scholarly journals Photometric determination of thioglycolic acid in cosmetics by using a stopped-flow reverse flow-injection system and the formation of gold nanoparticles

2011 ◽  
Vol 97 (2) ◽  
pp. 243-248 ◽  
Author(s):  
Marina Sierra-Rodero ◽  
Juan Manuel Fernández-Romero ◽  
Agustina Gómez-Hens
Keyword(s):  
Gold Nanoparticles ◽  
Flow Injection ◽  
Thioglycolic Acid ◽  
Reverse Flow ◽  
Photometric Determination ◽  
Injection System ◽  
Stopped Flow ◽  
Flow Injection System ◽  
Reverse Flow Injection

scholarly journals DETERMINATION OF NITRAZEPAM IN PHARMACEUTICAL PREPARATIONS USING SOLID-PHASE REACTOR - REVERSE FLOW INJECTION ANALYSIS

2018 ◽  
Vol 11 (7) ◽  
pp. 487
Author(s):  
Mariam Jamal ◽  
Hind Hadi
Keyword(s):  
Flow Injection ◽  
Solid Phase ◽  
Reverse Flow ◽  
Injection System ◽  
Physical Parameters ◽  
Relative Standard ◽  
Solid Phase Reactor ◽  
Oxidation Reactor ◽  
Reverse Flow Injection

Objective: A simple and fast reverse flow injection system including a solid-phase reactor containing PbO2 with spectrophotometric detection was suggested for the determination of nitrazepam (NIT) in pharmaceutical tablets.Methods: The method was based on oxidation of the reagent (phloroglucinol) with PbO2 immobilized in a polymeric matrix which was then coupled with reduced NIT in aqueous medium. The pink-colored product was measured at 530 nm.Results: The calibration graph was linear over the range of 50–400 μg/mL with a relative standard deviation of <2% (n=29) and a sample throughput of 48 samples per hour. The variables of the solid-phase reactor such as composition, particle size, and length of the reactor were studied. The chemical and physical parameters, which affect the reverse flow method, were also studied.Conclusion: The oxidation reactor engaged with a flow system was successfully applied for the determination of NIT with good sensitivity and precision.

Spectrofluorimetric optosensing of aluminium in a flow injection system: determination of aluminium in dialysis fluids and concentrates

The Analyst ◽  
1990 ◽  
Vol 115 (5) ◽  
pp. 575-579 ◽  
Author(s):  
Maria Rosario Pereiro García ◽  
Marta Elena Díaz García ◽  
Alfredo Sanz-Medel
Keyword(s):  
Flow Injection ◽  
Injection System ◽  
Flow Injection System ◽  
Dialysis Fluids
Sign in / Sign up

Export Citation Format

Share Document