Confirmation of the ω-phase in electron beam welded Ti–5Al–5V–5Mo–3Cr by high-resolution scanning transmission electron microscopy: An initial investigation into its effects on embrittlement

2014 ◽  
Vol 92 ◽  
pp. 15-18 ◽  
Author(s):  
J.C. Sabol ◽  
C.J. Marvel ◽  
M. Watanabe ◽  
T. Pasang ◽  
W.Z. Misiolek
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Electron Beam ◽  
High Resolution ◽  
Scanning Transmission Electron Microscopy ◽  
Initial Investigation ◽  
Scanning Transmission Electron ◽  
Ω Phase ◽  
Transmission Electron ◽  
Scanning Transmission

scholarly journals Identification of interstratified mica and pyrophyllite monolayers within chlorite using advanced scanning/transmission electron microscopy

2019 ◽  
Vol 104 (10) ◽  
pp. 1436-1443
Author(s):  
Guanyu Wang ◽  
Hejing Wang ◽  
Jianguo Wen
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Electron Beam ◽  
Clay Minerals ◽  
Scanning Transmission Electron Microscopy ◽  
Dark Field ◽  
Chemical Compositions ◽  
Scanning Transmission Electron ◽  
Transmission Electron ◽  
Scanning Transmission

Abstract Interstratified clay minerals reflect the weathering degree and record climatic conditions and the pedogenic processes in the soil. It is hard to distinguish a few layers of interstratified clay minerals from the chlorite matrix, due to their similar two-dimensional tetrahedral-octahedral-tetrahedral (TOT) structure and electron-beam sensitive nature during transmission electron microscopy (TEM) imaging. Here, we used multiple advanced TEM techniques including low-dose high-resolution TEM (HRTEM), high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM) imaging combined with energy-dispersive spectroscopic (EDS) mapping to study interstratified layers in a chlo-rite sample from Changping, Beijing, China. We demonstrated an interstratified mica or pyrophyllite monolayer could be well distinguished from the chlorite matrix by projected atomic structures, lattice spacings, and chemical compositions with advanced TEM techniques. Further investigation showed two different transformation mechanisms from mica or pyrophyllite to chlorite: either a 4 Å increase or decrease in the lattice spacing. This characterization approach can be extended to the studies of other electron-beam sensitive minerals.

scholarly journals The Importance of High-Resolution Scanning Transmission Electron Microscopy For Fine-Scale Dislocation Analysis

2010 ◽  
Vol 16 (S2) ◽  
pp. 1798-1799
Author(s):  
PJ Phillips ◽  
L Kovarik ◽  
RR Unocic ◽  
D Wei ◽  
D Mourer ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
High Resolution ◽  
Scanning Transmission Electron Microscopy ◽  
Fine Scale ◽  
Scanning Transmission Electron ◽  
Transmission Electron ◽  
Scanning Transmission

Extended abstract of a paper presented at Microscopy and Microanalysis 2010 in Portland, Oregon, USA, August 1 – August 5, 2010.

Arrangements of Fe-Centered Zn12 Icosahedra in Fe-Zn Intermetallic Compounds Determined by Ultra-High Resolution Scanning Transmission Electron Microscopy

2015 ◽  
Vol 1760 ◽  
Author(s):  
Norihiko L. Okamoto ◽  
Akira Yasuhara ◽  
Katsushi Tanaka ◽  
Haruyuki Inui
Keyword(s):  
Crystal Structure ◽  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
High Resolution ◽  
Single Crystal ◽  
Scanning Transmission Electron Microscopy ◽  
Scanning Transmission Electron ◽  
Transmission Electron ◽  
Deformation Properties ◽  
Scanning Transmission

ABSTRACTThe crystal structure of the δ1p phase in the Fe-Zn system has been refined by single-crystal synchrotron X-ray diffraction combined with ultra-high resolution scanning transmission electron microscopy. The crystal structure can be described to build up with Fe-centered Zn12 icosahedra. The deformation properties obtained by single-crystal micropillar compression tests of the δ1p phase is discussed in terms of the arrangement of the Fe-centered Zn12 icosahedra in contrast with the ζ phase in the Fe-Zn system.

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