Synthesis of mesoporous titania and the photocatalytic activity for decomposition of methyl orange

2006 ◽  
Vol 60 (20) ◽  
pp. 2493-2496 ◽  
Author(s):  
Zhonghua Wang ◽  
Tingshun Jiang ◽  
Yongmin Du ◽  
Kangmin Chen ◽  
Hengbo Yin
Keyword(s):  
Photocatalytic Activity ◽  
Methyl Orange ◽  
Mesoporous Titania

Preparation of (Fe, Ni)-Codoped ZnO and Its Photocatalytic Activity for Deg-radation of Methyl Orange

2010 ◽  
Vol 31 (7) ◽  
pp. 797-802 ◽  
Author(s):  
Tianhua FU ◽  
Qianqian GAO ◽  
Fei LIU ◽  
Huajun DAI ◽  
Xingming KOU
Keyword(s):  
Photocatalytic Activity ◽  
Methyl Orange

scholarly journals Tailoring Mesoporous Titania Features by Ultrasound-Assisted Sol-Gel Technique: Effect of Surfactant/Titania Precursor Weight Ratio

Nanomaterials ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 1263
Author(s):  
Elvira Mahu ◽  
Cristina Giorgiana Coromelci ◽  
Doina Lutic ◽  
Iuliean Vasile Asaftei ◽  
Liviu Sacarescu ◽  
...  
Keyword(s):  
Photocatalytic Activity ◽  
Sol Gel ◽  
Weight Ratio ◽  
Soft Template ◽  
Synthesis Process ◽  
Mesoporous Titania ◽  
Cavitation Effect ◽  
Titania Precursor ◽  
Gel Technique ◽  
Ultrasound Assisted

A mesoporous titania structure has been prepared using the ultrasound-assisted sol-gel technique in order to find out a way to tailor its structure. The TiO2 obtained was compared to the same version of titania but synthesized by a conventional sol-gel method with the objective of understanding the effect of ultrasound in the synthesis process. All synthesis experiments were focused on the preparation of a titania photocatalyst. Thus, the anatase photocatalytic active phase of titania was proven by X-ray diffraction. Additionally, the ultrasonation treatment proved to increase the crystallinity of titania samples, being one of the requirements to having good photocatalytic activity for titania. The influence of surfactant/titania precursor weight ratio on the structural (XRD), textural (N2-sorption measurements), morphological (TEM), surface chemistry (FTIR) and optical properties (UVDR) was investigated. It was observed that the crystallite size, specific surface area, band gap energy and even photocatalytic activity was affected by the synergism occurring between cavitation effect and the surfactant/titania precursor weight ratio. The study yielded interesting great results that could be considered for further application of ultrasound to tailor mesoporous titania features via sol-gel soft template synthesis, against conventional sol-gel process.

scholarly journals Synthesis of a mesoporous titania thin film with a pseudo-single-crystal framework by liquid-phase epitaxial growth, and enhancement of photocatalytic activity

RSC Advances ◽  
2020 ◽  
Vol 10 (67) ◽  
pp. 40658-40662
Author(s):  
Norihiro Suzuki ◽  
Chiaki Terashima ◽  
Kazuya Nakata ◽  
Ken-ichi Katsumata ◽  
Akira Fujishima
Keyword(s):  
Thin Film ◽  
Photocatalytic Activity ◽  
Liquid Phase ◽  
Single Crystal ◽  
Chemical Process ◽  
Anatase Phase ◽  
Mesoporous Titania ◽  
Titania Thin Film ◽  
Liquid Phase Epitaxial Growth ◽  
Pseudo Single Crystal

An anatase-phase mesoporous titania thin film with a pseudo-single-crystal framework was facilely synthesized by an inexpensive chemical process.

Solar, visible and UV light photocatalytic activity of CoWO4for the decolourization of methyl orange

2014 ◽  
Vol 54 (11) ◽  
pp. 3134-3145 ◽  
Author(s):  
Kandasamy Jothivenkatachalam ◽  
Saravanan Prabhu ◽  
Arjunan Nithya ◽  
Singaravelu Chandra Mohan ◽  
Kulandaivel Jeganathan
Keyword(s):  
Photocatalytic Activity ◽  
Methyl Orange ◽  
Uv Light

scholarly journals Zirconium-Doped Chromium IV Oxide Nanocomposites: Synthesis, Characterization, and Photocatalysis towards the Degradation of Organic Dyes

Catalysts ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 117
Author(s):  
Zahir Muhammad ◽  
Farman Ali ◽  
Muhammad Sajjad ◽  
Nisar Ali ◽  
Muhammad Bilal ◽  
...  
Keyword(s):  
Methylene Blue ◽  
Photocatalytic Activity ◽  
Methyl Orange ◽  
Solid State ◽  
Room Temperature ◽  
Organic Dyes ◽  
Uv Light ◽  
Heterogeneous Photocatalysis ◽  
Ft Ir ◽  
Complete Mineralization

Degradation of organic dyes and their byproducts by heterogeneous photocatalysts is an essential process, as these dyes can be potentially discharged in wastewater and threaten aquatic and xerophyte life. Therefore, their complete mineralization into nontoxic components (water and salt) is necessary through the process of heterogeneous photocatalysis. In this study, Zr/CrO2 (Zirconium-doped chromium IV oxide) nanocomposite-based photocatalysts with different compositions (1, 3, 5, 7 & 9 wt.%) were prepared by an environmentally friendly, solid-state reaction at room temperature. The as-prepared samples were calcined under air at 450 °C in a furnace for a specific period of time. The synthesis of Zr/CrO2 photocatalysts was confirmed by various techniques, including XRD, SEM, EDX, FT-IR, UV-Vis, and BET. The photocatalytic properties of all samples were tested towards the degradation of methylene blue and methyl orange organic dyes under UV light. The results revealed a concentration-dependent photocatalytic activity of photocatalysts, which increased the amount of dopant (up to 5 wt.%). However, the degradation efficiency of the catalysts decreased upon further increasing the amount of dopant due to the recombination of holes and photoexcited electrons.

scholarly journals The Role of H2C2O4 and Na2CO3 as Precipitating Agents on The Physichochemical Properties and Photocatalytic Activity of Bismuth Oxide

2020 ◽  
Vol 18 (1) ◽  
pp. 129-137
Author(s):  
Yayuk Astuti ◽  
Rizka Andianingrum ◽  
Abdul Haris ◽  
Adi Darmawan ◽  
Keyword(s):  
Photocatalytic Activity ◽  
Methyl Orange ◽  
Physicochemical Properties ◽  
Bismuth Oxide ◽  
Rate Constants ◽  
Degradation Rate ◽  
Precipitation Method ◽  
Methyl Orange Degradation ◽  
Methyl Orange Dye

AbstractSynthesis of bismuth oxide synthesis through the precipitation method using H2C2O4 and Na2CO3 precipitating agents, identification of physicochemical properties and its photocatalysis activity for methyl orange degradation were conducted. The bismuth oxide synthesis was undertaken by dissolving Bi(NO3)3.5H2O in HNO3, then added precipitating agents to form precipitate. The results showed that bismuth oxide produced by H2C2O4 precipitating agent was a yellow powder containing a mixture of α-Bi2O3 (monoclinic) and β-Bi2O3 (tetragonal), porous with size of 28-85 μm. Meanwhile, the use of Na2CO3 as precipitating agent resulted in bismuth oxide consisting of α-Bi2O3 and β-Bi2O3 and Bi2O4, irregular shape without pore being 40-115 μm in size. Bismuth oxide synthesized with H2C2O4 precipitating agent showed higher photocatalytic activity compared to bismuth oxide synthesized using Na2CO3 on degrading methyl orange dye with degradation rate constants of 2.35x10-5 s-1 for H2C2O4 and 1.81x10-5 s-1 for Na2CO3.

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