scholarly journals Template-free cyclic hexavanadate: Synthesis, characterization, solid-state structure, and solution-state dynamics

Polyhedron ◽  
2019 ◽  
Vol 169 ◽  
pp. 266-277 ◽  
Author(s):  
Rami J. Batrice ◽  
Jennifer N. Wacker ◽  
Elliot N. Glass ◽  
Safia Z. Jilani ◽  
YuYe J. Tong ◽  
...  
Keyword(s):  
Solid State ◽  
State Structure ◽  
Solid State Structure ◽  
Solution State ◽  
Template Free

NMR Study of the Solution-State Dynamics and Solid-State Structure of Tri-n-butyltin Fluoride

1994 ◽  
Vol 98 (18) ◽  
pp. 4919-4922 ◽  
Author(s):  
Y. W. Kim ◽  
A. Labouriau ◽  
C. M. Taylor ◽  
William L. Earl ◽  
L. G. Werbelow
Keyword(s):  
Solid State ◽  
State Structure ◽  
Solid State Structure ◽  
Solution State ◽  
Nmr Study

scholarly journals Does the solid-state structure of endothelin-1 provide insights concerning the solution-state conformational equilibrium?

FEBS Letters ◽  
1994 ◽  
Vol 355 (2) ◽  
pp. 140-146 ◽  
Author(s):  
Gregory M. Lee ◽  
Chinpan Chen ◽  
Thomas M. Marschner ◽  
Niels H. Andersen
Keyword(s):  
Solid State ◽  
Conformational Equilibrium ◽  
State Structure ◽  
Solid State Structure ◽  
Endothelin 1 ◽  
Solution State

scholarly journals Solid-state structure, solution-state behaviour and catalytic activity of electronically divergent C,N-chelating palladium–N-heterocyclic carbene complexes

2015 ◽  
Vol 44 (36) ◽  
pp. 15938-15948 ◽  
Author(s):  
Michael R. Chapman ◽  
Benjamin R. M. Lake ◽  
Christopher M. Pask ◽  
Bao N. Nguyen ◽  
Charlotte E. Willans
Keyword(s):  
Catalytic Activity ◽  
Solid State ◽  
Cross Coupling ◽  
State Structure ◽  
Carbene Complexes ◽  
Solid State Structure ◽  
Solution State ◽  
Structure Solution ◽  
State Behaviour

Electronically diverse pyridyl-substituted Pd(ii)-NHC complexes have been employed in Suzuki–Miyaura cross-coupling to yield a sterically congested tetra-ortho-substituted biaryl product.

1,2-Hydroboration and 1,1-Carboboration of Alkynyl(ferrocenyl)vinylsilanes. Novel Siloles

2014 ◽  
Vol 69 (11-12) ◽  
pp. 1269-1289 ◽  
Author(s):  
Bernd Wrackmeyer ◽  
Elena V. Klimkina ◽  
Wolfgang Milius ◽  
Christian Butterhof ◽  
Kathrin Inzenhofer
Keyword(s):  
Solid State ◽  
Single Molecule ◽  
State Structure ◽  
Solid State Structure ◽  
Solution State ◽  
Multinuclear Nmr ◽  
Nmr Parameters ◽  
Nmr Techniques ◽  
In The Beginning ◽  
Vinyl Group

Abstract Alkynyl(ferrocenyl)vinylsilanes containing up to three alkynyl units were prepared and treated with 9-borabicyclo[3.3.1]nonane (9-BBN). All reactions proceeded in the beginning by regioselective 1,2-hydroboration of the vinyl group, with boron attached to the terminal carbon. This was followed by intra-molecular 1,1-carboboration, leading to fused silacarbacycles, depending on the number of C≡C bonds. Thus, new siloles and even fused siloles became available. The solution-state structures were revealed by multinuclear NMR techniques (1H, 11B, 13C, 29Si NMR), complemented by calculated single-molecule structures and calculated NMR parameters at the B3LYP/6-311+G(d,p) level of theory. In one case, the solid-state structure of a bicyclic derivative was determined.

Receptor-Bound Conformation of Cilengitide Better Represented by Its Solution-State Structure than the Solid-State Structure

2014 ◽  
Vol 20 (44) ◽  
pp. 14201-14206 ◽  
Author(s):  
Udaya Kiran Marelli ◽  
Andreas O. Frank ◽  
Bernhard Wahl ◽  
Valeria La Pietra ◽  
Ettore Novellino ◽  
...  
Keyword(s):  
Solid State ◽  
State Structure ◽  
Solid State Structure ◽  
Solution State

Moschamindole

2000 ◽  
Vol 57 (1) ◽  
pp. o81-o82 ◽  
Author(s):  
Philip J. Cox ◽  
Margot Fergusson ◽  
Lutfun Nahar ◽  
Satyajit D. Sarker
Keyword(s):  
Hydrogen Bonding ◽  
Solid State ◽  
Intermolecular Hydrogen Bonding ◽  
State Structure ◽  
Solid State Structure ◽  
Solution State

The solid state structure of moschamindole {systematic name: 10-[2-(4-hydroxy-3-methoxyphenyl)]-1,2,3,4,10,10a-hexahydro-6H-furo[2,3,4-jk]pyrrolo[4,3,2-ef]-3-benzazocin-1-one}, C20H18N2O4is similar to its solution state structure, previously determined by NMR, and evidence of intermolecular hydrogen bonding is now presented.

The structure of [Cu(bipy)3][Cu(bipy)(ala)(ClO4)2]ClO4 � a Compound with Two Different Coordination Modes in the same Complex

2008 ◽  
Vol 59 (11) ◽  
Author(s):  
Mircea Braban ◽  
Ionel Haiduc
Keyword(s):  
Solid State ◽  
Chelate Ring ◽  
Octahedral Complex ◽  
State Structure ◽  
Complex Species ◽  
Solid State Structure ◽  
Coordination Modes ◽  
Coordination Center ◽  
Self Assembled ◽  
Chelate Rings

The paper describes the solid state structure of a compound of composition [Cu(bipy)3][Cu(bipy)(ala) (ClO4)2]ClO4, in which both the cation and anion are octahedral complex species with copper(II) as coordination center. The cation contains three chelate rings formed by bipy; the anion contains in the quatorial plane a CuONC2 chelate ring formed by the alaninato ligand and a CuN2C2 chelate ring formed by bipy, with two monodentate perchorato ligands in axial positions completing the six-coordination. In the crystal p-p stackings lead to a supramolecular self-assembled structure.

Synthesis and Solid-State Structure of (4-Hydroxy-3,5-diiodophenyl)phosphine Oxides. Dimeric Motifs with the Assistance of O-H···O=P Hydrogen Bonds

2015 ◽  
Vol 19 (5) ◽  
pp. 469-474 ◽  
Author(s):  
Nicholas Bewick ◽  
Agata Arendt ◽  
Yan Li ◽  
S.awomir Szafert ◽  
Tadeusz Lis ◽  
...  
Keyword(s):  
Solid State ◽  
Hydrogen Bonds ◽  
Phosphine Oxides ◽  
State Structure ◽  
Solid State Structure
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