Microstructural investigation of stress-assisted α″–α′ phase transformation in cold-rolled Ti–7.5Mo alloy

Micron ◽  
2014 ◽  
Vol 65 ◽  
pp. 34-44 ◽  
Author(s):  
Yen-Chun Chen ◽  
Chien-Ping Ju ◽  
Jiin-Huey Chern Lin
Keyword(s):  
Phase Transformation ◽  
Microstructural Investigation ◽  
Α Phase ◽  
Cold Rolled

Effects of α–γ–α Phase Transformation on the ∑3 Boundaries in High-Purity Iron

2021 ◽  
Author(s):  
Syed Ejaz Hussain ◽  
Weiguo Wang ◽  
Xinfu Gu ◽  
Yunkai Cui ◽  
Ahua Du ◽  
...  
Keyword(s):  
Phase Transformation ◽  
High Purity ◽  
Α Phase ◽  
Purity Iron ◽  
High Purity Iron

scholarly journals Oxygen Induced Phase Transformation in TC21 Alloy with a Lamellar Microstructure

Metals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 163
Author(s):  
Shu Wang ◽  
Yilong Liang ◽  
Hao Sun ◽  
Xin Feng ◽  
Chaowen Huang
Keyword(s):  
Electron Microscopy ◽  
Phase Transformation ◽  
Oxygen Uptake ◽  
Titanium Alloys ◽  
Electron Backscatter Diffraction ◽  
Lamellar Microstructure ◽  
Α Phase ◽  
Transmission Electron ◽  
The Matrix ◽  
Oxygen Ingress

The main objective of the present study was to understand the oxygen ingress in titanium alloys at high temperatures. Investigations reveal that the oxygen diffusion layer (ODL) caused by oxygen ingress significantly affects the mechanical properties of titanium alloys. In the present study, the high-temperature oxygen ingress behavior of TC21 alloy with a lamellar microstructure was investigated. Microstructural characterizations were analyzed through optical microscopy (OM), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and transmission electron microscopy (TEM). Obtained results demonstrate that oxygen-induced phase transformation not only enhances the precipitation of secondary α-phase (αs) and forms more primary α phase (αp), but also promotes the recrystallization of the ODL. It was found that as the temperature of oxygen uptake increases, the thickness of the ODL initially increases and then decreases. The maximum depth of the ODL was obtained for the oxygen uptake temperature of 960 °C. In addition, a gradient microstructure (αp + β + βtrans)/(αp + βtrans)/(αp + β) was observed in the experiment. Meanwhile, it was also found that the hardness and dislocation density in the ODL is higher than that that of the matrix.

scholarly journals High-Performance Formamidinium-Based Perovskite Solar Cells via Microstructure-Mediated δ-to-α Phase Transformation

2017 ◽  
Vol 29 (7) ◽  
pp. 3246-3250 ◽  
Author(s):  
Tanghao Liu ◽  
Yingxia Zong ◽  
Yuanyuan Zhou ◽  
Mengjin Yang ◽  
Zhen Li ◽  
...  
Keyword(s):  
Phase Transformation ◽  
Solar Cells ◽  
High Performance ◽  
Perovskite Solar Cells ◽  
Α Phase

Microstructure and Texture Evolution in a Cold-Rolled High Mn Steel with Microadditions of Ti and Nb

2013 ◽  
Vol 203-204 ◽  
pp. 71-76
Author(s):  
Sławomir Kołodziej ◽  
Joanna Kowalska ◽  
Wiktoria Ratuszek ◽  
Wojciech Ozgowicz ◽  
Krzysztof Chruściel
Keyword(s):  
Plastic Deformation ◽  
Texture Evolution ◽  
Hexagonal Structure ◽  
Cold Plastic Deformation ◽  
Α Phase ◽  
Ε Phase ◽  
Cold Rolled ◽  
Goss Orientation ◽  
Mn Steel ◽  
Microscopic Investigations

The aim of this work was the microstructure and texture analysis of a deformed via cold-rolling 24.5Mn-3.5Si-1.5Al-Ti-Nb TWIP/TRIP type steel. It was found, that during cold plastic deformation a phase transformation of austenite into martensite takes place. The transformation progress was confirmed by the microscopic investigations. The texture of austenite is characterized by a limited α1=||RD fibre and the γ=||ND fibre. The texture of austenite changed with increasing deformation rate. In the texture of deformed austenite the strongest orientation is the {110} Goss orientation, which belongs to the α=||ND orientation fibre. During cold plastic deformation γ→ε and γ→ε→α’ phase transformations as well as the deformation of γ, ε and α’ phases are taking place in the steel. The formed ε phase (hexagonal structure) also possesses a distinct texture.

Atomic-scale understanding of stress-induced phase transformation in cold-rolled Hf

2017 ◽  
Vol 131 ◽  
pp. 271-279 ◽  
Author(s):  
Henglv Zhao ◽  
Min Song ◽  
Song Ni ◽  
Shuai Shao ◽  
Jian Wang ◽  
...  
Keyword(s):  
Phase Transformation ◽  
Atomic Scale ◽  
Cold Rolled

scholarly journals Formation of Large Size Precipitate-Free Zones in β Annealing of the Near-β Ti-55531 Titanium Alloy

Metals ◽  
2019 ◽  
Vol 9 (5) ◽  
pp. 544 ◽  
Author(s):  
Xueqi Jiang ◽  
Xiaoqiang Shi ◽  
Xiaoguang Fan ◽  
Qi Li
Keyword(s):  
Titanium Alloy ◽  
Phase Transformation ◽  
Heterogeneous Nucleation ◽  
Isothermal Heat Treatment ◽  
Precipitate Free Zone ◽  
Mode Iii ◽  
Slow Cooling ◽  
Free Zone ◽  
Large Size ◽  
Α Phase

Large size (>10000 μm2) precipitate-free zones in the absence of microsegregation were observed in the near-β Ti-55531 titanium alloy after furnace cooling from high temperature and longtime annealing in the single-β phase field. To reveal the formation mechanism of the large size precipitate-free zone, continuous cooling and isothermal heat treatment were carried out to investigate the β-α phase transformation process. It was found that the large size precipitate free zone is attributed to the heterogeneous nucleation of α phase. The nucleation site evolves in three different modes: I-random nucleation inside the β grain, II-network nucleation inside the β grain and, III-heterogeneous nucleation on the precipitated α phase. Modes I and II lead to homogeneous transformed structure while Mode III results in the large size precipitate-free zone. Both modes II and III are promoted at high annealing temperature, rapid cooling above 600 °C or slow cooling below 600 °C. Mode II is common as it can minimize the strain energy in phase transformation. As a result, the formation of the large size precipitate-free zone is not deterministic.

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