structure and magnetic properties of Al2O3 nanoparticles by 27Al NMR data

2017 ◽  
Vol 59 (3) ◽  
pp. 514-519 ◽  
Author(s):  
K. N. Mikhalev ◽  
A. Yu. Germov ◽  
A. E. Ermakov ◽  
M. A. Uimin ◽  
A. L. Buzlukov ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Magnetic Properties ◽  
Al2o3 Nanoparticles ◽  
27Al Nmr ◽  
Nmr Data

scholarly journals NMR Crystallography

2017 ◽  
Vol 73 (3) ◽  
pp. 126-127 ◽  
Author(s):  
David L. Bryce ◽  
Francis Taulelle
Keyword(s):  
Nmr Crystallography

27Al NMR Study of Coordination States of Aluminum-tri-sec-butoxide Dissolved in Diacetone Alcohol

1994 ◽  
Vol 23 (8) ◽  
pp. 1507-1510 ◽  
Author(s):  
Kiyoharu Tadanaga ◽  
Tsutomu Minami ◽  
Noboru Tohge
Keyword(s):  
27Al Nmr ◽  
Diacetone Alcohol ◽  
Nmr Study

scholarly journals A 27Al NMR study of the interaction of water with AlPO4-11

1992 ◽  
pp. 1560 ◽  
Author(s):  
Mart P. J. Peeters ◽  
Jan W. de Haan ◽  
Leo J. M. van de Ven ◽  
Jan H. C. van Hooff
Keyword(s):  
27Al Nmr ◽  
Nmr Study
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