Role of Capping Agent in Wet Synthesis of Nanoparticles

2017 ◽  
Vol 121 (17) ◽  
pp. 3213-3219 ◽  
Author(s):  
Chi M. Phan ◽  
Hoang M. Nguyen
2001 ◽  
Vol 704 ◽  
Author(s):  
Tommy J. Wilkinson ◽  
Dale L. Perry ◽  
Erik Spiller ◽  
Paul Berdahl ◽  
Stephen E. Derenzo ◽  
...  

AbstractThe red, tetragonal form of lead oxide, α-PbO, litharge, has been synthesized in the nanoparticle range using a rapid, one-step reaction sequence using water as the reaction medium. The product was characterized by powder x-ray diffraction and scanning electron microscopy. With time at room temperature, the original material slowly changed in color intensity, indicating its alteration to β-PbO, massicot. Grinding the aged material converted it back to the original litharge form. The role of impurities in the experimental synthesis of the material and microstructural variations in the final product are discussed, along with the PbO-phase compositions of commercial products.


2021 ◽  
Author(s):  
Sapana Jadoun ◽  
Narendra Pal Singh Chauhan ◽  
Payam Zarrintaj ◽  
Mahmood Barani ◽  
Rajender S. Varma

Abstract Nanotechnology has permeated all areas of sciences as one of the most propitious technology with the deployment of nanoparticles in environmental remediation and biomedical fields; their synthesis under greener conditions has been bourgeoned using microorganisms, plants, etc. to decrease the use of toxic chemicals. Synthesis of nanoparticles by exploiting microorganisms has opened up a new prospect at the interface of nanotechnology, chemistry, and biology enabling access via a biocompatible, safe, sustainable, eco-friendly, and reliable route; microorganisms offer crystal growth, stabilization, and prevention of aggregation thus performing a dual role of reducing and capping agent because of the presence of biomolecules such as enzymes, peptides, poly (amino acids), polyhydroxyalkanoate (PHA), and polysaccharides. Herein, the microorganisms-based synthesis of various nanoparticles comprising gold, silver, platinum, palladium, copper, titanium dioxide, zinc oxide, iron oxide, and selenium along with their appliances in waste treatment, biomedicine namely cancer treatment, antibacterial, antimicrobial, antifungal, and antioxidants, are deliberated.


2021 ◽  
Vol 13 (4) ◽  
pp. 1781
Author(s):  
Gaurav Chugh ◽  
Kadambot H. M. Siddique ◽  
Zakaria M. Solaiman

Nanobiotechnology in agriculture is a driver for modern-day smart, efficient agricultural practices. Nanoparticles have been shown to stimulate plant growth and disease resistance. The goal of sustainable farming can be accomplished by developing and sustainably exploiting the fruits of nanobiotechnology to balance the advantages nanotechnology provides in tackling environmental challenges. This review aims to advance our understanding of nanobiotechnology in relevant areas, encourage interactions within the research community for broader application, and benefit society through innovation to realize sustainable agricultural practices. This review critically evaluates what is and is not known in the domain of nano-enabled agriculture. It provides a holistic view of the role of nanobiotechnology in multiple facets of agriculture, from the synthesis of nanoparticles to controlled and targeted delivery, uptake, translocation, recognition, interaction with plant cells, and the toxicity potential of nanoparticle complexes when presented to plant cells.


Small ◽  
2016 ◽  
Vol 12 (25) ◽  
pp. 3444-3452 ◽  
Author(s):  
Maryam Hajfathalian ◽  
Kyle D. Gilroy ◽  
Robert A. Hughes ◽  
Svetlana Neretina
Keyword(s):  

2017 ◽  
Vol 6 (2) ◽  
Author(s):  
Nokwethemba Precious Sibiya ◽  
Makwena Justice Moloto

AbstractEmploying a capping agent during the synthesis of nanoparticles has been reported to play a role in controlling size and shape of the nanoparticles. Due to this reason, this study reports the synthesis of silver selenide nanoparticles using different environmentally friendly capping agents (green tea, glucose, ascorbic acid and chitosan) in order to investigate their effect on the size and shape of the nanoparticles. Transmission electron microscopy (TEM) results showed that the nanoparticles have different shapes (rods, spheres and cubes) with an average size of 8–96 nm depending on the capping agent used. Fourier transformer infrared (FTIR) spectroscopy confirmed that the capping of nanoparticles was successful, while X-ray diffraction (XRD) showed that the nanoparticles have an orthorhombic phase.


2015 ◽  
Vol 39 (5) ◽  
pp. 3948-3955 ◽  
Author(s):  
Sahar Zinatloo-Ajabshir ◽  
Masoud Salavati-Niasari

Triethylenetetramine with high hindrance in the presence of PEG plays a role of a co-capping agent for the Pr(OH)3 nanoparticles.


2020 ◽  
Vol 9 (3) ◽  
pp. 1427-1443

Nanotechnology is an escalating branch whose feelers are mesmerizing nearly every field of science. It is the evolving field in forensic science, the advancement of emergent techniques of nanoparticles being unified with latent fingerprinting. The size of nanomaterials made them unique and have adjustable mechanical, electrical, and optical properties. At the crime scene, the prints that are left behind are generally latent (invisible) fingerprints. The Current review paper encompasses the synthesis of nanoparticles from conventional and advances synthetic pathways. Their applications, with and without modifications and their impacts on the enhancement of latent fingerprints, have also been discussed.


2016 ◽  
Vol 8 (2) ◽  
pp. 1039-1048 ◽  
Author(s):  
Manpreet Kaur ◽  
Anu Kalia

Synthesis of nanoparticles (NPs) having unique potentials and properties is of great importance in nanotechnology. The NP synthesis techniques may include the wet chemistry to microbial incubation reduction methods. This work reports generation of ZnO NPs by identical preparation including incubation of different zinc salts i.e. zinc acetate, zinc chloride and zinc sulphate as precursors with cell free extracts of Bacillus circulans MTCC 7906 (Bc7906) and Pleurotus florida (Pf). The synthesized NPs exhibited variation in their absorption peaks in UV-Vis spectra which appeared at 275 nm, 325 nm and 375 nm with P. florida for the three salt precursors respectively while the Bc7906 generated ZnO NPs showed peaks between 300-350 nm. A variation in ZnO NP morphology ranged from 50 to 120 nm in size and spherical, oval, cylindrical to trigonal anisotropic in shape by transmission EM. Further, the rough and corrugated surface topography of ZnO NPs was observed in Scanning EM. The % weight for Zn element surface composition as recorded by SEM-EDS was observed to be highest for zinc acetate (2.34%) and zinc sulphate (7.54 %) on microbial synthesis from Bc7906 and Pf respectively. The antimicrobial potential of the synthesized ZnO NPs on human pathogenic and plant beneficial bacteria was tested and it was observed to be highest for microbially synthesized ZnO NPs using zinc acetate (15 mm) and zinc sulphate (14 mm) as salt precursors @ 10 ppm. This is the first report on differential antimicrobial behavior of ZnO NPs on human pathogenic and plant beneficial microbes.


Catalysts ◽  
2016 ◽  
Vol 6 (12) ◽  
pp. 185 ◽  
Author(s):  
Sebastiano Campisi ◽  
Marco Schiavoni ◽  
Carine Chan-Thaw ◽  
Alberto Villa

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