Automated purity determination by stepwise melting in differential scanning calorimetry

1980 ◽  
Vol 52 (9) ◽  
pp. 1474-1479 ◽  
Author(s):  
Arnold C. Ramsland
2008 ◽  
Vol 33 (4) ◽  
pp. 61-68 ◽  
Author(s):  
C. T. de Carvalho ◽  
A. B. Siqueira ◽  
E. Y. Ionashiro ◽  
M. Pivatto ◽  
M. Ionashiro

The 2-methoxycinnamylidenepyruvic acid (2-MeO-HCP) was synthesized and characterized for nuclear magnetic resonance (¹H and 13C NMR), mass spectrometry (MS), Infrared spectroscopy (FTIR) and differential scanning calorimetry (DSC). The application of DSC for purity determination is well documented in literature and is used in the analysis of pure organic compounds. The molecular geometry and vibrational frequencies of 2-MeO-HCP have been calculated.


1980 ◽  
Vol 17 (6) ◽  
pp. 231 ◽  
Author(s):  
Peter Burroughs ◽  
E. Paterson ◽  
M. I. Pope

2009 ◽  
Vol 159 (1-2) ◽  
pp. 162-165 ◽  
Author(s):  
Haifeng Wang ◽  
Jia Li ◽  
Guohua Sun ◽  
Kang Ma ◽  
Qinghe Zhang

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