Self-assembled mesoporous manganese oxide with high surface area by ambient temperature synthesis and its enhanced electrochemical properties

2011 ◽  
Vol 13 (7) ◽  
pp. 730-733 ◽  
Author(s):  
Vinod Mathew ◽  
Jinsub Lim ◽  
Jungwon Kang ◽  
Jihyeon Gim ◽  
Alok Kumar Rai ◽  
...  
Nanomaterials ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 1328 ◽  
Author(s):  
Marlon Danny Jerez-Masaquiza ◽  
Lenys Fernández ◽  
Gema González ◽  
Marjorie Montero-Jiménez ◽  
Patricio J. Espinoza-Montero

In this work, a new hydrogen peroxide (H2O2) electrochemical sensor was fabricated. Prussian blue (PB) was electrodeposited on a glassy carbon (GC) electrode modified with zirconia doped functionalized carbon nanotubes (ZrO2-fCNTs), (PB/ZrO2-fCNTs/GC). The morphology and structure of the nanostructured system were characterized by scanning and transmission electron microscopy (TEM), atomic force microscopy (AFM), specific surface area, X-ray diffraction (XRD), thermogravimetric analysis (TGA), Raman and Fourier transform infrared (FTIR) spectroscopy. The electrochemical properties were studied by cyclic voltammetry (CV) and chronoamperometry (CA). Zirconia nanocrystallites (6.6 ± 1.8 nm) with cubic crystal structure were directly synthesized on the fCNTs walls, obtaining a well dispersed distribution with a high surface area. The experimental results indicate that the ZrO2-fCNTs nanostructured system exhibits good electrochemical properties and could be tunable by enhancing the modification conditions and method of synthesis. The fabricated sensor could be used to efficiently detect H2O2, presenting a good linear relationship between the H2O2 concentration and the peak current, with quantification limit (LQ) of the 10.91 μmol·L−1 and detection limit (LD) of 3.5913 μmol·L−1.


2015 ◽  
Vol 39 (12) ◽  
pp. 9124-9131 ◽  
Author(s):  
Savita Patil ◽  
Shrikant Raut ◽  
Ratnakar Gore ◽  
Babasaheb Sankapal

Room-temperature synthesis of Cd(OH)2 thin film consisting of high-surface-area nanowires. Device-grade development as a symmetric supercapacitor.


Nanoscale ◽  
2021 ◽  
Author(s):  
Usama Zulfiqar ◽  
Nikolaos Kostoglou ◽  
Andrew Thomas ◽  
Claus Rebholz ◽  
Allan Matthews ◽  
...  

This paper reports a study involving the formation of a self-assembled polymeric monolayer on the surface of a high surface area activated carbon to engineer its affinity towards organic contaminants....


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