Electromigration effect upon single- and two-phase Ag-Cu alloy strips: An in situ study

2019 ◽  
Vol 173 ◽  
pp. 134-138
Author(s):  
Yu-chen Liu ◽  
Yung-si Yu ◽  
Shih-kang Lin ◽  
Shang-Jui Chiu
2020 ◽  
Vol 829 ◽  
pp. 154612
Author(s):  
Ya Li ◽  
Yunlai Deng ◽  
Shitong Fan ◽  
Xiaobin Guo ◽  
Keda Jiang ◽  
...  

2014 ◽  
Vol 790-791 ◽  
pp. 349-354 ◽  
Author(s):  
Andrew M. Mullis ◽  
Caroline R. Clopet ◽  
Robert F. Cochrane

A melt encasement (fluxing) method has been used to undercool Ag-Cu alloy at its eutectic composition. The recalescence of the undercooled alloy has been filmed at high frame rate. At low undercooling lamellar eutectic is observed to grow, giving way to a mixed anomalous-lamellar structure at higher undercooling. In situ observation of the spot brightness reveals, as expected, that the lamellar eutectic grows via a planar front mechanism, while the anomalous eutectic grows via a more complex process characterised by a double recalescence. The first recalescence is non-space-filling (dendritic) in character and is followed shortly afterwards by a second recalescence which appears to be of the planar front type. Moreover, the first recalescence event appears to be to a temperature in excess of the equilibrium eutectic temperature. This is strongly suggestive that the anomalous eutectic morphology arises due to the growth and subsequent partial remelting of a dendritic morphology, probably a two-phase (eutectic) dendrite, followed by planar front growth of a lamellar eutectic into the residual liquid.


Author(s):  
J. R. Reed ◽  
D. J. Michel ◽  
P. R. Howell

The Al6Li3Cu (T2) phase, which exhibits five-fold or icosahedral symmetry, forms through solid state precipitation in dilute Al-Li-Cu alloys. Recent studies have reported that the T2 phase transforms either during TEM examination of thin foils or following ion-milling of thin foil specimens. Related studies have shown that T2 phase transforms to a microcrystalline array of the TB phase and a dilute aluminum solid solution during in-situ heating in the TEM. The purpose of this paper is to report results from an investigation of the influence of ion-milling on the stability of the T2 phase in dilute Al-Li-Cu alloy.The 3-mm diameter TEM disc specimens were prepared from a specially melted Al-2.5%Li-2.5%Cu alloy produced by conventional procedures. The TEM specimens were solution heat treated 1 h at 550°C and aged 1000 h at 190°C in air to develop the microstructure. The disc specimens were electropolished to achieve electron transparency using a 20:80 (vol. percent) nitric acid: methanol solution at -60°C.


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