Observation of Dynamic Interfacial Layers in Li-Ion and Li-O2 Batteries by Scanning Electrochemical Microscopy

2016 ◽  
Vol 199 ◽  
pp. 366-379 ◽  
Author(s):  
Heinz Bülter ◽  
Patrick Schwager ◽  
Daniela Fenske ◽  
Gunther Wittstock
2015 ◽  
Vol 17 (43) ◽  
pp. 28441-28450 ◽  
Author(s):  
E. Ventosa ◽  
W. Schuhmann

Scanning electrochemical microscopy has demonstrated to be a powerful analytical tool for the investigation of various processes in Li-ion batteries.


2016 ◽  
Vol 52 (41) ◽  
pp. 6825-6828 ◽  
Author(s):  
E. Ventosa ◽  
P. Wilde ◽  
A.-H. Zinn ◽  
M. Trautmann ◽  
A. Ludwig ◽  
...  

In operando SECM is employed to monitor the evolution of the electrically insulating character of a Si electrode surface during (de-)lithiation.


Sensors ◽  
2021 ◽  
Vol 21 (4) ◽  
pp. 1132 ◽  
Author(s):  
Rejane M. P. da Silva ◽  
Javier Izquierdo ◽  
Mariana X. Milagre ◽  
Abenchara M. Betancor-Abreu ◽  
Isolda Costa ◽  
...  

Amperometric and potentiometric probes were employed for the detection and characterization of reactive sites on the 2098-T351 Al-alloy (AA2098-T351) using scanning electrochemical microscopy (SECM). Firstly, the probe of concept was performed on a model Mg-Al galvanic pair system using SECM in the amperometric and potentiometric operation modes, in order to address the responsiveness of the probes for the characterization of this galvanic pair system. Next, these sensing probes were employed to characterize the 2098-T351 alloy surface immersed in a saline aqueous solution at ambient temperature. The distribution of reactive sites and the local pH changes associated with severe localized corrosion (SLC) on the alloy surface were imaged and subsequently studied. Higher hydrogen evolution, lower oxygen depletion and acidification occurred at the SLC sites developed on the 2098-T351 Al-alloy.


Nanoscale ◽  
2021 ◽  
Author(s):  
Katarina A. Novčić ◽  
Christian Iffelsberger ◽  
Siowwoon Ng ◽  
Martin Pumera

MoS2 and WS2 and their heterojunctions are used to modify thermally activated 3D-printed nanocarbon structures. Herein, the local electrochemical performance for HER of the modified structures is demonstrated by scanning electrochemical microscopy.


Author(s):  
Dylan T. Jantz ◽  
Ryan J. Balla ◽  
Siao-Han Huang ◽  
Niraja Kurapati ◽  
Shigeru Amemiya ◽  
...  

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