Separation of trace metal impurities from nuclear grade uranium by long-chain amine extraction and direct determination by atomic absorption spectrophotometry

1974 ◽  
Vol 46 (12) ◽  
pp. 1812-1814 ◽  
Author(s):  
Sergio. De Moraes ◽  
Alcidio. Abrao
Keyword(s):  
Trace Metal ◽  
Atomic Absorption ◽  
Direct Determination ◽  
Atomic Absorption Spectrophotometry ◽  
Nuclear Grade ◽  
Absorption Spectrophotometry ◽  
Metal Impurities ◽  
Nuclear Grade Uranium ◽  
Long Chain

Spectrophotometric investigation of sensitive complexing agents for the determination of zinc in serum.

1985 ◽  
Vol 31 (8) ◽  
pp. 1310-1313 ◽  
Author(s):  
R Homsher ◽  
B Zak
Keyword(s):  
Trace Metal ◽  
Atomic Absorption ◽  
Serum Zinc ◽  
Atomic Absorption Spectrophotometry ◽  
Molar Absorptivity ◽  
Water Soluble ◽  
The Other ◽  
Complexing Agents ◽  
Absorption Spectrophotometry

Abstract Of two sensitive complexometric reagents for the colorimetry of serum zinc that we investigated, one, 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (Br-PADAP), was found to be a potentially useful compound for trace-metal determinations. It has a high molar absorptivity (120 000 L mol-1 cm-1) but is not convenient to use because it is not very soluble in water. The other reagent, a related pyridylazo compound, is 2-(5-bromo-2-pyridylazo)-5-(N-n-propyl-N-3-sulfopropylamino)phenol (5-BR-PAPS). It seems better suited for use in routine zinc determinations because, besides being water soluble, it has a higher molar absorptivity, 130 000 L mol-1 cm-1. Results by the proposed method developed with 5-Br-PAPS correlated well with those by atomic absorption spectrophotometry. The between-run CV for control sera was less than 5%; the within-run CV (same controls) was less than 4%.

Direct Determination of Nickel in Catalytic-Cracking Feedstocks by Atomic-Absorption Spectrophotometry

1966 ◽  
Vol 20 (4) ◽  
pp. 212-213 ◽  
Author(s):  
J. D. Kerber
Keyword(s):  
Detection Limit ◽  
Atomic Absorption ◽  
Catalytic Cracking ◽  
Direct Determination ◽  
Atomic Absorption Spectrophotometry ◽  
Rapid Testing ◽  
Absorption Spectrophotometry ◽  
Determination Of Nickel ◽  
No Sample Preparation

Nickel in catalytic-cracking feedstocks is determined by atomic-absorption spectrophotometry with no sample preparation other than dilution in p–xylene. A modification of the method of additions permits rapid testing with a detection limit of 0.05 ppm Ni and a precision of 0.05 ppm.

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