Synthesis of lead oxide nanoparticles by Sonochemical method and its application as cathode and anode of lead-acid batteries

2008 ◽  
Vol 108 (2-3) ◽  
pp. 337-344 ◽  
Author(s):  
Hasan Karami ◽  
Mohammad Ali Karimi ◽  
Saeed Haghdar ◽  
Abbas Sadeghi ◽  
Rasool Mir-Ghasemi ◽  
...  
Keyword(s):  
Lead Oxide ◽  
Oxide Nanoparticles ◽  
Sonochemical Method ◽  
Lead Acid Batteries ◽  
Lead Acid

Recycling lead from spent lead pastes using oxalate and sodium oxalate and preparation of novel lead oxide for lead-acid batteries

RSC Advances ◽  
2015 ◽  
Vol 5 (115) ◽  
pp. 94895-94902 ◽  
Author(s):  
Cheng Ma ◽  
Yuehong Shu ◽  
Hongyu Chen
Keyword(s):  
Energy Cost ◽  
Lead Oxide ◽  
Low Energy ◽  
Sodium Oxalate ◽  
Lead Acid Batteries ◽  
Smelting Method ◽  
Lead Acid

A sustainable method, with minimal pollution and low energy cost in comparison with the conventional smelting method, is proposed for treating components of spent lead acid batteries with oxalate and sodium oxalate.

Lead recovery from spent lead acid battery paste by hydrometallurgical conversion and thermal degradation

2019 ◽  
Vol 38 (3) ◽  
pp. 263-270
Author(s):  
Wenke Liu ◽  
Qingwei Qin ◽  
Dengqi Li ◽  
Guangqiang Li ◽  
Yinjie Cen ◽  
...  
Keyword(s):  
Thermal Degradation ◽  
Lead Oxide ◽  
Lead Dioxide ◽  
Scanning Calorimetry ◽  
Lead Carbonate ◽  
Lead Acid Batteries ◽  
Novel Approach ◽  
Lead Recovery ◽  
Main Component ◽  
Lead Acid

Spent lead paste is the main component in lead-acid batteries reaching end of life. It contains about 55% lead sulphate and 35% lead dioxide, as well as minor amounts of lead oxide. It is necessary to recycle spent lead paste with minimal pollution and low energy consumption instead of the conventional smelting method. In this study, a novel approach involving hydrometallurgical desulphurisation and thermal degradation is developed to recover lead as PbO products from spent lead acid batteries. First, the desulphurisation effects and phase compositions of products with different transforming agents were compared, and the optimum conditions using (NH4)2CO3 as a transforming agent were determined. And then, the thermal degradation processes of both precursors lead carbonate and lead dioxide were investigated to prepare α-PbO, Pb3O4, and β-PbO products in argon and air atmospheres, respectively. Both the desulphurisation precursors and the calcination products were characterised by thermogravimetry and differential scanning calorimetry, X-ray diffraction, and scanning electron microscopy. The results showed that the lead oxide products were prepared, including α-PbO at 450°C in argon, Pb3O4 and β-PbO at 480°C and 620°C in air, respectively.

Effect of iron doped lead oxide on the performance of lead acid batteries

2011 ◽  
Vol 196 (20) ◽  
pp. 8802-8808 ◽  
Author(s):  
Jianwen Liu ◽  
Danni Yang ◽  
Linxia Gao ◽  
Xinfeng Zhu ◽  
Lei Li ◽  
...  
Keyword(s):  
Lead Oxide ◽  
Lead Acid Batteries ◽  
Iron Doped ◽  
Lead Acid

Preparation of High Purity Lead Oxide from Spent Lead Acid Batteries via Desulfurization and Recrystallization in Sodium Hydroxide

2016 ◽  
Vol 55 (7) ◽  
pp. 2059-2068 ◽  
Author(s):  
Junqing Pan ◽  
Xuan Zhang ◽  
Yanzhi Sun ◽  
Shuang Song ◽  
Wei Li ◽  
...  
Keyword(s):  
Sodium Hydroxide ◽  
High Purity ◽  
Lead Oxide ◽  
Lead Acid Batteries ◽  
Lead Acid

The effect and mechanism of bismuth doped lead oxide on the performance of lead-acid batteries

2001 ◽  
Vol 95 (1-2) ◽  
pp. 108-118 ◽  
Author(s):  
H.Y Chen ◽  
L Wu ◽  
C Ren ◽  
Q.Z Luo ◽  
Z.H Xie ◽  
...  
Keyword(s):  
Lead Oxide ◽  
Lead Acid Batteries ◽  
Lead Acid

The effect of barium sulfate-doped lead oxide as a positive active material on the performance of lead acid batteries

RSC Advances ◽  
2016 ◽  
Vol 6 (32) ◽  
pp. 27205-27212 ◽  
Author(s):  
Xiqing Yuan ◽  
Jingping Hu ◽  
Jingyi Xu ◽  
Yucheng Hu ◽  
Wei Zhang ◽  
...  
Keyword(s):  
Lead Oxide ◽  
Barium Sulfate ◽  
Active Material ◽  
Active Materials ◽  
Positive Active Material ◽  
Lead Acid Batteries ◽  
Lead Acid

Barium sulfate (BaSO4) is a common impurity in recycled lead paste, and the effect of this impurity in positive active materials on the performance of recycled lead acid batteries was investigated.

Reduction of lead dioxide with oxalic acid to prepare lead oxide as the positive electrode material for lead acid batteries

RSC Advances ◽  
2016 ◽  
Vol 6 (110) ◽  
pp. 108513-108522 ◽  
Author(s):  
Wei Liu ◽  
Beibei Ma ◽  
Fajun Li ◽  
Yan Fu ◽  
Jian Tai ◽  
...  
Keyword(s):  
Oxalic Acid ◽  
Electrode Material ◽  
Lead Oxide ◽  
Lead Dioxide ◽  
Positive Electrode ◽  
Lead Acid Batteries ◽  
Positive Electrode Material ◽  
Lead Oxides ◽  
Lead Acid

Sponge-like lead oxides prepared from PbO2can discharge a capacity of 115.2 mA h g−1after 50 cycles at 100 mA g−1.

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