scholarly journals Effects of annealing time on the structure and optical properties of ZnAl2O4/ZnO prepared via citrate sol-gel process

2018 ◽  
Vol 14 ◽  
pp. 294-301 ◽  
Author(s):  
Setumo Victor Motloung ◽  
Pushpa Kumari ◽  
Lehlohonolo Fortune Koao ◽  
Tshwafo Elias Motaung ◽  
Thulani Thokozani Hlatshwayo ◽  
...  
2011 ◽  
Vol 509 (30) ◽  
pp. 7854-7860 ◽  
Author(s):  
A. Esmaielzadeh Kandjani ◽  
M. Farzalipour Tabriz ◽  
O. Mohammad Moradi ◽  
H.R. Rezaeian Mehr ◽  
S. Ahmadi Kandjani ◽  
...  

1991 ◽  
Vol 74 (1) ◽  
pp. 238-240 ◽  
Author(s):  
Masayuki Nogami ◽  
Yi-Qing Zhu ◽  
Yoshihide Tohyama ◽  
Katsumi Nagasaka ◽  
Takashi Tokizaki ◽  
...  

2004 ◽  
Vol 458 (1-2) ◽  
pp. 274-280 ◽  
Author(s):  
H. Guo ◽  
W. Zhang ◽  
L. Lou ◽  
A. Brioude ◽  
J. Mugnier

2019 ◽  
Vol 07 (01n02) ◽  
pp. 1950002
Author(s):  
Nadir Lalou ◽  
Ahmed Kadari

This work proposes the synthesis of nanocrystalline calcium oxide (CaO) pure and doped with different concentrations of lithium (Li[Formula: see text]) ions by sol–gel process. Calcium nitrate (Ca(NO[Formula: see text]4H2O; 99.99%) and lithium nitrate (LiNO3; 99.99%) were used as precursors. The synthesized powders were characterized by several techniques such as: UV-Vis transmission spectroscopy, Fourier Transform Infra-red spectroscopy (FT-IR) and X-ray diffraction (XRD). The main objective of this paper is to study the influence of lithium (Li[Formula: see text] ratio) on the structural and optical properties of synthesized powders. The band gap values decreased with the increasing of Li[Formula: see text] ions in CaO lattice; the slight change in the band gap was directly related to the energy transfer between the CaO excited states and the 2s levels of Li[Formula: see text] ions. The influence of Li[Formula: see text] doping on the physical properties of CaO nanocrystalline will be studied for the first time in this work; no literature has previously published this kind of impurities.


2009 ◽  
Vol 620-622 ◽  
pp. 651-654
Author(s):  
Leticia M. Torres-Martínez ◽  
Cecilia Sánchez-Trinidad ◽  
Vicente Rodríguez-González ◽  
Ricardo Gómez

Indium-alkali microfibers doped ceramic were prepared by the sol-gel process. The gels preparation samples, were heat treated at 700°C for different length of time. The products were characterized by means of XRD, SEM-EDS and UV–Vis-DRS. The XRD showed the formation of the Na2Ti6O13 phase whose crystallinity depends on the annealing time. The band gap calculated from the UV–Vis Kubelka-Munk function shows very similar values (3.53-3.55 eV). The SEM images of the indium-alkali titanates show microfiber clumps morphologies of about 5 µm, and the EDS spectra show that In2O3 is on the Na2Ti6O13 surface. The results of the evaluation of the In-Na2Ti6O13 semiconductors in the 2, 4-dichlorophenoxyacetic acid (2, 4-D) photodecomposition under UV light irradiation, show that the photoactivity depends on the time of heat treatment of the samples.


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