Synthesis of oleic acid-capped CuInS2 nanocrystals from bimetallic hydroxide precursor

2016 ◽  
Vol 603 ◽  
pp. 243-248 ◽  
Author(s):  
Seonho Jung ◽  
Ji-Hyun Cha ◽  
Duk-Young Jung
Keyword(s):  
Oleic Acid ◽  
Cuins2 Nanocrystals

Oleic acid assisted formation mechanism of CuInS2 nanocrystals with tunable structures

RSC Advances ◽  
2014 ◽  
Vol 4 (69) ◽  
pp. 36875-36881 ◽  
Author(s):  
Fengcong Gong ◽  
Shouqin Tian ◽  
Baoshun Liu ◽  
Dehua Xiong ◽  
Xiujian Zhao
Keyword(s):  
Oleic Acid ◽  
Formation Mechanism ◽  
Zinc Blende ◽  
Phase Structures ◽  
Cuins2 Nanocrystals ◽  
Low Crystallinity

CuInS2 nanocrystals with different phase structures were synthesized by a facile heat-up method through simply adjusting the OA dosage. This is because a high OA dosage could facilitate the formation and crystallization of the CuIn(SR)x intermediate, giving a metastable wurtzite CuInS2 structure, while low OA dosage would lead to low crystallinity of the intermediate, producing a stable zinc-blende phase.

A magnetic super lattice

1987 ◽  
Vol 45 ◽  
pp. 360-361 ◽  
Author(s):  
M.D. Bentzon ◽  
J. v. Wonterghem ◽  
A. Thölén
Keyword(s):  
Thermal Decomposition ◽  
Oleic Acid ◽  
Magnetic Fluid ◽  
Magnetic Particles ◽  
Carbon Film ◽  
Thick Layer ◽  
Amorphous Iron ◽  
Super Lattice ◽  
Carrier Liquid ◽  
Median Diameter

We report on the oxidation of a magnetic fluid. The oxidation results in magnetic super lattice crystals. The “atoms” are hematite (α-Fe2O3) particles with a diameter ø = 6.9 nm and they are covered with a 1-2 nm thick layer of surfactant molecules.Magnetic fluids are homogeneous suspensions of small magnetic particles in a carrier liquid. To prevent agglomeration, the particles are coated with surfactant molecules. The magnetic fluid studied in this work was produced by thermal decomposition of Fe(CO)5 in Declin (carrier liquid) in the presence of oleic acid (surfactant). The magnetic particles consist of an amorphous iron-carbon alloy. For TEM investigation a droplet of the fluid was added to benzine and a carbon film on a copper net was immersed. When exposed to air the sample starts burning. The oxidation and electron irradiation transform the magnetic particles into hematite (α-Fe2O3) particles with a median diameter ø = 6.9 nm.

Intestinal Absorption of Iodine131-Labeled Triolein and Oleic Acid in Normal Subjects and in Steatorrhea

1958 ◽  
Vol 34 (5) ◽  
pp. 901-909 ◽  
Author(s):  
Ervin Kaplan ◽  
Bernard D. Edidin ◽  
Robert C. Fruin ◽  
Lyle A. Baker
Keyword(s):  
Oleic Acid ◽  
Intestinal Absorption ◽  
Normal Subjects

Oleic acid

2015 ◽  
Author(s):  
LB Becnel ◽  
YF Darlington ◽  
S Orechsner ◽  
J Easton-Marks ◽  
CA Watkins ◽  
...  
Keyword(s):  
Oleic Acid

Reusability Study of Sulfated Zirconia Functionalized SBA-15 Catalyst for Biolubricant Oil Production from Oleic Acid

2019 ◽  
Vol 1 (1) ◽  
pp. 46
Author(s):  
F R Rangganita ◽  
L Hermida ◽  
A Angraeni ◽  
D Khoirunnisa
Keyword(s):  
Oleic Acid ◽  
Sulfated Zirconia ◽  
Room Temperature ◽  
Oil Production ◽  
Catalyst Reusability

Sulfated zirconia functionalized SBA-15 catalsyt (SZr-SBA-15) was prepared byreacting SBA-15 with Zirkoniumoxychloride and urea at 90oC to form ZrO2-SBA-15. Then, ZrO2-SBA-15 was reacted with H2SO4 at room temperature to produceSZr-SBA-15 catalsyt.. The catalyst was characterized in terms of adsorptiondesorption nitrogen analysis, SEM-EDX and FTIR. Based on SEM-EDX andadsorption-desorption nitrogen analysis results, it was found that Zr had beenincorporated in SBA-15. By using the SZr-SBA-15 catalyst, esterification reactionof oleic acid with TMP to produce biolubricant oil of Trimethylolpropanetrioleatachieved 85% oleic acid conversion and selectivity of 63,7%. Reusability study ofSZr-SBA-15 catalyst was carried out for 3 rounds of reaction. It was found that thecatalyst could be used up to 3 rounds without significant decrease in activityKeywords: biolubricant oil, catalyst reusability, sba-15, sulfated zirconia.

PEMBUATAN SURFAKTAN DARI ASAM OLEAT

2019 ◽  
Vol 1 (3) ◽  
pp. 68
Author(s):  
Puguh Setyopratomo ◽  
Edy Purwanto ◽  
H. Yefrico ◽  
H. Yefrico
Keyword(s):  
Oleic Acid ◽  
Optimum Condition ◽  
Reaction Temperature ◽  
Catalyst Concentration ◽  
Acid Number ◽  
Esterification Reaction ◽  
Number Density ◽  
Sample Analysis ◽  
Reaction Conversion ◽  
Glycerol Mono

The synthesis of glycerol mono oleic from oleic acid and glycerol is classified as an esterification reaction. This research is aimed to study the influent of reaction temperature and catalyst concentration on reaction conversion. During the experiment the temperature of reaction mixture was varied as 110 oC, 130 oC, and 150 oC, while the catalyst concentration of 1%, 3 %, and 5% was used. The batch experiment was conducted in a glass reactor equipped with termometer, agitator, and reflux condensor. The oleic acid – glycerol mol ratio of 1 : 2 was used as a mixture feed. To maintain the reaction temperature at certain level, the oil bath was used. After the temperature of reaction mixture was reached the expected value, then H2SO4 catalyst was added to the reactor.  To measure the extent of the reaction, every 30 minutes the sample was drawn out from the reactor vessel. The sample analysis include acid number, density, and viscosity measurement. From this research the optimum condition which is the temperature of reaction of 150 oC and 1% catalyst concentration was obtained. At this optimum condition the convertion reach 86% and the analysis of other physical properties of the product show the acid number of 24.12, the density of 0.922 g/cc, and the viscosity of 118.4 cp.

Preparation and Surface Activities of Novel Sodium Sulfated Aryl Oleic Acid Alkanolamides

2005 ◽  
Vol 42 (4) ◽  
pp. 245-247 ◽  
Author(s):  
Xu Zhigang ◽  
Yuan Bing ◽  
Yan Jie ◽  
Li Zongshi ◽  
Qiao Weihong ◽  
...  
Keyword(s):  
Oleic Acid ◽  
Surface Activities
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