Identification of intermetallic precipitates formed during re-solidification of brazed aluminium alloys

2006 ◽  
Vol 55 (2) ◽  
pp. 191-194 ◽  
Author(s):  
M DEHMAS ◽  
R VALDES ◽  
M LAFONT ◽  
J LACAZE ◽  
B VIGUIER
Keyword(s):  
Aluminium Alloys ◽  
Intermetallic Precipitates

Microanalytical Identification of a New Zr-Nb-Fe Phase

1990 ◽  
Vol 48 (2) ◽  
pp. 132-133
Author(s):  
O.T. Woo ◽  
G.J.C. Carpenter
Keyword(s):  
Trace Elements ◽  
Cold Rolling ◽  
Proportionality Factor ◽  
Tube Material ◽  
X Ray ◽  
Metal Foils ◽  
Arc Melting ◽  
Intermetallic Particles ◽  
Intermetallic Precipitates ◽  
Cold Worked

To study the influence of trace elements on the corrosion and hydrogen ingress in Zr-2.5 Nb pressure tube material, buttons of this alloy containing up to 0.83 at% Fe were made by arc-melting. The buttons were then annealed at 973 K for three days, furnace cooled, followed by ≈80% cold-rolling. The microstructure of cold-worked Zr-2.5 at% Nb-0.83 at% Fe (Fig. 1) contained both β-Zr and intermetallic precipitates in the α-Zr grains. The particles were 0.1 to 0.7 μm in size, with shapes ranging from spherical to ellipsoidal and often contained faults. β-Zr appeared either roughly spherical or as irregular elongated patches, often extending to several micrometres.The composition of the intermetallic particles seen in Fig. 1 was determined using Van Cappellen’s extrapolation technique for energy dispersive X-ray analysis of thin metal foils. The method was employed to avoid corrections for absorption and fluorescence via the Cliff-Lorimer equation: CA/CB = kAB · IA/IB, where CA and CB are the concentrations by weight of the elements A and B, and IA and IB are the X-ray intensities; kAB is a proportionality factor.

“Cavity” formation in superplastically deformed aluminium alloys

1990 ◽  
Vol 48 (4) ◽  
pp. 958-959
Author(s):  
A. Cziráki ◽  
E. Ková-csetényi ◽  
T. Torma ◽  
T. Turmezey
Keyword(s):  
Grain Boundaries ◽  
Aluminium Alloys ◽  
Superplastic Deformation ◽  
Volume Fraction ◽  
Superplastic Forming ◽  
Polished Surface ◽  
Cavity Formation ◽  
Stress Concentrations ◽  
Electron Microscopic ◽  
Commercial Aluminium

It is known that the formation of cavities during superplastic deformation can be correlated with the development of stress concentrations at irregularities along grain boundaries such as particles, ledges and triple points. In commercial aluminium alloys Al-Fe-Si particles or other coarse constituents may play an important role in cavity formation.Cavity formation during superplastic deformation was studied by optical metallography and transmission scanning electron microscopic investigations on Al-Mg-Si and Al-Mg-Mn alloys. The structure of particles was characterized by selected area diffraction and X-ray micro analysis. The volume fraction of “voids” was determined on mechanically polished surface.It was found by electron microscopy that strongly deformed regions are formed during superplastic forming at grain boundaries and around coarse particles.According to electron diffraction measurements these areas consist of small micro crystallized regions. See Fig.l.Comparing the volume fraction and morphology of cavities found by optical microscopy a good correlation was established between that of micro crystalline regions.

PRECISION PRESSURE WELDING OF ALUMINIUM ALLOYS

2017 ◽  
pp. 67-76 ◽  
Author(s):  
Oleg Novomlynets ◽  
◽  
Serhii Oleksiienko ◽  
Svitlana Yushchenko ◽  
Evgen Polovetskiy ◽  
...  
Keyword(s):  
Aluminium Alloys ◽  
Pressure Welding
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