Fracture toughness of a hot-extruded multiphase Nb–10Si–2Fe in situ composite

2009 ◽  
Vol 61 (6) ◽  
pp. 620-623 ◽  
Author(s):  
J.L. Yu ◽  
K.F. Zhang ◽  
Z.K. Li ◽  
X. Zheng ◽  
G.F. Wang ◽  
...  
1993 ◽  
Vol 322 ◽  
Author(s):  
I. Weiss ◽  
M. Thirukkonda ◽  
R. Srinivasan

AbstractNb-10 a/o Si alloy is an in-situ composite. The microstructure of the cast alloy consists of pro-eutectic Nb dendrites distributed in a matrix of eutectic Nb3Si + Nb phases. The microstructure of the as-cast alloy was modified by multiple hot extrusions producing an oriented composite. Extensive grain size refinement occurred in both the Nb and Nb3Si phases. The ductile primary (pro-eutectic) Nb particles were aligned along the extrusion direction. Bend strength and fracture toughness measured by three point bend and four point bend tests, respectively, showed that both the yield strength and fracture toughness of the alloy increases considerably following this thermomechanical processing. These improvements have been attributed to the changes in size, morphology and spacing of the constituent phases and their microstructural refinement.


2012 ◽  
Vol 44 (1) ◽  
pp. 73-80 ◽  
Author(s):  
Kun Zhang ◽  
Wang Fen ◽  
Jianfeng Zhu ◽  
Huae Wu

Al2O3/TiAl in situ composites doped with Cr and V2O5 were successfully prepared from Ti, Al, TiO2, Cr and V2O5 by hot pressing. The effect of in situ formed Al2O3 content on the phase composition, microstructure and mechanical properties of Al2O3/TiAl composites were investigated. The results show that the as-synthesized composites mainly consisted of ?-TiAl/?2-Ti3Al matrix and dispersive Al2O3 reinforcing phases. The in situ formed fine Al2O3 ceramic particles mainly disperse on the grain boundaries of TiAl, resulting in refinement of TiAl matrix, which improves the mechanical properties of the Al2O3/TiAl in situ composite. The composite with 7.54 at.% Al2O3 possesses the maximum flexural strength and fracture toughness of 335.38 MPa and 5.39 MPa m1/2, respectively. The strengthening mechanism was also discussed in detail.


2007 ◽  
Vol 22 (2) ◽  
pp. 428-436 ◽  
Author(s):  
S. Jayalakshmi ◽  
J.P. Ahn ◽  
K.B. Kim ◽  
E. Fleury

We report the hydrogenation characteristics and mechanical properties of Ti50Zr25Cu25 in situ composite ribbons, composed of β-Ti crystalline phase dispersed in an amorphous matrix. Upon cathodic charging at room temperature, high hydrogen absorption up to ∼60 at.% (H/M = ∼1.2) is obtained. At such a high concentration, hydrogen-induced amorphization occurs. Mechanical tests conducted on the composite with varying hydrogen concentrations indicate that the Ti50Zr25Cu25 alloy is significantly resistant to hydrogen embrittlement when compared to conventional amorphous alloys. A possible mechanism that would contribute toward hydrogen-induced amorphization and hydrogen embrittlement is discussed.


2012 ◽  
Vol 581-582 ◽  
pp. 819-822 ◽  
Author(s):  
Bin Meng ◽  
Jin Hui Peng

The corundum-mullite was toughened by in-situ synthesized mullite whiskers and the process parameters influencing the fracture toughness of corundum-mullite, such as sintering temperature, addition amount of AlF3 and V2O5, were optimized by means of response surface method. Corundum-mullite with fracture toughness of 9.44 MPa.m-1/2 could be obtained under the optimized conditions, i.e. sintering temperature of 1400°C, 4.8 wt.% of AlF3 and 5.8 wt.% of V2O5. The results showed that it was feasible to prepare corundum-mullite toughened by in-situ synthesized mullite whiskers by the optimized parameters. In addition, an accurate model based on response surface method was proposed to predict the experimental results.


1991 ◽  
Vol 25 (9) ◽  
pp. 2109-2114 ◽  
Author(s):  
B. Cockeram ◽  
H.A. Lipsitt ◽  
R. Srinivasan ◽  
I. Weiss

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