Determining trace metal elements in the tooth enamel from Hui and Han Ethnic groups in China using microwave digestion and inductively coupled plasma mass spectrometry (ICP-MS)

2016 ◽  
Vol 127 ◽  
pp. 142-144 ◽  
Author(s):  
Maoyong He ◽  
Hai Lu ◽  
Chongguang Luo ◽  
Tongxiang Ren
Keyword(s):  
Mass Spectrometry ◽  
Trace Metal ◽  
Ethnic Groups ◽  
Inductively Coupled Plasma ◽  
Tooth Enamel ◽  
Microwave Digestion ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Trace Metal Elements ◽  
Plasma Mass Spectrometry

scholarly journals Simultaneous Analysis of Cadmium, Lead, Mercury, and Arsenic Content in Foodstuffs of Animal Origin by Inductively Coupled Plasma/Mass Spectrometry after Closed Vessel Microwave Digestion: Method Validation

2005 ◽  
Vol 88 (6) ◽  
pp. 1811-1821 ◽  
Author(s):  
Laurent Noël ◽  
Vincent Dufailly ◽  
Nadège Lemahieu ◽  
Christelle Vastel ◽  
Thierry Guérin
Keyword(s):  
Mass Spectrometry ◽  
Method Validation ◽  
Inductively Coupled Plasma ◽  
Limit Of Detection ◽  
Microwave Digestion ◽  
Animal Origin ◽  
Closed Vessel ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Plasma Mass Spectrometry

Abstract A method validation of the total analysis of cadmium (Cd), lead (Pb), arsenic (As), and mercury (Hg) in foodstuffs by inductively coupled plasma/mass spectrometry (ICP/MS) after closed vessel microwave digestion is presented. Due to the lack of reference method for ICP/MS techniques in food and, based on the project of the European Committee of Normalization (CEN/TC 275/WG 10), the Agence Française de Normalisation (AFNOR) guidelines NF V03–110 were used for the evaluation of this method based on 2 steps, sample preparation and multielement detection. Several criteria considered as compulsory (linearity, specificity, precision under repeatability conditions, and trueness) have been estimated and discussed, in addition to intermediate precision reproducibility, the limit of detection, and the limit of quantification. Furthermore, a comparison with in-house methods using electrothermal atomic absorption was performed using an external proficiency testing scheme and food samples. The results indicated that this method could be used in the laboratory for the routine determination of these 4 cumulative toxic metals in foodstuffs with acceptable analytical performance.

scholarly journals Trace Metal Element Analysis in Some Seafood in the Coastal Zone of the Red River (Ba Lat Estuary, Vietnam) by Green Sample Preparation and Inductively Coupled Plasma-Mass Spectrometry (ICP-MS)

2021 ◽  
Vol 2021 ◽  
pp. 1-14
Author(s):  
Nhu Da Le ◽  
Thi Thu Ha Hoang ◽  
Vu Phong Phung ◽  
Thi Lien Nguyen ◽  
Thi Thuy Duong ◽  
...  
Keyword(s):  
Trace Metal ◽  
Coastal Zone ◽  
Inductively Coupled Plasma ◽  
Red River ◽  
Metal Elements ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Trace Metal Elements ◽  
Plasma Mass Spectrometry ◽  
Green Sample

Fisheries and aquaculture production in the coastal zone of Vietnam contribute significantly to the national economy. However, seafood quality and safety, especially in terms of metal contents, are of increasing concern, for both domestic and international markets. This paper presents the results of an investigation in some trace metal elements (iron (Fe), zinc (Zn), manganese (Mn), copper (Cu), arsenic (As), cadmium (Cd), and mercury (Hg)) concentrations in some fishes, crustaceans, and molluscs in the coastal zone of the Red River (in the Ba Lat estuary in Thai Binh and Nam Dinh provinces) during four sampling campaigns in 2020. All samples were treated by a green sample preparation using microwave digestion and then analyzed by inductively coupled plasma-mass spectrometry (ICP-MS). The results showed that the trace metal element concentrations in fish, crustacean, and mollusc samples decreased in the following order: Fe > Zn > Mn > Cu > As > Cd ∼ Hg. In more details, the ranges of trace metal elements in seafood samples were 13.13–202.73; 7.63–82.71; 0.48–22.73; 0.72–15.58; 0.18–5.12; 0.001–1.114; and 0.001–0.923 mg·kg−1 for Fe, Zn, Mn, Cu, As, Cd, and Hg, respectively. The research results contribute to the dataset of the seafood (both fishery and aquacultural seafood) quality in the Red River coastal zone. Although the mean values of different trace metal elements observed in this study were lower than the allowed values of Vietnam’s or European’s threshold for food safety, some high concentrations were detected. The survey results suggest the need to expand the monitoring scope (frequency of monitoring, number of samples, and observed variables) for obtaining a fully comprehensive assessment of seafood quality in this region. Our results also indicate that it is necessary to manage water quality in coastal areas, especially where aquaculture activities are carried out.

scholarly journals Optimized Simultaneous Determination of Several Elements in Human Intestinal Caco-2 TC7 Cells by Inductively Coupled Plasma-Mass Spectrometry after Closed Vessel Microwave Digestion

2003 ◽  
Vol 86 (6) ◽  
pp. 1225-1231 ◽  
Author(s):  
Laurent Noël ◽  
Thierry Guérin ◽  
Jean-Marc Frémy ◽  
Hélène Huet ◽  
Martine Kolf-Clauw
Keyword(s):  
Mass Spectrometry ◽  
Inductively Coupled Plasma ◽  
Certified Reference Materials ◽  
Microwave Digestion ◽  
Absorption Spectrometry ◽  
Inductively Coupled ◽  
Flame Atomic Absorption ◽  
Icp Ms ◽  
Plasma Mass Spectrometry

Abstract A rapid procedure, based on closed vessels microwave digestion and inductively coupled plasma-mass spectrometry (ICP-MS), was evaluated to ascertain the effect of chronic exposure to cadmium on intracellular accumulation of minor and essential trace elements in cultured epithelial cells (Caco-2 TC7). For all measurements, the method of external calibration was used and 3 elements (Be, Sc, In) were selected as internal standards. Optimization procedures are discussed and results are presented for the total determination of 9 key analytes (Na, Mg, Ca, Cr, Mn, Cu, Zn, Mo, and Cd) in certified reference materials (CRMs) and 20 samples of Caco-2 TC7 cells long-term exposed to Cd. The performance characteristics of the analytical system were evaluated by calibration and linearity, limits of detection and quantitation, accuracy with spiking, trueness and repeatability with available CRMs. As a complement to the ICP-MS determinations, both available CRMs and cell samples were analyzed either by electro thermal-or flame atomic absorption spectrometry. The results were in good agreement with the ICP-MS results.

Determination of Boron in Coal Using Closed-Vessel Microwave Digestion and Inductively Coupled Plasma Mass Spectrometry (ICP-MS)

2014 ◽  
Vol 28 (7) ◽  
pp. 4517-4522 ◽  
Author(s):  
Shifeng Dai ◽  
Weijiao Song ◽  
Lei Zhao ◽  
Xiao Li ◽  
James C. Hower ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Inductively Coupled Plasma ◽  
Microwave Digestion ◽  
Closed Vessel ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Plasma Mass Spectrometry

Determination of Elements in Carbon Fiber Using Inductively Coupled Plasma Mass Spectrometry (ICP-MS)

2013 ◽  
Vol 423-426 ◽  
pp. 767-770
Author(s):  
Ting Zhao ◽  
Ming Qiang Zhou ◽  
Wei Li Liu ◽  
Wei Huang ◽  
Jun Zhi He ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Carbon Fiber ◽  
Inductively Coupled Plasma ◽  
Microwave Digestion ◽  
Volatile Elements ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Dry Digestion ◽  
Plasma Mass Spectrometry

Based on microwave digestion and dry digestion, the concentrations of Si, S, Ca, Cr, Fe, Ni, Cu, Al, Mo, Sb, Ti, V, Y and Zn in carbon fiber were determined using inductively coupled plasma mass spectrometry (ICP-MS). Compare with the concentrations in the solution got by microwave digestion, the concentrations in the solution got by dry digestion are higher. And microwave digestion is more suitable for treatment of carbon fiber containing volatile elements than dry digestion.

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