scholarly journals Comprehensive Characterization of Extractable and Nonextractable Phenolic Compounds by High-Performance Liquid Chromatography–Electrospray Ionization–Quadrupole Time-of-Flight of a Grape/Pomegranate Pomace Dietary Supplement

2018 ◽  
Vol 66 (3) ◽  
pp. 661-673 ◽  
Author(s):  
Iza F. Pérez-Ramírez ◽  
Rosalía Reynoso-Camacho ◽  
Fulgencio Saura-Calixto ◽  
Jara Pérez-Jiménez
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
Phenolic Compounds ◽  
Electrospray Ionization ◽  
Dietary Supplement ◽  
High Performance ◽  
Time Of Flight ◽  
Comprehensive Characterization

Rapid Detection and Characterization of Steroidal Saponins in the Root of Asparagus cochinchinensis by High-Performance Liquid Chromatography Coupled to Electrospray Ionization and Quadrupole Time-of-Flight Mass Spectrometry

2020 ◽  
Vol 58 (5) ◽  
pp. 454-463
Author(s):  
Yun Ling ◽  
Xin He ◽  
Renliang Jiang ◽  
Qi Zhang ◽  
Shuqin Yuan ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
Electrospray Ionization ◽  
High Performance ◽  
Time Of Flight ◽  
Steroidal Saponins ◽  
Flight Mass Spectrometry ◽  
Asparagus Cochinchinensis

Abstract The dried root of Asparagus cochinchinensis (RAC) has been used as an important traditional Chinese medicine for a long time in China. Steroidal saponins (SSs) are considered to be the main active ingredients of this herb. However, the isolation and structural determination of SSs from RAC are time-consuming and laborious. For this reason, the development of new methods for the separation and characterization of SSs is highly desirable. In this study, a new high-performance liquid chromatography coupled to electrospray ionization and quadrupole time-of-flight mass spectrometry (HPLC-ESI-QTOF-MS/MS) method with precursor ions and the corresponding fragment ions was developed for the identification of SSs in RAC. Finally, 30 SSs have been detected and identified, including 17 potential new compounds. This is the first systematic study of SSs in RAC by HPLC-ESI-QTOF-MS/MS method.

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