Effect of annealing on the microstructure and magnetic properties of soft magnetic Fe-Si produced via laser additive manufacturing

2018 ◽  
Vol 142 ◽  
pp. 121-125 ◽  
Author(s):  
M. Garibaldi ◽  
I. Ashcroft ◽  
J.N. Lemke ◽  
M. Simonelli ◽  
R. Hague
Author(s):  
Yingtao Zhang ◽  
Gang Wang ◽  
Zhenguo Nie ◽  
Wankai Shi ◽  
Yiming Rong

The good DC magnetic properties can be achieved for 1J50 soft magnetic alloy by applying high temperature hydrogen annealing. Annealing process parameters, e.g., atmosphere, soaking temperature, and time, are critical to soft magnetic properties. Qualitative results had been done for years. However a quantitative research among process parameters, microstructure, and magnetic properties can be more comprehensive and specific. In this study, a serial of experiments for 1J50 samples under the Chinese national standards. The influence of annealing temperature and socking time on DC magnetic properties and microstructure of the samples has been investigated on DC magnetic properties and microstructure of samples. The result shows that annealing process parameters have a nonlinear effect on the development of material microstructure and magnetic properties. Furthermore, the models among magnetic property, grain size, and process parameters have been built to quantitatively describe the interrelationship in between.


2017 ◽  
Vol 31 (16-19) ◽  
pp. 1744013 ◽  
Author(s):  
Liang Yan ◽  
Biao Yan

Fe–6.5 wt.% Si powder coated with 10 wt.% MnZn(Fe2O4)2 (MnZn ferrite) was successfully prepared by using dry-type stirring ball milling. The Fe–6.5 wt.% Si/MnZn(Fe2O4)2 soft magnetic composites were prepared by subsequent spark plasma sintering. This paper aims at analyzing the microstructure and magnetic properties of Fe–6.5 wt.% Si/MnZn(Fe2O4)2 soft magnetic composites (sintering temperature: 750[Formula: see text]C, sintering pressure: 50 MPa, holding time: 8 min, heating rate: 60 K/min). Based on X-ray diffraction and scanning electron microscopy, microstructure and powder morphology were examined and magnetic measurements on bulk samples were conducted by vibrating sample magnetometer and impedance analyzer. According to the experiments results, Fe–6.5 wt.% Si/MnZn(Fe2O4)2 composites displayed a core-shell structure, and ceramic phase was observed after sintering. The Fe–6.5 wt.% Si/MnZn(Fe2O4)2 composites achieved high resistivity ([Formula: see text] m[Formula: see text]/cm) while maintaining excellent magnetic properties ([Formula: see text] emu/g). Core losses especially at medium and high frequencies were significantly reduced.


2018 ◽  
Vol 466 ◽  
pp. 75-80 ◽  
Author(s):  
Xiaoshan Yang ◽  
Xiufang Cui ◽  
Guo Jin ◽  
Jinna Liu ◽  
Yanbo Chen ◽  
...  

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