Comprehensive Solid-Phase Extraction Method for Persistent Organic Pollutants. Validation and Application to the Analysis of Persistent Chlorinated Pesticides

2003 ◽  
Vol 75 (1) ◽  
pp. 71-77 ◽  
Author(s):  
Courtney D. Sandau ◽  
Andreas Sjödin ◽  
Mark D. Davis ◽  
John R. Barr ◽  
Vincent L. Maggio ◽  
...  
Keyword(s):  
Solid Phase Extraction ◽  
Organic Pollutants ◽  
Persistent Organic Pollutants ◽  
Extraction Method ◽  
Solid Phase ◽  
Phase Extraction ◽  
Chlorinated Pesticides

scholarly journals In Situ Miniaturised Solid Phase Extraction (m-SPE) for Organic Pollutants in Seawater Samples

2018 ◽  
Vol 2018 ◽  
pp. 1-6 ◽  
Author(s):  
B. Abaroa-Pérez ◽  
G. Sánchez-Almeida ◽  
J. J. Hernández-Brito ◽  
D. Vega-Moreno
Keyword(s):  
Solid Phase Extraction ◽  
Organic Pollutants ◽  
Marine Environment ◽  
Persistent Organic Pollutants ◽  
Solid Phase ◽  
In Situ Monitoring ◽  
Phase Extraction ◽  
Polycyclic Aromatic ◽  
Seawater Samples

Solid phase extraction (SPE) is a consolidated technique for determining pollutants in seawater samples. The current tendency is to miniaturise systems that extract and determine pollutants in the environment, reducing the use of organic solvents, while maintaining the quality in the extraction and preconcentration. On the other hand, there is a need to develop new extraction systems that can be fitted to in situ continual monitoring buoys, especially for the marine environment. This work has developed a first model of a low-pressure micro-SPE (m-SPE) for persistent organic pollutants (POPs) that can be simply applied to in situ monitoring in the marine environment. This system reduces the volumes of sample and solvents required in the laboratory in comparison with conventional SPE. In the future, it could be used in automated or robotic systems in marine technologies such as marine gliders and oceanographic buoys. This system has been optimised and validated to determine polycyclic aromatic hydrocarbons (PAH) in seawater samples, but it could also be applied to other kinds of persistent organic pollutants (POPs) and emerging pollutants.

Application of micro-solid-phase extraction for the determination of persistent organic pollutants in tissue samples

2008 ◽  
Vol 1186 (1-2) ◽  
pp. 358-364 ◽  
Author(s):  
Chanbasha Basheer ◽  
Kothandaraman Narasimhan ◽  
Meihui Yin ◽  
Changqing Zhao ◽  
Mahesh Choolani ◽  
...  
Keyword(s):  
Solid Phase Extraction ◽  
Organic Pollutants ◽  
Persistent Organic Pollutants ◽  
Solid Phase ◽  
Phase Extraction ◽  
Tissue Samples
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