Template free and facile microwave-assisted synthesis method to prepare mesoporous copper sulfide nanosheets for high-performance hybrid supercapacitor

2019 ◽  
Vol 319 ◽  
pp. 49-60 ◽  
Author(s):  
Muhammad Naveed ◽  
Waqar Younas ◽  
Youqi Zhu ◽  
Souleymen Rafai ◽  
Quanqing Zhao ◽  
...  
Keyword(s):  
Copper Sulfide ◽  
High Performance ◽  
Synthesis Method ◽  
Microwave Assisted Synthesis ◽  
Hybrid Supercapacitor ◽  
Microwave Assisted ◽  
Template Free

Assessment of Magnetic Properties between Fe and Ni Doped ZnO Nanoparticles Synthesized by Microwave Assisted Synthesis Method

2021 ◽  
Vol 317 ◽  
pp. 119-124
Author(s):  
Sabiu Said Abdullahi ◽  
Garba Shehu Musa Galadanci ◽  
Norlaily Mohd Saiden ◽  
Josephine Ying Chyi Liew
Keyword(s):  
Magnetic Properties ◽  
Zno Nanoparticles ◽  
Room Temperature ◽  
Synthesis Method ◽  
Dilute Magnetic Semiconductors ◽  
High Coercivity ◽  
Microwave Assisted Synthesis ◽  
Ferromagnetic Behavior ◽  
Microwave Assisted ◽  
Doped Zno

The emergence of Dilute Magnetic Semiconductors (DMS) with a potentials for spintronic application have attracted much researches attention, special consideration has been given to ZnO semiconductor material due to its wide band gap of 3.37 eV, large exciting binding energy of 60 meV, moreover, its ferromagnetic behavior at room temperature when doped with transition metals. MxZn1-xO (M = Fe or Ni) nanoparticles were synthesized by microwave assisted synthesis method calcined at 600°C. The structural, morphological and magnetic properties of these nanoparticles were studied using X-ray Diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM) and Vibrating Sample Magnetometer (VSM) respectively. Single phase Wurtzite hexagonal crystal structure was observed for the undoped and Fe doped ZnO nanoparticles with no any impurity, whereas Ni doped ZnO nanoparticles shows the formation of NiO impurities. The magnetic measurement reveals a diamagnetic behavior for the undoped ZnO meanwhile a clear room temperature ferromagnetism was observed for both Fe and Ni doped ZnO. Fe doped ZnO present a high saturation magnetization compared to Ni doped ZnO. However, Ni doped ZnO present high coercivity. The research was confirmed that Fe doped ZnO material will be good material combination for spintronic applications.

Rapid microwave-assisted synthesis of high-rate FeS2 nanoparticles anchored on graphene for hybrid supercapacitors with ultrahigh energy density

2018 ◽  
Vol 6 (30) ◽  
pp. 14956-14966 ◽  
Author(s):  
Zhiqin Sun ◽  
Huiming Lin ◽  
Feng Zhang ◽  
Xue Yang ◽  
He Jiang ◽  
...  
Keyword(s):  
Solid State ◽  
Energy Density ◽  
Specific Capacity ◽  
High Rate ◽  
Microwave Assisted Synthesis ◽  
Ultrahigh Energy ◽  
Hybrid Supercapacitor ◽  
High Specific Capacity ◽  
Hybrid Supercapacitors ◽  
Microwave Assisted

Benefitting from the high specific capacity (793 C g−1) of the FeS2/graphene anode, an assembled all-solid-state hybrid supercapacitor device based on the FeS2/graphene anode and a Ni(OH)2@Co9S8 cathode achieves an ultrahigh energy density of up to 95.8 W h kg−1 at a power density of 949 W kg−1.

scholarly journals Microwave-assisted synthesis of high thermal stability and colourless polyimides containing pyridine

2019 ◽  
Vol 6 (6) ◽  
pp. 190196 ◽  
Author(s):  
Kai Cheng ◽  
Jie-pin Hu ◽  
Yan-cheng Wu ◽  
Chu-qi Shi ◽  
Zhi-geng Chen ◽  
...  
Keyword(s):  
Thermal Stability ◽  
Synthesis Method ◽  
Optical Transmittance ◽  
Aromatic Diamine ◽  
Microwave Assisted Synthesis ◽  
Step Method ◽  
Light Emitting ◽  
Microwave Assisted ◽  
One Step ◽  
Biphenyltetracarboxylic Dianhydride

A novel aromatic diamine containing pyridyl side group, 4-pyridine-4,4-bis(3,5-dimethyl-5-aminophenyl)methane (PyDPM), was successfully synthesized via electrophilic substitution reaction. The polyimides (PIs) containing pyridine were obtained via the microwave-assisted one-step polycondensation of the PyDPM with pyromellitic dianhydride (PMDA), 3,3′,4,4′-biphenyltetracarboxylic dianhydride (BPDA), 3,3′,4,4′-diphenylether tetracarboxylic dianhydride (ODPA) and 4,4′-(hexafluoroisopropylidene)diphthalic anhydride (6FDA). Contrarily to the reported similar PIs, these PIs exhibit much higher thermal stability or heat resistance, i.e. high glass transition temperatures ( T g s) in the range of 358–473°C, and the decomposition temperatures at 5% weight loss over 476°C under nitrogen. They can afford flexible and strong films with tensile strength of 82.1–93.3 MPa, elongation at break of 3.7%–15.2%, and Young's modulus of 3.3–3.8 GPa. Furthermore, The PI films exhibit good optical transparency with the cut-off wavelength at 313–366 nm and transmittance higher than 73% at 450 nm. The excellent thermal and optical transmittance can be attributed to synthesis method and the introduction of pyridine rings and ortho-methyl groups. The inherent viscosities of PIs via one-step method were found to be 0.58–1.12 dl g −1 in DMAc, much higher than those via two-step method. These results indicate these PIs could be potential candidates for optical substrates of organic light emitting diodes (OLEDs).

Citrate complexation microwave-assisted synthesis of Ce0.8Zr0.2O2 nanocatalyst over Al2O3 used in CO oxidation for hydrogen purification: influence of composite loading and synthesis method

RSC Advances ◽  
2016 ◽  
Vol 6 (40) ◽  
pp. 34055-34065 ◽  
Author(s):  
Leila Rezaee ◽  
Mohammad Haghighi
Keyword(s):  
Co Oxidation ◽  
Synthesis Method ◽  
Composite Catalyst ◽  
Microwave Assisted Synthesis ◽  
Hydrogen Purification ◽  
Microwave Assisted ◽  
Microwave Combustion

Nanostructured Ce0.8Zr0.2O2/Al2O3 composite catalyst was synthesized by modified citrate complexation method. Utilizing microwave combustion endowed the sample with more uniform and homogenous pattern leading to better CO oxidation.

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