Simultaneous treatment of heat and high pressure homogenization of zein in ethanol–water solution: Physical, structural, thermal and morphological characteristics

2016 ◽  
Vol 34 ◽  
pp. 161-170 ◽  
Author(s):  
Cuixia Sun ◽  
Lei Dai ◽  
Fuguo Liu ◽  
Yanxiang Gao
Keyword(s):  
High Pressure ◽  
Water Solution ◽  
Morphological Characteristics ◽  
High Pressure Homogenization ◽  
Simultaneous Treatment

scholarly journals Synthesis of Nanosilica via Olivine Mineral Carbonation under High Pressure in an Autoclave

Metals ◽  
2019 ◽  
Vol 9 (6) ◽  
pp. 708 ◽  
Author(s):  
Srecko Stopic ◽  
Christian Dertmann ◽  
Ichiro Koiwa ◽  
Dario Kremer ◽  
Hermann Wotruba ◽  
...  
Keyword(s):  
High Pressure ◽  
Ph Value ◽  
Water Solution ◽  
Synthesis Method ◽  
Morphological Characteristics ◽  
Spherical Particles ◽  
Alkaline Solutions ◽  
Spray Pyrolysis Method ◽  
Co2 Absorption ◽  
Silicon Dioxide Nanoparticles

Silicon dioxide nanoparticles, also known as silica nanoparticles or nanosilica, are the basis for a great deal of biomedical and catalytic research due to their stability, low toxicity and ability to be functionalized with a range of molecules and polymers. A novel synthesis route is based on CO2 absorption/sequestration in an autoclave by forsterite (Mg2SiO4), which is part of the mineral group of olivines. Therefore, it is a feasible and safe method to bind carbon dioxide in carbonate compounds such as magnesite forming at the same time as the spherical particles of silica. Indifference to traditional methods of synthesis of nanosilica such as sol gel, ultrasonic spray pyrolysis method and hydrothermal synthesis using some acids and alkaline solutions, this synthesis method takes place in water solution at 175 °C and above 100 bar. Our first experiments have studied the influence of some additives such as sodium bicarbonate, oxalic acid and ascorbic acid, solid/liquid ratio and particle size on the carbonation efficiency, without any consideration of formed silica. This paper focuses on a carbonation mechanism for synthesis of nanosilica under high pressure and high temperature in an autoclave, its morphological characteristics and important parameters for silica precipitation such as pH-value and rotating speed.

scholarly journals Buttermilk as Encapsulating Agent: Effect of Ultra-High-Pressure Homogenization on Chia Oil-in-Water Liquid Emulsion Formulations for Spray Drying

Foods ◽  
2021 ◽  
Vol 10 (5) ◽  
pp. 1059
Author(s):  
Fatemeh Aghababaei ◽  
Mary Cano-Sarabia ◽  
Antonio J. Trujillo ◽  
Joan M. Quevedo ◽  
Victoria Ferragut
Keyword(s):  
High Pressure ◽  
Spray Drying ◽  
Encapsulation Efficiency ◽  
Morphological Characteristics ◽  
High Pressure Homogenization ◽  
Omega 3 ◽  
Potential Measurement ◽  
Ultra High Pressure ◽  
Oil In Water ◽  
Functional Components

Functional foods are highly demanded by consumers. Omega-3 rich oil and commercial buttermilk (BM), as functional components, used in combination to produce emulsions for further drying may facilitate the incorporation to foods. Ultra-high-pressure homogenization (UHPH) has a great potential for technological and nutritional aspects in emulsions production. The present study aimed to examine the potential improvement of UHPH technology in producing buttermilk-stabilized omega-3 rich emulsions (BME) for further drying, compared with conventional homogenization. Oil-in-water emulsions formulated with 10% chia: sunflower oil (50:50); 30% maltodextrin and 4 to 7% buttermilk were obtained by using conventional homogenization at 30 MPa and UHPH at 100 and 200 MPa. Particle size analysis, rheological evaluation, colloidal stability, zeta-potential measurement, and microstructure observations were performed in the BME. Subsequent spray drying of emulsions were made. As preliminary approximation for evaluating differences in the homogenization technology applied, encapsulation efficiency and morphological characteristics of on spray-dried emulsions (SDE) containing 21.3 to 22.7% oil content (dry basis) were selected. This study addresses the improvement in stability of BME treated by UHPH when compared to conventional homogenization and the beneficial consequences in encapsulation efficiency and morphology of SDE.

High-Pressure Homogenization Alters Physicochemical Properties and In Vitro Digestibility of Chinese Yam (Dioscorea Opposita Thunb.) Starch

2018 ◽  
Vol 18 (1) ◽  
pp. 10-15
Author(s):  
Wang Yi-Wei ◽  
He Yong-Zhao ◽  
An Feng-Ping ◽  
Huang Qun ◽  
Zeng Feng ◽  
...  
Keyword(s):  
High Pressure ◽  
Physicochemical Properties ◽  
Starch Content ◽  
In Vitro Digestibility ◽  
High Pressure Homogenization ◽  
Starch Granules ◽  
Cross Polarization ◽  
Chinese Yam ◽  
Crystal Type

In this study, Chinese yam starch-water suspension (8%) were subjected to high-pressure homogenization (HPH) at 100 MPa for increasing cycle numbers, and its effect of on the physicochemical properties of the starch was investigated. Results of the polarizing microscope observations showed that the starch granules were disrupted (i.e. greater breakdown value) after HPH treatment, followed by a decrease in cross polarization. After three HPH cycles, the crystallinity of starch decreased, while the crystal type remained unaltered. Meanwhile, the contents of rapidly digestible starch and slowly digestible starch were increased. On the contrary, resistant starch content was decreased. Our results indicate that HPH treatment resulted in reduction of starch crystallinity and increase of starch digestibility.

scholarly journals Cavitation patterns in high-pressure homogenization nozzles with cylindrical orifices: Influence of mixing stream in Simultaneous Homogenization and Mixing

2021 ◽  
Author(s):  
V. Gall ◽  
E. Rütten ◽  
H. P. Karbstein
Keyword(s):  
High Pressure ◽  
Process Design ◽  
High Speed ◽  
State Of The Art ◽  
Back Pressure ◽  
High Pressure Homogenization ◽  
Unit Operation ◽  
Mixing Chamber ◽  
Cavitation Intensity ◽  
Droplet Sizes

AbstractHigh-pressure homogenization is the state of the art to produce high-quality emulsions with droplet sizes in the submicron range. In simultaneous homogenization and mixing (SHM), an additional mixing stream is inserted into a modified homogenization nozzle in order to create synergies between the unit operation homogenization and mixing. In this work, the influence of the mixing stream on cavitation patterns after a cylindrical orifice is investigated. Shadow-graphic images of the cavitation patterns were taken using a high-speed camera and an optically accessible mixing chamber. Results show that adding the mixing stream can contribute to coalescence of cavitation bubbles. Choked cavitation was observed at higher cavitation numbers σ with increasing mixing stream. The influence of the mixing stream became more significant at a higher orifice to outlet ratio, where a hydraulic flip was also observed at higher σ. The decrease of cavitation intensity with increasing back-pressure was found to be identical with conventional high-pressure homogenization. In the future, the results can be taken into account in the SHM process design to improve the efficiency of droplet break-up by preventing cavitation or at least hydraulic flip.

Impact of high-pressure homogenization on the microstructure and rheological properties of citrus fiber

2020 ◽  
Vol 0 (0) ◽  
Author(s):  
Dianbin Su ◽  
Xin-Di Zhu ◽  
Yong Wang ◽  
Dong Li ◽  
Li-Jun Wang
Keyword(s):  
Particle Size ◽  
High Pressure ◽  
Rheological Properties ◽  
Binding Capacity ◽  
Loss Modulus ◽  
High Pressure Homogenization ◽  
Carreau Model ◽  
Hydration Properties ◽  
Water Binding ◽  
Water Holding

Abstract Citrus fiber dispersion with different concentrations (5–25 g/kg) was treated by high-pressure homogenization (90 and 160 MPa) for two cycles. The particle size distribution, hydration properties of powders, morphology and rheological measurements were carried out to study the microstructure and rheological properties changes by high-pressure homogenization (HPH). In conclusion, the HPH can reduce the particle size of fiber, improve the water holding capacity and water binding capacity. Furthermore, fiber shape can be modified from globular cluster to flake-like slices, and tiny pores can be formed on the surface of citrus fiber. The apparent viscosity, storage modulus and loss modulus were increased by HPH whereas the activation energy was reduced. The Hershcel–Bulkley model, Carreau model and Power Law mode were selected to evaluate the rheological properties.

Enzymatic Hydrolysis Combined with Mechanical Shearing and High-Pressure Homogenization for Nanoscale Cellulose Fibrils and Strong Gels

2007 ◽  
Vol 8 (6) ◽  
pp. 1934-1941 ◽  
Author(s):  
M. Pääkkö ◽  
M. Ankerfors ◽  
H. Kosonen ◽  
A. Nykänen ◽  
S. Ahola ◽  
...  
Keyword(s):  
High Pressure ◽  
Enzymatic Hydrolysis ◽  
High Pressure Homogenization ◽  
Cellulose Fibrils ◽  
Mechanical Shearing
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