scholarly journals Crystallographic texture control of beta-type Ti–15Mo–5Zr–3Al alloy by selective laser melting for the development of novel implants with a biocompatible low Young's modulus

2017 ◽  
Vol 132 ◽  
pp. 34-38 ◽  
Author(s):  
Takuya Ishimoto ◽  
Koji Hagihara ◽  
Kenta Hisamoto ◽  
Shi-Hai Sun ◽  
Takayoshi Nakano
2021 ◽  
Vol 1016 ◽  
pp. 1797-1801
Author(s):  
Mitsuharu Todai ◽  
Takeshi Nagase ◽  
Takayoshi Nakano

In this study, we sucsess the fabrication of dense compornent of Ti-20at.%X (X = Cr and Nb) alloys by Selected laser melting (SLM) pwocess, from a mixture of poweder element powders. The volume rasio of pore and non-molten particles is dependent of the enegy density. The difficulty of fabrication of Ti-X alloy comporment is dependent of melting temperature of X element. Thus, Ti-20at.%Cr alloys, which has the lowest melting temperature of X is easier to monufacture of dense comporment. The Ti-20at.%Cr alloys and Ti-20at.%Nb comprise β-Ti single-phase components without any non-molten particles and macroscopic defects. In addtion, the {001}〈100〉 crystallographic texture of these Ti-Cr and Ti-Nb alloys can be controlled effectively by optimizing the SLM parameters. This means that the SLM is key techmelogy of controlling of Young’s modulus and shape at the same time because Young's modulus of be-ta phase in Ti alloys is strongly related to the crystal orientation.


Author(s):  
Jie Niu ◽  
Hui Leng Choo ◽  
Wei Sun ◽  
Sui Him Mok

Research on materials, design, processing, and manufacturability of parts produced by additive manufacturing (AM) has been investigated significantly in the past. However, limited research on tensile behavior of cellular lattice structures by AM was carried out. In this paper, effective tensile Young's modulus, E*, of triangular lattice structures was determined. Firstly, analytical solution was derived based on Euler–Bernoulli beam theory. Then, numerical results of E* were obtained by finite element analysis (FEA) for triangular lattice structures classified by three shape parameters. The effects of side length, L, beam thickness, t, and height, h, on E* were investigated individually. FEA results revealed that there is a relationship between E* and the relative density and shape parameters. Among them, t has the most significant effect on E*. Numerical results were also compared with the results from modified general function for cellular structures and modified formula for triangular honeycomb. The E* predicted by the proposed analytical solution shows the best agreement with the numerical results. Finally, tensile tests were carried out using AlSi10 Mg triangular lattice structures manufactured by selective laser melting (SLM) process. The experimental results show that both analytical and numerical solutions are able to predict E* with good accuracy. In the future, the proposed solution can be used to design lightweight structures with triangular unit cells.


2017 ◽  
Vol 743 ◽  
pp. 9-12
Author(s):  
Zhanna G. Kovalevskaya ◽  
Margarita A. Khimich ◽  
Andrey V. Belyakov

Porosity, values of nanohardness and Young’s modulus of the specimens obtained with the method of selective laser melting were measured with optical methods, scanning electron microscopy and Nano Hardness Tester NHT-S-AX-000X device for measuring physicomechanical properties. Ti-45wt%Nb powder obtained with mechanical alloying was used for selective laser melting. The results have shown that increased heat input due to the laser power growth up to 80 W and scanning speed decrease down to 40 mm/s decreases the porosity of the specimen. The nanohardness average value is not sensitive to the changes of scanning modes in the investigated range. The Young’s modulus decreases with energy input increase.


2012 ◽  
Vol 535-537 ◽  
pp. 1222-1229 ◽  
Author(s):  
Francesco Cardaropoli ◽  
Vittorio Alfieri ◽  
Fabrizia Caiazzo ◽  
Vincenzo Sergi

The paper discusses the possibility of manufacturing dental implants through Selective Laser Melting (SLM) of a Ti-6Al-4V alloy powder. Among all possible biomaterials, this alloy is widely used in biomedical applications due to high biocompatibility. Selective Laser Melting allows to obtain biomaterials with peculiar characteristics in terms of porosity gradient, roughness, customized geometry, and mechanical properties. Influence of input process parameters on porosity and analysis of Selective Laser Melting capabilities in implant dentistry have been focused. Porosity is a key parameter in dental implants as it affects stiffness, which is related to Young’s modulus. Ti-6Al-4V bulk material presents a Young’s modulus of 110 GPa, whereas the bone one ranges from 10 to 26 GPa. The relative difference of mechanical properties causes the phenomenon of stress shielding, which has a detrimental effect on the longevity of dental implants. Total porosity is important in reducing the effective modulus of porous metals. Biomaterials specimens obtained during experimental phase have been examined in terms of porosity (in inverse ratio to relative density), microstructure, microhardness and roughness. According to test results discussed in this paper, Selective Laser Melting is proved to be an efficient technology for the construction of Ti-6Al-4V dental implants, because biomaterials with adequate properties can be obtained changing processing parameters. Other fabrication techniques fail to produce biomaterials for dental implants with the desired features.


Metals ◽  
2019 ◽  
Vol 9 (12) ◽  
pp. 1252 ◽  
Author(s):  
Martin Diehl ◽  
Jörn Niehuesbernd ◽  
Enrico Bruder

The influence of grain shape and crystallographic orientation on the global and local elastic and plastic behaviour of strongly textured materials is investigated with the help of full-field simulations based on texture data from electron backscatter diffraction (EBSD) measurements. To this end, eight different microstructures are generated from experimental data of a high-strength low-alloy (HSLA) steel processed by linear flow splitting. It is shown that the most significant factor on the global elastic stress–strain response (i.e., Young’s modulus) is the crystallographic texture. Therefore, simple texture-based models and an analytic expression based on the geometric mean to determine the orientation dependent Young’s modulus are able to give accurate predictions. In contrast, with regards to the plastic anisotropy (i.e., yield stress), simple analytic approaches based on the calculation of the Taylor factor, yield different results than full-field microstructure simulations. Moreover, in the case of full-field models, the selected microstructure representation influences the outcome of the simulations. In addition, the full-field simulations, allow to investigate the micro-mechanical fields, which are not readily available from the analytic expressions. As the stress–strain partitioning visible from these fields is the underlying reason for the observed macroscopic behaviour, studying them makes it possible to evaluate the microstructure representations with respect to their capabilities of reproducing experimental results.


Materials ◽  
2019 ◽  
Vol 12 (8) ◽  
pp. 1293 ◽  
Author(s):  
Michele Calandri ◽  
Shuo Yin ◽  
Barry Aldwell ◽  
Flaviana Calignano ◽  
Rocco Lupoi ◽  
...  

Nickel-based Inconel 718 is a very good candidate for selective laser melting (SLM). During the SLM process, Inconel 718 develops a complex and heterogeneous microstructure. A deep understanding of the microstructural features of the as-built SLM material is essential for the design of a proper post-process heat treatment. In this study, the microstructure of as-built SLM Inconel 718 was investigated at different length scales using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Electron backscatter diffraction (EBSD) was also used to analyze the grain morphology and crystallographic texture. Grains elongated in the build direction and crossing several deposited layers were observed. The grains are not constrained by the laser tracks or by the melt pools, which indicates epitaxial growth controls the solidification. Each grain is composed of fine columnar dendrites that develop along one of their <100> axes oriented in the direction of the local thermal gradient. Consequently, prominent <100> crystallographic texture was observed and the dendrites tend to grow to the build direction or with occasional change of 90° at the edge of the melt pools. At the dendrite length scale, the microsegregation of the alloying elements, interdendritic precipitates, and dislocations was also detected.


Materials ◽  
2018 ◽  
Vol 11 (8) ◽  
pp. 1337 ◽  
Author(s):  
Paul Lohmuller ◽  
Laurent Peltier ◽  
Alain Hazotte ◽  
Julien Zollinger ◽  
Pascal Laheurte ◽  
...  

The variations of the mechanical properties of the CoCrFeMnNi high entropy alloy (HEA) during groove cold rolling process were investigated with the aim of understanding their correlation relationships with the crystallographic texture. Our study revealed divergences in the variations of the microhardness and yield strength measured from samples deformed by groove cold rolling and conventional cold rolling processes. The crystallographic texture analyzed by electron back scattered diffraction (EBSD) revealed a hybrid texture between those obtained by conventional rolling and drawing processes. Though the groove cold rolling process induced a marked strengthening effect in the CoCrFeMnNi HEA, the mechanical properties were also characterized by an unusual decrease of the Young’s modulus as the applied groove cold rolled deformation increased up to about 0.5 before reaching a stabilized value. This decrease of the Young’s modulus was attributed to the increased density of mobile dislocations induced by work hardening during groove cold rolling processing.


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