Transition from the hierarchical distribution to a homogeneous formation in injection molded isotactic polypropylene (iPP) with dynamic mold temperature control

2017 ◽  
Vol 60 ◽  
pp. 299-306 ◽  
Author(s):  
Haibin Zhao ◽  
Xue Liu ◽  
Yang Sui ◽  
Yanan Zhang ◽  
Guoqun Zhao
Keyword(s):  
Temperature Control ◽  
Isotactic Polypropylene ◽  
Mold Temperature ◽  
Injection Molded ◽  
Homogeneous Formation

scholarly journals The Friction of Structurally Modified Isotactic Polypropylene

Materials ◽  
2021 ◽  
Vol 14 (23) ◽  
pp. 7462
Author(s):  
Natalia Wierzbicka ◽  
Tomasz Sterzyński ◽  
Marek Nowicki
Keyword(s):  
Isotactic Polypropylene ◽  
Heterogeneous Nucleation ◽  
Total Content ◽  
Mold Temperature ◽  
Pimelic Acid ◽  
Reciprocating Motion ◽  
Shore Hardness ◽  
Β Phase ◽  
Forming Temperature ◽  
Injection Molded

The purpose of studies was to analyse an impact of heterogeneous nucleation of modified isotactic polypropylene (iPP) on its tribological properties. The iPP injection molded samples, produced by mold temperature of 20 and 70 °C, were modified with compositions of two nucleating agents (NA’s), DMDBS creating α-form and mixture of pimelic acid with calcium stearate (PACS) forming β–phase of iPP, with a total content 0.2 wt.% of NA’s. A polymorphic character of iPP, with both, monoclinic (α) and pseudo-hexagonal (β) crystalline structures, depending on the NA’s ratio, was verified. The morphology observation, DSC, hardness and tribological measurements as test in reciprocating motion with “pin on flat” method, were realized, followed by microscopic observation (confocal and SEM) of the friction patch track. It was found that Shore hardness rises along with DMBDS content, independent on mold temperature. The friction coefficient (COF) depends on NA’s content and forming temperature—for upper mold temperature (70 °C), its value is higher and more divergently related to NA’s composition, what is not the case by 20 °C mold temperature. The height of friction scratches and the width of patch tracks due to its plastic deformation, as detected by confocal microscopy, are related to heterogeneous nucleation modified structure of iPP.

scholarly journals The use of IR thermography to show the mold and part temperature evolution in injection molding

2016 ◽  
Vol 36 (1) ◽  
pp. 40-43 ◽  
Author(s):  
Karol Bula ◽  
Leszek Różański ◽  
Lidia Marciniak-Podsadna ◽  
Dawid Wróbel
Keyword(s):  
Injection Molding ◽  
Isotactic Polypropylene ◽  
Infrared Camera ◽  
Mold Temperature ◽  
Temperature Evolution ◽  
Injection Mold ◽  
Ir Thermography ◽  
Molded Parts ◽  
Injection Molded

Abstract This study concerns the application of infrared camera for injection molding analysis by measuring temperatures of both injection molded parts and injection mold cavities in a function of injection cycles. The mold with two cavities, differing in thickness (1 and 3 mm), and a cold direct runner was used. Isotactic polypropylene homopolymer was utilized to produce parts. Mold temperature was set at 22°C and controlled by a water chiller. Five measuring points were determined: SP1, SP2 (placed in the 3 mm cavity), SP3, SP4 (located in the 1 mm cavity) and SP5 around an injection molding gate. Our investigations showed that the highest temperature is localized around SP2 point and the lowest at SP4. Also, it was proved that even after 62 injection molding cycles, temperatures of cavities were not stable, revealing their further increase with each cycle.

scholarly journals Study on External Gas-Assisted Mold Temperature Control with the Assistance of a Flow Focusing Device in the Injection Molding Process

Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 965 ◽  
Author(s):  
Nguyen Truong Giang ◽  
Pham Son Minh ◽  
Tran Anh Son ◽  
Tran Minh The Uyen ◽  
Thanh-Hai Nguyen ◽  
...  
Keyword(s):  
Injection Molding ◽  
Temperature Control ◽  
Mold Temperature ◽  
Injection Molding Process ◽  
Melt Flow ◽  
Flow Focusing ◽  
Molding Process ◽  
Heating Efficiency ◽  
Flow Length ◽  
Insert Plate

In the injection molding field, the flow of plastic material is one of the most important issues, especially regarding the ability of melted plastic to fill the thin walls of products. To improve the melt flow length, a high mold temperature was applied with pre-heating of the cavity surface. In this paper, we present our research on the injection molding process with pre-heating by external gas-assisted mold temperature control. After this, we observed an improvement in the melt flow length into thin-walled products due to the high mold temperature during the filling step. In addition, to develop the heating efficiency, a flow focusing device (FFD) was applied and verified. The simulations and experiments were carried out within an air temperature of 400 °C and heating time of 20 s to investigate a flow focusing device to assist with external gas-assisted mold temperature control (Ex-GMTC), with the application of various FFD types for the temperature distribution of the insert plate. The heating process was applied for a simple insert model with dimensions of 50 mm × 50 mm × 2 mm, in order to verify the influence of the FFD geometry on the heating result. After that, Ex-GMTC with the assistance of FFD was carried out for a mold-reading process, and the FFD influence was estimated by the mold heating result and the improvement of the melt flow length using acrylonitrile butadiene styrene (ABS). The results show that the air sprue gap (h) significantly affects the temperature of the insert and an air sprue gap of 3 mm gives the best heating rate, with the highest temperature being 321.2 °C. Likewise, the actual results show that the height of the flow focusing device (V) also influences the temperature of the insert plate and that a 5 mm high FFD gives the best results with a maximum temperature of 332.3 °C. Moreover, the heating efficiency when using FFD is always higher than without FFD. After examining the effect of FFD, its application was considered, in order to improve the melt flow length in injection molding, which increased from 38.6 to 170 mm, while the balance of the melt filling was also clearly improved.

Multi-objective evolutionary design of mold temperature control using DACE for parameter optimization

2007 ◽  
Vol 25 (1-4) ◽  
pp. 661-667 ◽  
Author(s):  
Jörn Mehnen ◽  
Thomas Michelitsch ◽  
Christian Lasarczyk ◽  
Thomas Bartz-Beielstein
Keyword(s):  
Parameter Optimization ◽  
Temperature Control ◽  
Mold Temperature ◽  
Evolutionary Design ◽  
Multi Objective

Numerical simulation of mold-temperature-control solidification

2007 ◽  
Vol 17 (3) ◽  
pp. 443-448 ◽  
Author(s):  
Dong-dong YOU ◽  
Ming SHAO ◽  
Yuan-yuan LI ◽  
Zhao-yao ZHOU
Keyword(s):  
Numerical Simulation ◽  
Temperature Control ◽  
Mold Temperature

scholarly journals Post-Processing Time Dependence of Shrinkage and Mechanical Properties of Injection-Molded Polypropylene

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 22
Author(s):  
Artur Kościuszko ◽  
Dawid Marciniak ◽  
Dariusz Sykutera
Keyword(s):  
Mechanical Properties ◽  
Impact Strength ◽  
Injection Molding ◽  
Accelerated Aging ◽  
Mold Temperature ◽  
Degree Of Crystallinity ◽  
Injection Mold ◽  
Secondary Crystallization ◽  
Scanning Calorimetry ◽  
Injection Molded

Dimensions of the injection-molded semi-crystalline materials (polymeric products) decrease with the time that elapses from their formation. The post-molding shrinkage is an effect of secondary crystallization; the increase in the degree of polymer crystallinity leads to an increase in stiffness and decrease in impact strength of the polymer material. The aim of this study was to assess the changes in the values of post-molding shrinkage of polypropylene produced by injection molding at two different temperatures of the mold (20 °C and 80 °C), and conditioned for 504 h at 23 °C. Subsequently, the samples were annealed for 24 h at 140 °C in order to conduct their accelerated aging. The results of shrinkage tests were related to the changes of mechanical properties that accompany the secondary crystallization. The degree of crystallinity of the conditioned samples was determined by means of density measurements and differential scanning calorimetry. It was found that the changes in the length of the moldings that took place after removal from the injection mold were accompanied by an increase of 20% in the modulus of elasticity, regardless of the conditions under which the samples were made. The differences in the shrinkage and mechanical properties of the samples resulting from mold temperature, as determined by tensile test, were removed by annealing. However, the samples made at two different injection mold temperature values still significantly differed in impact strength, the values of which were clearly higher for the annealed samples compared to the results determined for the samples immediately after the injection molding.

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