Lanthanide complexes with pyridinecarboxylic acids – Spectroscopic and thermal studies

Polyhedron ◽  
2018 ◽  
Vol 150 ◽  
pp. 97-109 ◽  
Author(s):  
Grzegorz Świderski ◽  
Monika Kalinowska ◽  
Agnieszka Z. Wilczewska ◽  
Julita Malejko ◽  
Włodzimierz Lewandowski
Keyword(s):  
Lanthanide Complexes ◽  
Thermal Studies ◽  
Pyridinecarboxylic Acids

Synthesis, Characterization and Thermal studies of Novel Organomercury Driven from Sulfa Drugs Part 1

2011 ◽  
Vol 7 (2) ◽  
pp. 1338-1347
Author(s):  
Tarek Ali Fahad ◽  
Shaker.A.N. AL-Jadaan
Keyword(s):  
Thermal Decomposition ◽  
Thermal Behavior ◽  
1H Nmr ◽  
Elemental Analysis ◽  
Thermal Studies ◽  
Spectroscopic Techniques ◽  
Sulfa Drugs ◽  
Acid Base ◽  
Ph Values ◽  
Multi Stage

Two new heterocyclic Organmercury compounds   were prepared from the reaction of Sulfamethaxazole and Sulfadiazine with 4-acetaminophenol as a coupler and separated as solids with characteristic colors. these compounds were characterized by F.T.IR-spectroscopy 1H-NMR , Micro-elemental Analysis and UV-Vis spectroscopic techniques . The work involves a study of acid – base properties compounds at different pH values, the ionization and protonation constants were calculated. The thermal behavior of these two compounds   were investigated on the basis of thermogravimetric (TGA) and differential thermogravimetric (DTG) analyses, Thermal decomposition of these compounds is multi-stage processes.

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