Facile one-pot synthesis of hollow NiCoP nanospheres via thermal decomposition technique and its free-standing carbon composite for supercapacitor application

2019 ◽  
Vol 25 ◽  
pp. 100893 ◽  
Author(s):  
Arthi Gopalakrishnan ◽  
Dan Yang ◽  
Joshua Charles Ince ◽  
Yen Bach Truong ◽  
Aimin Yu ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Carbon Composite ◽  
Decomposition Technique ◽  
Free Standing ◽  
One Pot ◽  
Supercapacitor Application ◽  
One Pot Synthesis

Facile One‐Pot Synthesis of Magnetic Targeted Polymers for Drug Delivery and Study on Thermal Decomposition Kinetics

2021 ◽  
Vol 6 (6) ◽  
pp. 1191-1198
Author(s):  
Zhen Shi ◽  
Yazhen Wang ◽  
Yu Sun ◽  
Xueying Wu ◽  
Tianyuan Xiao ◽  
...  
Keyword(s):  
Drug Delivery ◽  
Thermal Decomposition ◽  
Decomposition Kinetics ◽  
Thermal Decomposition Kinetics ◽  
One Pot ◽  
One Pot Synthesis

Cu/Fe3O4@carboxylate-rich carbon composite: One-pot synthesis, characterization, adsorption and photo-Fenton catalytic activities

2020 ◽  
Vol 129 ◽  
pp. 110913 ◽  
Author(s):  
Van Thuan Le ◽  
Van Dat Doan ◽  
Vy Anh Tran ◽  
Hoang Sinh Le ◽  
Dai Lam Tran ◽  
...  
Keyword(s):  
Carbon Composite ◽  
One Pot ◽  
Catalytic Activities ◽  
One Pot Synthesis

One-pot synthesis of β-acetamido-β-(phenyl) propiophenone using ZnO/Carbon Nanocomposites

2020 ◽  
Vol 23 ◽  
Author(s):  
Thangavelu Krithiga ◽  
Sunitha Salla ◽  
Jayabalan Karthikeyan ◽  
Jagadeesan Aravind Kumar
Keyword(s):  
Catalytic Activity ◽  
Carbon Source ◽  
Zno Nanoparticles ◽  
Acetyl Chloride ◽  
Combustion Method ◽  
Carbon Composite ◽  
Zinc Nitrate ◽  
Carbon Composites ◽  
One Pot ◽  
One Pot Synthesis

Aim and Objectives: The focus of the present work is to synthesize ZnO/C composite using dextrose as carbon source by combustion method and study the comparative evaluation on one-pot synthesis of β-acetamido- β-(phenyl) propiophenone over ZnO nanoparticles and ZnO/C composite catalyst. Materials and Methods: The ZnO nanoparticles has been synthesized by sol-gel method using zinc nitrate and NaOH and ZnO/Carbon composites by combustion method using zinc nitrate and dextrose as carbon source. The resulting gel was placed in a preheated muffle furnace at 400o C. The solution boils and ignites with a flame. On cooling highly amorphous powder of ZnO/Carbon composite is obtained. Results: The XRD patterns reveal the hexagonal phase with Wurtzite structure and the nanocrystalline nature of the catalysts. The SEM image of ZnO/C composite showed that it contains spherical particles with an average size of 41 nm. The average particle size of the composite was around 60nm by DLS method. The catalytic activity of the ZnO/Carbon composites has been analyzed by one-pot four-component condensation of benzaldehyde, acetophenone, acetyl chloride and acetonitrile. The feed molar ratio of 1:1 (Bz:AP) and catalyst loading of 30 mol% is found to be the optimal condition for βacetamido ketone conversion over ZnO/carbon composite. Conclusion: The substantial catalytic activity of the synthesized ZnO/C composite materials was tested by one-pot fourcomponent condensation of benzaldehyde (Bz), acetophenone (AP), acetyl chloride (AC) and acetonitrile (AN) which showed a high β-acetamido ketone conversion under the optimized reaction conditions. It has also been found that the catalyst is very stable and reusable.

scholarly journals One-Pot Synthesis of P(O)-N Containing Compounds Using N-Chlorosuccinimide and Their Influence in Thermal Decomposition of PU Foams

Polymers ◽  
2018 ◽  
Vol 10 (7) ◽  
pp. 740 ◽  
Author(s):  
Khalifah Salmeia ◽  
Florence Flaig ◽  
Daniel Rentsch ◽  
Sabyasachi Gaan
Keyword(s):  
Thermal Decomposition ◽  
One Pot ◽  
One Pot Synthesis ◽  
Pu Foams
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