A simple single molecular precursor route in the synthesis of high quality SnS nanoparticles

2016 ◽  
Vol 183 ◽  
pp. 30-33 ◽  
Author(s):  
V.S.R. Rajasekhar Pullabhotla ◽  
M.W. Mabila
RSC Advances ◽  
2019 ◽  
Vol 9 (54) ◽  
pp. 31386-31397 ◽  
Author(s):  
Nico Koslowski ◽  
Rudolf C. Hoffmann ◽  
Vanessa Trouillet ◽  
Michael Bruns ◽  
Sabine Foro ◽  
...  

Transformation of a new molecular precursor allows the formation of yttrium oxide under moderate conditions displaying high voltage breakthrough behaviour.


RSC Advances ◽  
2019 ◽  
Vol 9 (42) ◽  
pp. 24146-24153 ◽  
Author(s):  
Abdulaziz M. Alanazi ◽  
Firoz Alam ◽  
Abdelmajid Salhi ◽  
Mohamed Missous ◽  
Andrew G. Thomas ◽  
...  

In the present work we report on the synthesis of a tetragonal phase of stannite Cu2FeSnS4 powder from Sn(ii) and Sn(iv) using a solvent free melt method using a mixture of Cu, Fe, Sn(ii)/Sn(iv) O-ethylxanthates.


2019 ◽  
Vol 59 ◽  
pp. 161-165 ◽  
Author(s):  
Johannes Z. Mbese ◽  
Peter A. Ajibade ◽  
Funeka Matebese ◽  
Mojeed A. Agoro

We present the rational synthesis of novel nanocrystals CuS (nc-CuS) by single source molecular precursor (SSMP) method. Among the present materials synthetic routes, the SSMP route is high efficient and comfortable way to construct nanostructured materials. Both CuS nanocrystals capped with hexadecylamine (HDA) and trioctylphosphine oxide (TOPO) have been synthesized by thermolysing bis (N-diisopropyldithiocarbamate)Cu (II) complex at 180 °C. Various physicochemical characterizations such as SEM images of nc-CuS exhibited uniform exfoliated surface morphologies with uniform continuous network of about 50 μm agglomerated particles. Our method could be broadly applicable for the preparation of other high quality yield metal sulfide nanostructures


2003 ◽  
Vol 15 (5) ◽  
pp. 1040-1046 ◽  
Author(s):  
Richard L. Brutchey ◽  
Joshua E. Goldberger ◽  
Telly S. Koffas ◽  
T. Don Tilley

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