Microwave assisted synthesis of 3-benzazepin-2-ones as building blocks for 2,3-disubstituted tetrahydro-3-benzazepines

Tetrahedron ◽  
2012 ◽  
Vol 68 (12) ◽  
pp. 2687-2695 ◽  
Author(s):  
Soumya Sarkar ◽  
Syed Masood Husain ◽  
Dirk Schepmann ◽  
Roland Fröhlich ◽  
Bernhard Wünsch
ChemInform ◽  
2009 ◽  
Vol 40 (13) ◽  
Author(s):  
Nikita V. Tolstoluzhsky ◽  
Nikolay Yu. Gorobets ◽  
Nadezhda N. Kolos ◽  
Sergey M. Desenko

2005 ◽  
Vol 2005 (3) ◽  
pp. 167-168 ◽  
Author(s):  
Gui-Rong Qu ◽  
Yong Li ◽  
Su-Hui Han

The synthesis of N1/N9- (Ethoxycarbonylmethyl)pyrimidine/purine using as synthons for peptide nucleic acids has been described. Microwave irradiation provided the desired products by alkylation of the appropriately protected natural and substituted nucleobases with ethyl bromoacetate within 4–7 min in 48–85% yields.


Tetrahedron ◽  
2016 ◽  
Vol 72 (22) ◽  
pp. 2955-2963 ◽  
Author(s):  
Živilė Žukauskaitė ◽  
Vida Buinauskaitė ◽  
Joana Solovjova ◽  
Lina Malinauskaitė ◽  
Aistė Kveselytė ◽  
...  

ChemInform ◽  
2012 ◽  
Vol 43 (31) ◽  
pp. no-no
Author(s):  
Soumya Sarkar ◽  
Syed Masood Husain ◽  
Dirk Schepmann ◽  
Roland Froehlich ◽  
Bernhard Wuensch

2008 ◽  
Vol 10 (6) ◽  
pp. 893-896 ◽  
Author(s):  
Nikita V. Tolstoluzhsky ◽  
Nikolay Yu. Gorobets ◽  
Nadezhda N. Kolos ◽  
Sergey M. Desenko

Author(s):  
Ilaria Paolini ◽  
Francesca Nuti ◽  
Giuseppina Sabatino ◽  
Mario Chelli ◽  
Anna M. Papini

2011 ◽  
Vol 89 (10) ◽  
pp. 1236-1244 ◽  
Author(s):  
Kancherla Rajesh ◽  
Bandapalli Palakshi Reddy ◽  
Vijayaparthasarathi Vijayakumar

The one pot, three component reaction of p-hydroxy benzaldehyde, β-ketoester, and ammonium acetate afforded the corresponding monopodal 1,4-dihydropyridines as building blocks, which in turn converted into diversified novel bipodal, tripodal, and tetrapodal 1,4-dihydropyridines with different alkylating agents through conventional as well as microwave assisted reactions. The unambiguous structural confinements of the all the synthesized compounds were drawn out with the help of 2D NMR (H-H COSY and C-H COSY).


2018 ◽  
Vol 6 (14) ◽  
pp. 3743-3756 ◽  
Author(s):  
Michal P. Krompiec ◽  
Sean N. Baxter ◽  
Elena L. Klimareva ◽  
Dmitry S. Yufit ◽  
Daniel G. Congrave ◽  
...  

A facile one-pot, microwave-assisted synthesis of novel functionalized arylenedioxythiophenes as promising building blocks for conjugated polymers with tuneable electronic properties is presented.


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