X-ray Diffraction Analysis of Hexagonal Klockmannite CuSe Nanoparticles for Photodetectors under UV Light

2021 ◽  
Vol 125 (6) ◽  
pp. 3517-3526
Author(s):  
Kunjal Patel ◽  
G. K. Solanki ◽  
K. D. Patel ◽  
V. M. Pathak
Keyword(s):  
Diffraction Analysis ◽  
Uv Light ◽  
X Ray Diffraction ◽  
X Ray

scholarly journals Treatment and Nursing Values of Cd(II) Complex with Photocatalytic Activity on Bacterial Infection by Inhibiting the Gram-Positive Bacteria Growth

2021 ◽  
Vol 2021 ◽  
pp. 1-8
Author(s):  
Jing Peng ◽  
Quan-Zhen Tang ◽  
Jian Lu ◽  
Yan Hu ◽  
Jiao Ni
Keyword(s):  
Photocatalytic Activity ◽  
Bacterial Infection ◽  
Diffraction Analysis ◽  
Uv Light ◽  
Bacterial Survival ◽  
X Ray Diffraction ◽  
X Ray ◽  
Bacteria Growth ◽  
Survival Gene ◽  
Nursing Values

Presented here is a trinuclear cluster-based Cd(II) compound, namely, {[(CH3)2NH2][Cd6K(bdc)6(btz)3(H2O)6]}n (1 H2bdc = terephthalic acid, Hbtz = 1H-benzotriazole), has been solvothermally prepared and structurally determined by the single crystal X-ray diffraction analysis, elemental analysis, powder X-ray diffraction analysis, and thermogravimetric analysis. Notably, compound 1 shows excellent photocatalytic activity for degradation of MV irradiated by UV light. In addition to this, the biological activity of the new compound on bacterial infection was evaluated, and the corresponding mechanism was also studied. The ELISA assay was used to evaluate the TNF-α and IL-1β released into plasma after compound treatment. Then, the relative expression levels of the bacterial survival gene were measured with real-time RT-PCR.

scholarly journals Coordination of the ambiphilic phosphinoborane tBu2PCH2BPh2 to Cu(I)Cl

2017 ◽  
Vol 72 (11) ◽  
pp. 781-784 ◽  
Author(s):  
Devin H.A. Boom ◽  
Andreas W. Ehlers ◽  
Martin Nieger ◽  
J. Chris Slootweg
Keyword(s):  
Molecular Structure ◽  
Single Crystal ◽  
Diffraction Analysis ◽  
Uv Light ◽  
Metal Center ◽  
X Ray Diffraction ◽  
Green Fluorescence ◽  
X Ray

AbstractA chloro-bridged dimeric copper(I) complex with the ambiphilic phosphinoborane ligand tBu2PCH2BPh2 is reported. The molecular structure was determined by single-crystal X-ray diffraction analysis, revealing a secondary η1-C interaction of the ligand with the metal center. The complex exhibits green fluorescence when exposed to UV light at 366 nm.

Ten-Vertex Polyhedral Monocarbaborane Chemistry. The Novel High-Yield Formation of the Ten-Vertex closo Compound [6-(PMe2Ph)-closo-1-CB9H9] from the Thermolysis of [8,8-(PMe2Ph)2-nido-8,7-PtCB9H11]

1993 ◽  
Vol 58 (12) ◽  
pp. 2924-2935 ◽  
Author(s):  
Jane H. Jones ◽  
Bohumil Štíbr ◽  
John D. Kennedy ◽  
Mark Thornton-Pett
Keyword(s):  
Nmr Spectroscopy ◽  
Diffraction Analysis ◽  
High Yield ◽  
Monoclinic Space Group ◽  
The Novel ◽  
X Ray Diffraction ◽  
Metal Centre ◽  
X Ray ◽  
Yield Formation ◽  
Boiling Toluene

Thermolysis of [8,8-(PMe2Ph)2-nido-8,7-PtCB9H11] in boiling toluene solution results in an elimination of the platinum centre and cluster closure to give the ten-vertex closo species [6-(PMe2Ph)-closo-1-CB9H9] in 85% yield as a colourles air stable solid. The product is characterized by NMR spectroscopy and single-crystal X-ray diffraction analysis. Crystals (from hexane-dichloromethane) are monoclinic, space group P21/c, with a = 903.20(9), b = 1 481.86(11), c = 2 320.0(2) pm, β = 97.860(7)° and Z = 8, and the structure has been refined to R(Rw) = 0.045(0.051) for 3 281 observed reflections with Fo > 2.0σ(Fo). The clean high-yield elimination of a metal centre from a polyhedral metallaborane or metallaheteroborane species is very rare.

Bis(μ-carboxylato)dienerhodium(I) Complexes - Synthesis, Characterization and Catalytic Activity

2008 ◽  
Vol 73 (8-9) ◽  
pp. 1205-1221 ◽  
Author(s):  
Jiří Zedník ◽  
Jan Sedláček ◽  
Jan Svoboda ◽  
Jiří Vohlídal ◽  
Dmitrij Bondarev ◽  
...  
Keyword(s):  
Catalytic Activity ◽  
Diffraction Analysis ◽  
Spectroscopic Methods ◽  
X Ray Diffraction ◽  
X Ray

Dinuclear rhodium(I) η2:η2-cycloocta-1,5-diene (series a) and η2:η2-norborna-2,5-diene (series b) complexes with μ-RCOO- ligands, where R is linear C21H43 (complexes 1a, 1b), CH2CMe3 (2a, 2b), 1-adamantyl (3a, 3b) and benzyl (4a, 4b), have been prepared and characterized by spectroscopic methods. Structures of complexes 2b, 3a and 4a were determined by X-ray diffraction analysis. Complexes prepared show low to moderate catalytic activity in polymerization of phenylacetylene in THF giving high-cis-transoid polymers, but they show only oligomerization activity in dichloromethane.

scholarly journals Crystals of the trp repressor-operator complex suitable for X-ray diffraction analysis.

1987 ◽  
Vol 262 (10) ◽  
pp. 4917-4921 ◽  
Author(s):  
A. Joachimiak ◽  
R.Q. Marmorstein ◽  
R.W. Schevitz ◽  
W. Mandecki ◽  
J.L. Fox ◽  
...  
Keyword(s):  
Diffraction Analysis ◽  
X Ray Diffraction ◽  
Trp Repressor ◽  
X Ray
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