Three-dimensional observation of carbonaceous chondrites by synchrotron radiation X-ray CT – Quantitative analysis and developments for the future sample return missions

2013 ◽  
Vol 116 ◽  
pp. 17-32 ◽  
Author(s):  
M. Uesugi ◽  
K. Uesugi ◽  
A. Takeuchi ◽  
Y. Suzuki ◽  
M. Hoshino ◽  
...  
Keyword(s):  
Quantitative Analysis ◽  
Synchrotron Radiation ◽  
Three Dimensional ◽  
Carbonaceous Chondrites ◽  
Sample Return ◽  
X Ray ◽  
The Future ◽  
Future Sample

Three-dimensional quantitative analysis of polymer foams from synchrotron radiation x-ray microtomography

2003 ◽  
Vol 36 (10A) ◽  
pp. A37-A43 ◽  
Author(s):  
A Elmoutaouakkil ◽  
G Fuchs ◽  
P Bergounhon ◽  
R P res ◽  
F Peyrin
Keyword(s):  
Quantitative Analysis ◽  
Synchrotron Radiation ◽  
Three Dimensional ◽  
Polymer Foams ◽  
X Ray

scholarly journals Synchrotron radiation X-ray tomographic microscopy (SRXTM) of brachiopod shell interiors for taxonomy: Preliminary report

2010 ◽  
pp. 109-117 ◽  
Author(s):  
Neda Motchurova-Dekova ◽  
David Harper
Keyword(s):  
Synchrotron Radiation ◽  
Three Dimensional ◽  
X Rays ◽  
X Ray ◽  
Fine Grained ◽  
Internal Structures ◽  
Efficient Alternative ◽  
Micro Tomography ◽  
Light Beams ◽  
Non Destructive

Synchrotron radiation X-ray tomographic microscopy (SRXTM) is a non-destructive technique for the investigation and visualization of the internal features of solid opaque objects, which allows reconstruction of a complete three-dimensional image of internal structures by recording of the differences in the effects on the passage of waves of energy reacting with those structures. Contrary to X-rays, produced in a conventional X-ray tube, the intense synchrotron light beams are sharply focused like a laser beam. We report encouraging results from the use of SRXTM for purely taxonomic purposes in brachiopods: an attempt to find a non-destructive and more efficient alternative to serial sectioning and several other methods of dissection together with the non-destructive method of X-ray computerised micro-tomography. Two brachiopod samples were investigated using SRXTM. In ?Rhynchonella? flustracea it was possible to visualise the 3D shape of the crura and dental plates. In Terebratulina imbricata it was possible to reveal the form of the brachidium. It is encouraging that we have obtained such promising results using SRXTM with our very first two fortuitous samples, which had respectively fine-grained limestone and marl as infilling sediment, in contrast to the discouraging results communicated to us by some colleagues who have tested specimens with such infillings using X-ray micro-tomography. In future the holotypes, rare museum specimens or delicate Recent material may be preferentially subjected to this mode of analysis.

scholarly journals Development of an X-ray real-time stereo imaging technique using synchrotron radiation

2011 ◽  
Vol 18 (4) ◽  
pp. 569-574 ◽  
Author(s):  
Masato Hoshino ◽  
Kentaro Uesugi ◽  
James Pearson ◽  
Takashi Sonobe ◽  
Mikiyasu Shirai ◽  
...  
Keyword(s):  
Synchrotron Radiation ◽  
Real Time ◽  
Imaging System ◽  
Silicon Crystal ◽  
Three Dimensional ◽  
Stereo Image ◽  
Large Field ◽  
Depth Information ◽  
Stereo Imaging ◽  
X Ray

An X-ray stereo imaging system with synchrotron radiation was developed at BL20B2, SPring-8. A portion of a wide X-ray beam was Bragg-reflected by a silicon crystal to produce an X-ray beam which intersects with the direct X-ray beam. Samples were placed at the intersection point of the two beam paths. X-ray stereo images were recorded simultaneously by a detector with a large field of view placed close to the sample. A three-dimensional wire-frame model of a sample was created from the depth information that was obtained from the lateral positions in the stereo image. X-ray stereo angiography of a mouse femoral region was performed as a demonstration of real-time stereo imaging. Three-dimensional arrangements of the femur and blood vessels were obtained.

Nondestructive Observation of Thermal Fatigue Crack Propagation in FBGA and Die Attached Solder Joints by Synchrotron Radiation X-Ray Laminography

2015 ◽  
Author(s):  
Hiroyuki Tsuritani ◽  
Toshihiko Sayama ◽  
Yoshiyuki Okamoto ◽  
Takeshi Takayanagi ◽  
Masato Hoshino ◽  
...  
Keyword(s):  
Fatigue Crack ◽  
Synchrotron Radiation ◽  
Crack Propagation ◽  
Thermal Fatigue ◽  
Solder Joints ◽  
Fatigue Cracks ◽  
Three Dimensional ◽  
X Ray ◽  
Micro Cracks ◽  
Solder Bumps

The reliability of solder joints on printed circuit boards (PCBs) is significantly affected by thermal fatigue processes due to downsizing and high density packaging in electronic components. Accordingly, there is a strong desire in related industries for development of a new nondestructive inspection technology to detect fatigue cracks appearing in these joints. The authors have applied the SP-μCT, a synchrotron radiation X-ray microtomography system, to the nondestructive observation of such cracks. However, for planar objects such as PCB substrates, reconstruction of CT images is difficult due to insufficient X-ray transmission along the parallel axis of the substrate. In order to solve this problem, a synchrotron radiation X-ray laminography system was developed to overcome the size limits of such specimens. In this work, this system was applied to the three-dimensional, nondestructive observation of thermal fatigue cracks in solder joints, for which X-ray CT inspection has been extremely difficult. The observed specimens included two typical joint structures formed using Sn-3.0Ag-0.5Cu solder: (1) a fine pitch ball grid array (FBGA) joint specimen in which an LSI package is connected to a substrate by solder bumps 360 μm in diameter, and (2) a die-attached specimen in which a 3 mm square ceramic chip is mounted on a substrate. The optical system developed for use in X-ray laminography was constructed to provide a rotation axis with a 30° tilt from the right angle to the X-ray beam, and to obtain X-ray projection images via the beam monitor. The same solder joints were observed successively using the laminography system at beamline BL20XU at SPring-8, the largest synchrotron radiation facility in Japan. In the FBGA type specimen, fatigue cracks were clearly observed to appear at the periphery of the joint interface, and to propagate gradually to the inner regions of the solder bumps as thermal cycling proceeded. In contrast, in the die-attached joint specimen, micro-cracks were observed to appear and propagate through the thin solder layer. An important observation was that these micro-cracks become interconnected prior to propagation of the main fatigue crack. The fatigue crack propagation lifetime was also estimated in both specimens by measuring the crack surface area and calculating the average crack propagation rate through the three-dimensional images. Consequently, the sectional images obtained by the laminography system clearly show the process of crack propagation due to thermal cyclic loading.

scholarly journals Three-dimensional visualization of fossil flowers, fruits, seeds, and other plant remains using synchrotron radiation X-ray tomographic microscopy (SRXTM): new insights into Cretaceous plant diversity

2014 ◽  
Vol 88 (4) ◽  
pp. 684-701 ◽  
Author(s):  
Else Marie Friis ◽  
Federica Marone ◽  
Kaj Raunsgaard Pedersen ◽  
Peter R. Crane ◽  
Marco Stampanoni
Keyword(s):  
Synchrotron Radiation ◽  
Three Dimensional ◽  
Three Dimensions ◽  
Fossil Plants ◽  
Post Processing ◽  
Thin Sections ◽  
X Ray ◽  
Rapid Acquisition ◽  
Fossil Material ◽  
Plant Fossil

The application of synchrotron radiation X-ray tomographic microscopy (SRXTM) to the study of mesofossils of Cretaceous age has created new possibilities for the three-dimensional visualization and analysis of the external and internal structure of critical plant fossil material. SRXTM provides cellular and subcellular resolution of comparable or higher quality to that obtained from permineralized material using thin sections or the peel technique. SRXTM also has the advantage of being non-destructive and results in the rapid acquisition of large quantities of data in digital form. SRXTM thus refocuses the effort of the investigator from physical preparation to the digital post-processing of X-ray tomographic data, which allows great flexibility in the reconstruction, visualization, and analysis of the internal and external structure of fossil material in multiple planes and in two or three dimensions. A review of recent applications in paleobotany demonstrates that SRXTM will dramatically expand the level of information available for diverse fossil plants. Future refinement of SRXTM approaches that further increases resolution and eases digital post-processing, will transform the study of mesofossils and create new possibilities for advancing paleobotanical knowledge. We illustrate these points using a variety of Cretaceous mesofossils, highlighting in particular those cases where SRXTM has been essential for resolving critical structural details that have enhanced systematic understanding and improved phylogenetic interpretations.

scholarly journals Three-dimensional diffusion of non-sorbing species in porous sandstone: computer simulation based on X-ray microtomography using synchrotron radiation

2004 ◽  
Vol 74 (1-4) ◽  
pp. 253-264 ◽  
Author(s):  
Yoshito Nakashima ◽  
Tsukasa Nakano ◽  
Koichi Nakamura ◽  
Kentaro Uesugi ◽  
Akira Tsuchiyama ◽  
...  
Keyword(s):  
Computer Simulation ◽  
Synchrotron Radiation ◽  
Three Dimensional ◽  
X Ray ◽  
Dimensional Diffusion ◽  
Porous Sandstone ◽  
Simulation Based

Absorption correction procedures for quantitative analysis of fluid inclusions using synchrotron radiation X-ray fluorescence

1998 ◽  
Vol 144 (1-2) ◽  
pp. 121-136 ◽  
Author(s):  
P Philippot ◽  
B Menez ◽  
P Chevallier ◽  
F Gibert ◽  
F Legrand ◽  
...  
Keyword(s):  
Quantitative Analysis ◽  
Synchrotron Radiation ◽  
Fluid Inclusions ◽  
X Ray ◽  
Absorption Correction
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