Determination of sub-nanogram per gram quantities of light hydrocarbons (C2-C9) in rock samples by hydrogen stripping in the flow system of a capillary gas chromatograph

1978 ◽  
Vol 50 (13) ◽  
pp. 1848-1854 ◽  
Author(s):  
Rainer G. Schaefer ◽  
Bernd. Weiner ◽  
Detlev. Leythaeuser
1983 ◽  
Vol 66 (6) ◽  
pp. 1528-1531 ◽  
Author(s):  
Hiroshi Nakanishi

Abstract A gas chromatographic procedure is described for determining monosodium glutamate (MSG) in several types of food. A sample is extracted with acetone- water (1 + 1). Acetone is evaporated and an aliquot of the extract is buffered with 1M NH4OH-1M NH4CI pH 9 solution, and chromatographed directly on a column of QAE Sephadex A-25 that has been pretreated with the same buffer. MSG is eluted with 0.1N HC1, and a portion of the eluate is evaporated to dryness and reacted with dimethylformamide( DMF)-dimethylacetal to form the glutamic acid derivative, which is injected into a gas chromatograph and measured by flame ionization detection. Recoveries of MSG from sample fortified at 5-500 mg ranged from 92.8 to 100%.


2010 ◽  
Vol 178 (1-3) ◽  
pp. 57-65 ◽  
Author(s):  
Arlindo C. Gomes ◽  
José C. Nunes ◽  
Rogério M.S. Simões

2006 ◽  
Vol 572 (1) ◽  
pp. 148-154 ◽  
Author(s):  
Carmen Pons ◽  
Ildikó V. Tóth ◽  
António O.S.S. Rangel ◽  
Rafael Forteza ◽  
Víctor Cerdà

1998 ◽  
Vol 360 (1) ◽  
pp. 130-132 ◽  
Author(s):  
W. Qin ◽  
Z. J. Zhang ◽  
F. C. Wang
Keyword(s):  

1975 ◽  
Vol 63 (1) ◽  
pp. 69-77 ◽  
Author(s):  
G. L. Corte ◽  
L. Dubois
Keyword(s):  

2016 ◽  
Vol 911 ◽  
pp. 82-91 ◽  
Author(s):  
Edyta Nalewajko-Sieliwoniuk ◽  
Magdalena Iwanowicz ◽  
Sławomir Kalinowski ◽  
Anatol Kojło

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