Preparation and electrochemical characterization of palladium single crystal electrodes in 0.1M H2SO4 and HClO4

2007 ◽  
Vol 52 (18) ◽  
pp. 5733-5748 ◽  
Author(s):  
M. Hara ◽  
U. Linke ◽  
Th. Wandlowski
Keyword(s):  
Single Crystal ◽  
Electrochemical Characterization

Preparation and Electrochemical Characterization of LiCoO2 Single Crystal Particles prepared by Super Critical Water Synthesis (SCWS)

1999 ◽  
Vol 575 ◽  
Author(s):  
Kiyoshi Kanamura ◽  
Takao Umegaki ◽  
Katsunori Toyoshima ◽  
Ken-ichi Okada ◽  
Yukiya Hakuta ◽  
...  
Keyword(s):  
Particle Size ◽  
Single Crystal ◽  
Discharge Capacity ◽  
Standard Method ◽  
Electrochemical Characterization ◽  
Electrochemical Methods ◽  
Structural Defects ◽  
Amorphous Phases ◽  
Preparation Conditions

ABSTRACTLiCoO2 single crystal particles were obtained by super critical water synthesis (SCWS) under optimized preparation conditions. The particle size of the LiCoO2 was less than 1 μm, which was much smaller than that of LiCoO2 prepared by a standard method. However, some unknown crystalline and amorphous phases coexisted with the well defined LiCoO2 single crystal particles. The discharge and charge characteristics of the LiCoO2 prepared by the SCWS were examined by some electrochemical methods. In the first cycle, an irreversible behavior was observed, and then the gradual decrease of the discharge capacity with discharge and charge cycle was also detected. The stable discharge capacity was estimated to be 80 mA h g−1 after the 100th cycle. This result may be due to the existence of amorphous phases and some structural defects.

Electrochemical characterization of a 1,8-octanedithiol self-assembled monolayer (ODT-SAM) on a Au(111) single crystal electrode

2008 ◽  
Vol 53 (27) ◽  
pp. 8026-8033 ◽  
Author(s):  
Daniel García-Raya ◽  
Rafael Madueño ◽  
José Manuel Sevilla ◽  
Manuel Blázquez ◽  
Teresa Pineda
Keyword(s):  
Single Crystal ◽  
Electrochemical Characterization ◽  
Self Assembled Monolayer ◽  
Self Assembled ◽  
Single Crystal Electrode

Electrochemical Characterization of the Alkaneselenol-Based SAMs on Au(111) Single Crystal Electrode

Langmuir ◽  
2002 ◽  
Vol 18 (24) ◽  
pp. 9342-9349 ◽  
Author(s):  
Lesia V. Protsailo ◽  
W. Ronald Fawcett ◽  
Dale Russell ◽  
Ryan L. Meyer
Keyword(s):  
Single Crystal ◽  
Electrochemical Characterization ◽  
Single Crystal Electrode

Preparation and electrochemical characterization of low-index rhodium single crystal electrodes in sulfuric acid

2009 ◽  
Vol 54 (23) ◽  
pp. 5509-5521 ◽  
Author(s):  
Qinqin Xu ◽  
Udo Linke ◽  
Renata Bujak ◽  
Thomas Wandlowski
Keyword(s):  
Sulfuric Acid ◽  
Single Crystal ◽  
Electrochemical Characterization

Spectral Investigation on the Growth and Characterization of NLO Crystals of Thiourea Succinic Acid Single Crystal.

2015 ◽  
Vol 2 (2) ◽  
pp. 70-73
Author(s):  
Kannan.P ◽  
Thambidurai.S ◽  
Suresh.N
Keyword(s):  
Single Crystal ◽  
Succinic Acid ◽  
Slow Evaporation Technique ◽  
Absorption Studies ◽  
Dta Analysis ◽  
Evaporation Technique ◽  
Ft Ir ◽  
Ir Spectroscopic ◽  
Thermal Stability Of

Growth of optically transparent single crystals of thiourea succinic acid (TUSA) was grown successfully from aqueous solution by slow evaporation technique. The crystal structure was elucidated using the single crystal XRD. The various functional groups and the modes of vibrations were identified by FT-IR spectroscopic analysis. The optical absorption studies indicate that the optical transparency window is quite wide making its suitable for NLO applications. Thermal stability of the crown crystal carried out by TGA-DTA analysis.

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