Nicotinamide Riboside Derivatives: Single Crystal Growth and Determination of X-ray Structures

2019 ◽  
Vol 19 (7) ◽  
pp. 4019-4028 ◽  
Author(s):  
Ricardo Alvarez ◽  
Günter Schabert ◽  
Aysel Soydemir ◽  
Lukas Wick ◽  
Urs Spitz ◽  
...  
Keyword(s):  
Crystal Growth ◽  
Single Crystal ◽  
Single Crystal Growth ◽  
X Ray ◽  
Nicotinamide Riboside

Single Crystal Growth of High-Pressure Phases of Ice and Salt Hydrate Far Below the Original Melting Point by Mixing Alcohol: Crystal Structure Determination of Magnesium Chloride Heptahydrate

2020 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Hiroyuki Kagi
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Crystal Growth ◽  
Single Crystal ◽  
Room Temperature ◽  
Growth Technique ◽  
Salt Hydrate ◽  
X Ray

An crystal-growth technique for single crystal x-ray structure analysis of high-pressure forms of hydrogen-bonded crystals is proposed. We used alcohol mixture (methanol: ethanol = 4:1 in volumetric ratio), which is a widely used pressure transmitting medium, inhibiting the nucleation and growth of unwanted crystals. In this paper, two kinds of single crystals which have not been obtained using a conventional experimental technique were obtained using this technique: ice VI at 1.99 GPa and MgCl<sub>2</sub>·7H<sub>2</sub>O at 2.50 GPa at room temperature. Here we first report the crystal structure of MgCl2·7H2O. This technique simultaneously meets the requirement of hydrostaticity for high-pressure experiments and has feasibility for further in-situ measurements.

Single Crystal Growth and Structure Determination of the Natural “High Potency” Sweetener Rebaudioside A

2012 ◽  
Vol 12 (2) ◽  
pp. 990-993 ◽  
Author(s):  
Mani Upreti ◽  
Jared P. Smit ◽  
Eric J. Hagen ◽  
Valeriya N. Smolenskaya ◽  
Indra Prakash
Keyword(s):  
Crystal Growth ◽  
Single Crystal ◽  
Structure Determination ◽  
Single Crystal Growth ◽  
Rebaudioside A ◽  
High Potency

Kristallzucht und Strukturaufklärung von K2[Pt(CN)4Cl2], K2[Pt(CN)4Br2], K2[Pt(CN)4I2] und K2[Pt(CN)4Cl2] · 2H2O/ Crystal Growth and Crystal Structure Determination of K2[Pt(CN)4Cl2], K2[Pt(CN)4Br2], K2[Pt(CN)4I2] and K2[Pt(CN)4]Cl2] · 2H2O

2004 ◽  
Vol 59 (5) ◽  
pp. 567-572 ◽  
Author(s):  
Claus Mühle ◽  
Andrey Karpov ◽  
Jürgen Nuss ◽  
Martin Jansen
Keyword(s):  
Crystal Structure ◽  
Infrared Spectroscopy ◽  
Crystal Growth ◽  
Single Crystal ◽  
Structure Determination ◽  
Spectroscopy Data ◽  
Crystal Data ◽  
X Ray ◽  
Raman And Infrared Spectroscopy

Abstract Crystals of K2Pt(CN)4Br2, K2Pt(CN)4I2 and K2Pt(CN)4Cl2 ·2H2O were grown, and their crystal structures have been determined from single crystal data. The structure of K2Pt(CN)4Cl2 has been determined and refined from X-ray powder data. All compounds crystallize monoclinicly (P21/c; Z = 2), and K2Pt(CN)4X2 with X = Cl, Br, I are isostructural. K2Pt(CN)4Cl2: a = 708.48(2); b = 903.28(3); c = 853.13(3) pm; β = 106.370(2)°; Rp = 0.064 (N(hkl) = 423). K2Pt(CN)4Br2: a = 716.0(1); b = 899.1(1); c = 867.9(1) pm; β = 106.85(1)°; R(F)N′ = 0.026 (N’(hkl) = 3757). K2Pt(CN)4I2: a = 724.8(1); b = 914.5(1); c = 892.1(1) pm; β = 107.56(1)°; R(F)N′ = 0.025 (N’(hkl) = 2197). K2Pt(CN)4Cl2 ·2H2O: a = 763.76(4); b = 1143.05(6); c = 789.06(4) pm; β = 105.18(1)°; R(F)N′ = 0.021 (N’(hkl) = 2281). Raman and infrared spectroscopy data are reported.

scholarly journals Single crystal growth and structure determination of Rb1.5Mn8O16 hollandite.

1990 ◽  
Vol 15 (2) ◽  
pp. 41-49 ◽  
Author(s):  
Naoichi YAMAMOTO ◽  
Yoshio OKA ◽  
Osamu TAMADA
Keyword(s):  
Crystal Growth ◽  
Single Crystal ◽  
Structure Determination ◽  
Single Crystal Growth

Single-crystal growth and structure determination of misfit layer oxide [Sr2TlO3][CoO2]1.77

2007 ◽  
Vol 306 (1) ◽  
pp. 233-239 ◽  
Author(s):  
Markus Valkeapää ◽  
Martin Valldor ◽  
Sven Lidin ◽  
Tomasz Lada ◽  
Andrzej Morawski ◽  
...  
Keyword(s):  
Crystal Growth ◽  
Single Crystal ◽  
Structure Determination ◽  
Single Crystal Growth

Single Crystal Growth of High-Pressure Phases of Ice and Salt Hydrate Far Below the Original Melting Point by Mixing Alcohol: Crystal Structure Determination of Magnesium Chloride Heptahydrate

2019 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Hiroyuki Kagi
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Crystal Growth ◽  
Single Crystal ◽  
Room Temperature ◽  
Growth Technique ◽  
Salt Hydrate ◽  
X Ray

An crystal-growth technique for single crystal x-ray structure analysis of high-pressure forms of hydrogen-bonded crystals is proposed. We used alcohol mixture (methanol: ethanol = 4:1 in volumetric ratio), which is a widely used pressure transmitting medium, inhibiting the nucleation and growth of unwanted crystals. In this paper, two kinds of single crystals which have not been obtained using a conventional experimental technique were obtained using this technique: ice VI at 1.99 GPa and MgCl<sub>2</sub>·7H<sub>2</sub>O at 2.51 GPa at room temperature. Here we first report the crystal structure of MgCl2·7H2O. This technique simultaneously meets the requirement of hydrostaticity for high-pressure experiments and has feasibility for further in-situ measurements.

Single-Crystal Growth and Structure Determination of a New Oxide Apatite, NaLa9(GeO4)6O2

1998 ◽  
Vol 139 (2) ◽  
pp. 304-309 ◽  
Author(s):  
Masaru Takahashi ◽  
Kazuyoshi Uematsu ◽  
Zuo-Guang Ye ◽  
Mineo Sato
Keyword(s):  
Crystal Growth ◽  
Single Crystal ◽  
Structure Determination ◽  
Single Crystal Growth

Die Kristall- und Molekülstruktur von Tris(dimethylamino)boran / The Crystal and Molecular Structure of Tris(dimethylamino)borane

1982 ◽  
Vol 37 (10) ◽  
pp. 1230-1233 ◽  
Author(s):  
Günter Schmid ◽  
Roland Boese ◽  
Dieter Bläser
Keyword(s):  
Molecular Structure ◽  
Crystal Growth ◽  
Single Crystal ◽  
Room Temperature ◽  
Crystal And Molecular Structure ◽  
Melting Process ◽  
Single Crystal Growth ◽  
Zone Melting ◽  
X Ray Diffraction ◽  
X Ray

Abstract Tris(dimethylamino)borane, X-ray The crystal and molecular structure of tris(dimethylamino)borane, a liquid at room temperature, has been determined by single-crystal X-ray diffraction methods at - 116°C. The single-crystal growth was accomplished by means of a miniature zone melting process on the diffractometer. The structure data are compared with those of other aminoboranes.

On the Structure of Carbon Films Deposited on Si(111) by Mass-Selected Low Energy C+ Beams

1989 ◽  
Vol 152 ◽  
Author(s):  
J. L. Robertson ◽  
X. G. Jiang ◽  
P. C. Chow ◽  
S. C. Moss ◽  
Y. Lifshitz ◽  
...  
Keyword(s):  
Raman Spectrum ◽  
Crystal Growth ◽  
Single Crystal ◽  
Single Crystals ◽  
Ion Beam ◽  
Diamond Films ◽  
Single Crystal Growth ◽  
Carbon Films ◽  
Low Energy ◽  
X Ray

ABSTRACTOur recent report of epitaxial single crystal growth of C+ ion-beam-deposited diamond films on (111) single crystals of silicon is shown to be incorrect. We briefly describe the circumstances leading to this revision (and to our earlier finding) and discuss the possible structure of these films based on preliminary synchrotron X-ray data and on the Raman spectrum.

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