In-situ Fourier transform infrared spectroscopy gas phase studies of vanadium (IV) oxide coating by atmospheric pressure chemical vapour deposition using vanadyl (IV) acetylacetonate

2008 ◽  
Vol 516 (14) ◽  
pp. 4502-4507 ◽  
Author(s):  
D. Vernardou ◽  
M.E. Pemble ◽  
D.W. Sheel
2020 ◽  
Vol 22 (6) ◽  
pp. 3481-3489 ◽  
Author(s):  
Fatin Bazilah Fauzi ◽  
Edhuan Ismail ◽  
Syed Noh Syed Abu Bakar ◽  
Ahmad Faris Ismail ◽  
Mohd Ambri Mohamed ◽  
...  

An in-depth systematic study on the importance of fluid dynamics at the gas–solid interface to graphene growth in APCVD.


2020 ◽  
Vol 10 (1) ◽  
Author(s):  
Alexander Jones ◽  
Kissan Mistry ◽  
Manfred Kao ◽  
Ahmed Shahin ◽  
Mustafa Yavuz ◽  
...  

AbstractA technique is presented for collecting data on both the spatial and temporal variations in the electrical properties of a film as it is deposited on a flexible substrate. A flexible printed circuit board substrate with parallel electrodes distributed across its surface was designed. Zinc oxide films were then deposited on the flexible substrate at different temperatures via atmospheric pressure chemical vapour deposition (AP-CVD) using a spatial atomic layer deposition system. AP-CVD is a promising high-throughput thin film deposition technique with applications in flexible electronics. Collecting data on the film properties in-situ allows us to directly observe how deposition conditions affect the evolution of those properties in real-time. The spatial uniformity of the growing film was monitored, and the various stages of film nucleation and growth on the polymer substrate were observed. The measured resistance of the films was observed to be very high until a critical amount of material has been deposited, consistent with Volmer–Weber growth. Furthermore, monitoring the film resistance during post-deposition cooling enabled immediate identification of metallic or semiconducting behaviour within the conductive ZnO films. This technique allows for a more complete understanding of metal chalcogen film growth and properties, and the high volume of data generated will be useful for future implementations of machine-learning directed materials science.


2021 ◽  
Vol 11 (6) ◽  
pp. 2021-2025
Author(s):  
Liujin Wei ◽  
Guan Huang ◽  
Yajun Zhang

The combination of time-resolved transient photoluminescence with in-situ Fourier transform infrared spectroscopy has been conducted to investigate the intrinsic phase structure-dependent activity of Bi2O3 catalyst for CO2 reduction.


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