Analysis by UPLC–DAD–ESI-MS of Phenolic Compounds and HPLC–DAD-Based Determination of Carotenoids in Noni (Morinda citrifolia L.) Bagasse

2019 ◽  
Vol 67 (26) ◽  
pp. 7365-7377 ◽  
Author(s):  
Claudia Barraza-Elenes ◽  
Irma L. Camacho-Hernández ◽  
Elhadi M. Yahia ◽  
José J. Zazueta-Morales ◽  
Ernesto Aguilar-Palazuelos ◽  
...  
Molecules ◽  
2019 ◽  
Vol 24 (4) ◽  
pp. 677 ◽  
Author(s):  
Federica Pasini ◽  
Fabio Chinnici ◽  
Maria Caboni ◽  
Vito Verardo

Grape seeds are a copious part of the grape pomace produced by wine and juice industry and they represent an interesting source of phenolic compounds. Proanthocyanidins (PAs) are the main class of grape seed phenols and are important dietary supplements for their well-known beneficial properties. In this study enriched extracts obtained from Chardonnay and Pignoletto grape seeds were characterized for their proanthocyanidins and other minor phenolic compounds content and composition. Seed PAs were fractionated using Sephadex LH-20, using different ethanol aqueous solutions as mobile phase and analysed by normal phase HPLC-FLD-ESI-MS. Monomers, oligomers up to dodecamers and polymers were recorded in all samples. For both cultivars, the extracts showed a high content in PAs. The determination of other phenolic compounds was carried out using a HPLC-QqQ-ESI-MS and Chardonnay samples reported a greater content compared to Pignoletto samples. Contrary to PAs fraction, extracts obtained with ethanol/water 50/50 (v/v) presented a significant higher phenolic content than the others.


Molecules ◽  
2020 ◽  
Vol 25 (8) ◽  
pp. 1804 ◽  
Author(s):  
Marta Olech ◽  
Wioleta Pietrzak ◽  
Renata Nowak

Fast and reliable determination of polyphenols is a quite common goal during investigation of new plant materials and herbal products, their standardization, quality control, or chemo-taxonomical studies. The aim of this study was to develop and validate methods based on the application of reversed phase liquid chromatography/electrospray ionization triple quadrupole mass spectrometry (LC-ESI-MS/MS) using multiple reaction monitoring (MRM) for comprehensive quantitative and qualitative analysis of phenolic acids and flavonoid aglycones. LC-MS/MS-MRM protocols were applied for the determination of free and bound phenolics in a series of plant samples prepared from leaves and achenes (true fruits) of Japanese rose (Rosa rugosa Thunb.). The presence of large amount of phenolic compounds was detected in rose leaves (786.44 µg/g and 14.46 µg/g of phenolic acids and flavonoid aglycones, respectively). Isoferulic acid and five aglycones were revealed for the first time in this plant material. Moreover, 15 phenolic acids and six aglycones were found in the rose achenes, including eight phenolic acids and four aglycones that had not been previously reported in this rose organ. It was shown that leaves and achenes may constitute an industrially relevant source of phenolic compounds for potential commercial use in pharmaceutical, food, or cosmetic industry.


2017 ◽  
Vol 52 (4) ◽  
pp. 954-963 ◽  
Author(s):  
Eliza Mariane Rotta ◽  
Charles Windson Isidoro Haminiuk ◽  
Liane Maldaner ◽  
Jesuí Vergilio Visentainer

2016 ◽  
Vol 87 ◽  
pp. 60-67 ◽  
Author(s):  
Siluana Katia Tischer Seraglio ◽  
Andressa Camargo Valese ◽  
Heitor Daguer ◽  
Greici Bergamo ◽  
Mônia Stremel Azevedo ◽  
...  

2013 ◽  
Vol 61 (22) ◽  
pp. 5328-5337 ◽  
Author(s):  
Ana María Gómez-Caravaca ◽  
Vito Verardo ◽  
Moreno Toselli ◽  
Antonio Segura-Carretero ◽  
Alberto Fernández-Gutiérrez ◽  
...  
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