Method development for the determination of PFOA and PFOS in honey based on the dispersive Solid Phase Extraction (d-SPE) with micro-UHPLC–MS/MS system

2015 ◽  
Vol 121 ◽  
pp. 150-156 ◽  
Author(s):  
Magdalena Surma ◽  
Wiesław Wiczkowski ◽  
Ewa Cieślik ◽  
Henryk Zieliński
Keyword(s):  
Solid Phase Extraction ◽  
Method Development ◽  
Solid Phase ◽  
Phase Extraction ◽  
Dispersive Solid Phase Extraction

Recent Trends in the Development of Green Microextraction Techniques for the Determination of Hazardous Organic Compounds in Wine

2019 ◽  
Vol 15 (7) ◽  
pp. 788-800 ◽  
Author(s):  
Natasa P. Kalogiouri ◽  
Victoria F. Samanidou
Keyword(s):  
Sample Preparation ◽  
Solid Phase Extraction ◽  
Organic Compounds ◽  
Method Development ◽  
Solid Phase ◽  
Stir Bar Sorptive Extraction ◽  
Phase Extraction ◽  
Microextraction Techniques ◽  
Hazardous Organic Compounds

Background:The sample preparation is the most crucial step in the analytical method development. Taking this into account, it is easily understood why the domain of sample preparation prior to detection is rapidly developing. Following the modern trends towards the automation, miniaturization, simplification and minimization of organic solvents and sample volumes, green microextraction techniques witness rapid growth in the field of food quality and safety. In a globalized market, it is essential to face the consumers need and develop analytical methods that guarantee the quality of food products and beverages. The strive for the accurate determination of organic hazards in a famous and appreciated alcoholic beverage like wine has necessitated the development of microextraction techniques.Objective:The objective of this review is to summarize all the recent microextraction methodologies, including solid phase extraction (SPE), solid phase microextraction (SPME), liquid-phase microextraction (LPME), dispersive liquid-liquid microextraction (DLLME), stir bar sorptive extraction (SBSE), matrix solid-phase dispersion (MSPD), single-drop microextraction (SDME) and dispersive solid phase extraction (DSPE) that were developed for the determination of hazardous organic compounds (pesticides, mycotoxins, colorants, biogenic amines, off-flavors) in wine. The analytical performance of the techniques is evaluated and their advantages and limitations are discussed.Conclusion:An extensive investigation of these techniques remains vital through the development of novel strategies and the implication of new materials that could upgrade the selectivity for the extraction of target analytes.

scholarly journals Dispersive solid-phase extraction based on butylamide silica for the determination of sulfamethoxazole in milk samples by capillary electrophoresis

2016 ◽  
Vol 39 (14) ◽  
pp. 658-665 ◽  
Author(s):  
Gabriela Islas ◽  
José A. Rodríguez ◽  
M. Elena Páez-Hernández ◽  
Silvia Corona-Avendaño ◽  
Alberto Rojas-Hernández ◽  
...  
Keyword(s):  
Capillary Electrophoresis ◽  
Solid Phase Extraction ◽  
Solid Phase ◽  
Phase Extraction ◽  
Dispersive Solid Phase Extraction ◽  
Milk Samples

Determination of active ingredients in Chinese medicine Danning Tablets using dispersion solid-phase extraction by molecular imprinting nanomaterials coupled with HPLC-DAD

2017 ◽  
Vol 9 (17) ◽  
pp. 2585-2589 ◽  
Author(s):  
Jieping Luo ◽  
Ning Chen ◽  
Zaiyue Yang ◽  
Jiyong Han ◽  
Wanying Zhu ◽  
...  
Keyword(s):  
Solid Phase Extraction ◽  
Molecularly Imprinted Polymers ◽  
Solid Phase ◽  
Phase Extraction ◽  
Dispersive Solid Phase Extraction ◽  
Molecularly Imprinted ◽  
Imprinted Polymers ◽  
Pretreatment Method ◽  
Magnetic Molecularly Imprinted Polymers

A reliable pretreatment method of magnetic molecularly imprinted polymers/dispersive solid-phase extraction was developed for selectivity and enrichment of targets.

Determination of phthalates in beverages using multiwalled carbon nanotubes dispersive solid-phase extraction before HPLC-MS

2018 ◽  
Vol 41 (12) ◽  
pp. 2613-2622 ◽  
Author(s):  
Javier González-Sálamo ◽  
Javier Hernández-Borges ◽  
María del Mar Afonso ◽  
Miguel Ángel Rodríguez-Delgado
Keyword(s):  
Carbon Nanotubes ◽  
Solid Phase Extraction ◽  
Multiwalled Carbon Nanotubes ◽  
Solid Phase ◽  
Phase Extraction ◽  
Dispersive Solid Phase Extraction ◽  
Multiwalled Carbon
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