Synthesis and characterization of the [Ni6Ge13(CO)5]4− and [Ge9Ni2(PPh3)]2− Zintl ion clusters

Polyhedron ◽  
2006 ◽  
Vol 25 (2) ◽  
pp. 521-529 ◽  
Author(s):  
Emren N. Esenturk ◽  
James Fettinger ◽  
Bryan Eichhorn
Keyword(s):  
Synthesis And Characterization ◽  
Ion Clusters ◽  
Zintl Ion

Probing Individual Steps of Dynamic Exchange with31P EXSY NMR Spectroscopy:  Synthesis and Characterization of the [E7PtH(PPh3)]2-Zintl Ion Complexes [E = P, As]

2000 ◽  
Vol 122 (45) ◽  
pp. 11101-11107 ◽  
Author(s):  
Banu Kesanli ◽  
Scott Charles ◽  
Yiu-Fai Lam ◽  
Simon G. Bott ◽  
James Fettinger ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Synthesis And Characterization ◽  
Dynamic Exchange ◽  
Zintl Ion

Synthesis and Characterization of the Three Dicyclopentapyrenes

1996 ◽  
Vol 61 (10) ◽  
pp. 3572-3572
Author(s):  
Lawrence T. Scott ◽  
Atena Necula
Keyword(s):  
Synthesis And Characterization

Synthesis and characterization of TiN / Ti / AISI 410 coatings

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama
Keyword(s):  
Synthesis And Characterization ◽  
Photoemission Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Columnar Grains ◽  
Tin Thin Films ◽  
Steel Aisi ◽  
Interacting Surfaces ◽  
Stainless Steel Aisi

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.

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