Short- and long-term dynamic accuracies determination of satellite-based positioning devices using a specially designed testing facility

2011 ◽  
Vol 76 (2) ◽  
pp. 297-305 ◽  
Author(s):  
M. Gavric ◽  
M. Martinov ◽  
S. Bojic ◽  
Dj. Djatkov ◽  
M. Pavlovic
Keyword(s):  
Testing Facility ◽  
Short And Long Term ◽  
Positioning Devices

scholarly journals Quantitative Determination of Vinpocetine in Dietary Supplements

2016 ◽  
Vol 11 (5) ◽  
pp. 1934578X1601100
Author(s):  
John M. T. French ◽  
Matthew D. King ◽  
Owen M. McDougal
Keyword(s):  
United States ◽  
Quantitative Determination ◽  
Dietary Supplements ◽  
Nootropic Drugs ◽  
Regulatory Policies ◽  
Short And Long Term ◽  
Pharmacologically Active ◽  
Active Substances

Current United States regulatory policies allow for the addition of pharmacologically active substances in dietary supplements if derived from a botanical source. The inclusion of certain nootropic drugs, such as vinpocetine, in dietary supplements has recently come under scrutiny due to the lack of defined dosage parameters and yet unproven short- and long-term benefits and risks to human health. This study quantified the concentration of vinpocetine in several commercially available dietary supplements and found that a highly variable range of 0.6–5.1 mg/serving was present across the tested products, with most products providing no specification of vinpocetine concentrations.

scholarly journals Determination of polyadenylate-rich ribonucleic acid in the nucleus and in the cytoplasm of plasmacytoma cells

1975 ◽  
Vol 149 (3) ◽  
pp. 669-674 ◽  
Author(s):  
K A Abraham ◽  
T S Eikhom
Keyword(s):  
Ph Dependence ◽  
Specific Radioactivity ◽  
Nuclear Fraction ◽  
High Concentration ◽  
Millipore Filter ◽  
Filter Technique ◽  
Short And Long Term ◽  
Millipore Filters

A number of parameters affecting the adsorption of rRNA and poly(A)-containing RNA to Millipore filters were investigated separately. Binding of both types of RNA to the filter was dependent on the concentration of RNA, pH and Mg2+ concentration of the reaction mixture. Both types of RNA bound to the filter optimally at slightly acid pH values. The binding of poly(A)-containing RNA to the filter exhibited a broad pH-dependence compared with that of rRNA. The ratio of poly(A)-rich RNA/rRNA retained by the filter was maximal between pH7 and 8. The presence of 1 mM-EDTA or a high concentration of NaCl (over 0.5M) decreased the affinity of RNA for the filter. The amount of poly(A)-containing RNA in the nucleus and in the cytoplasm of a plasmacytoma cell line (MPC-11) labelled with [32P]Pi was determined by the Millipore-filter technique under conditions that minimized contamination by rRNA. These data were compared with the estimations made by oligo(dT)-cellulose chromatography. The results obtained by these two methods were in good agreement for RNA labelled for short periods (up to 2h). In long labelling and pulse-chase experiments, however, contamination of the filter by rRNA of increasing specific radioactivity in the cytoplasm gave an erroneous value for poly(A)-containing RNA by the Millipore-filter technique. Determinations made on the nuclear fraction by these two methods did not show significant variation in short- and long-term labelling experiments.

The Evaluation of the PXQ for the Analysis of Cements and Related Materials

1958 ◽  
Vol 2 ◽  
pp. 215-227
Author(s):  
George Andermann ◽  
J. L. Jones ◽  
E. Davidson
Keyword(s):  
Flow Rate ◽  
Gas Flow ◽  
Applied Research ◽  
Production Control ◽  
Helium Flow ◽  
X Ray ◽  
Long Term Stability ◽  
Short And Long Term

AbstractThe analysis of cements and ores has been studied using the Applied Research Laboratories, Inc. Production Control X-ray Quantometer (PXQ), Elements included in the program were magnesium, aluminum, silicon, phosphorus, calcium and iron. The PXQ, utilizing the polychromator concept, allows the simultaneous determination of the listed elements.Focusing ADP, EDT, quartz and LiF crystals were used with flow Geigers or Multitrons. Helium paths were used as required. The choice of crystals, detectors, and slit widths was determined to give optimum results for each element.The effects of briquetting and ratioing to scattered background on accuracy were studied. Various instrumental factors such as helium flow rate, detector gas flow rate, short and long term stability were also investigated.

Determination of native (wood derived) formaldehyde by the desiccator method in particleboards generated during panel production

Holzforschung ◽  
2010 ◽  
Vol 64 (4) ◽  
Author(s):  
Michael J. Birkeland ◽  
Linda Lorenz ◽  
James M. Wescott ◽  
Charles R. Frihart
Keyword(s):  
Hot Pressing ◽  
Urea Formaldehyde ◽  
Chromotropic Acid ◽  
Monitoring Methods ◽  
Emission Testing ◽  
Short And Long Term ◽  
The Common ◽  
Short Time

Abstract Hot-pressing wood, particularly in the production of wood composites, generates significant “native” (wood-based) formaldehyde (FA), even in the absence of adhesive. The level of native FA relates directly to the time and temperature of hot-pressing. This native FA dissipates in a relatively short time and is not part of the long-term FA emission issue commonly associated with hydrolyzing urea-formaldehyde bonds. This paper demonstrates that the common desiccator/chromotropic acid method is very specific for FA and is not influenced by other volatile compounds set free from wood during hot-pressing. Furthermore, it is shown that particleboard produces native FA at high levels even in the absence of adhesives or in the presence of one type of no-added formaldehyde (NAF) adhesive. Soy-based adhesives suppress native FA emission and provide low FA emission levels in both the short and long term. This study highlights an often overlooked aspect that should be considered for emission testing: standardizing the time and conditions employed immediately after pressing and prior to the onset of emissions testing. Addressing this issue in more detail would improve the reliability of correlation between data obtained by rapid process monitoring methods and emission measurements in large chambers.

Rubidium Sulfate Flame Detector: Effect of Design of Alkali Source and Anode on Sensitivity and Stability

1969 ◽  
Vol 52 (3) ◽  
pp. 533-541
Author(s):  
Hiroko K DeLoach ◽  
D D Hemphill
Keyword(s):  
Detection System ◽  
Physical Stability ◽  
Optimum Conditions ◽  
Flame Detector ◽  
Short And Long Term ◽  
Rubidium Sulfate ◽  
Relationship Of ◽  
The Relationship

Abstract An improved alkali-flame detector using pure rubidium sulfate and an anode of new design were optimized for the quantitative determination of organophosphate pesticides. The performance of this detection system was evaluated for response to organophosphate standards, noise level, fluctuation of baseline, short- and long-term reproducibility at low pesticides levels, conditioning time of instrument, life and physical stability of alkali source, and required frequency of detector cleaning. Under optimum conditions the detector was sensitive to 1 pg pesticide standard. To define the parameters of the alkali flame detector, studies were made of different designs of the alkali source which influence flame configuration and the relationship of the position and shape of the anode to the flame. The most important parameter appears to be the method of introducing alkali vapor.

scholarly journals Development studies of captopril certified reference material

2011 ◽  
Vol 47 (2) ◽  
pp. 339-350 ◽  
Author(s):  
Raquel Nogueira ◽  
Eliane Cristina Pires do Rego ◽  
Marcus Vinicius Barreto Sousa ◽  
Wagner Wollinger ◽  
Thaís Elias da Silva ◽  
...  
Keyword(s):  
Reference Material ◽  
Certified Reference Material ◽  
Active Pharmaceutical Ingredient ◽  
Stability Studies ◽  
Long Term Stability ◽  
Short And Long Term ◽  
Determination Of Impurities ◽  
Mass Balance Approach

This paper describes the studies performed with the candidate Certified Reference Material (CRM) of captopril, the first CRM of an active pharmaceutical ingredient (API) in Brazil, including determination of impurities (organic, inorganic and volatiles), homogeneity testing, short- and long-term stability studies, calculation of captopril content using the mass balance approach, and estimation of the associated measurement uncertainty.

Development of a procedure to determine odour emissions from animal farming for regulatory purposes in Flanders

2001 ◽  
Vol 44 (9) ◽  
pp. 205-210 ◽  
Author(s):  
H. Van Langenhove ◽  
G. De Bruyn
Keyword(s):  
Large Scale ◽  
Ventilation Rate ◽  
External Parameter ◽  
Animal Farming ◽  
Short And Long Term ◽  
Odour Emissions ◽  
One Year ◽  
Fattening Pigs

The purpose of the project described in this paper was to develop a procedure to determine odour emissions at existing and new intensive animal farming houses. The procedure should be scientifically valid and preferably applicable on a large scale at reasonable costs. In this project odour emissions were measured during one year at the same farm. Measurements included 20 olfactometric sampling days and 50 sniffing measurements, all spread over one year. For each olfactometric sampling day, samples were taken in duplicate for the different pig categories. The olfactometric analysis resulted in the determination of odour emission factors for growing/fattening pigs, weaned piglets, dry sows and farrowing sows. The influence of external parameters (ventilation rate, inside temperature, outside temperature, pen dirtiness, number of pigs and their weight) was examined. Good correlation between the odour emission and an external parameter could only be found for the ventilation rate (r = 0.98) and outside temperature (r = 0.87). The sniffing measurements resulted in maximal odour perception distances and odour emissions calculated with short and long term dispersion models. No significant influence of the outside temperature (season) could be found here. The results of the olfactometric and sniffing measurements will be presented, including a combination of both techniques to determine the odour emission of an agricultural construction.

Predicted and measured stresses and displacements around the Darlington Intake Tunnel

1984 ◽  
Vol 21 (1) ◽  
pp. 147-165 ◽  
Author(s):  
K. Y. Lo ◽  
B. Lukajic
Keyword(s):  
Field Measurements ◽  
Time Dependent ◽  
Long Term Conditions ◽  
Field Instrumentation ◽  
Deformation Properties ◽  
Strength And Deformation ◽  
Short And Long Term ◽  
Keywords Stress

The C.W. Intake Tunnel of the Darlington Nuclear Station is D-shaped in section with a span of 8 m and a length of 925 m beneath Lake Ontario. The tunnel is located in a horizontally bedded limestone with variable shaly interbeds.The geotechnical investigation including in-situ rock stress measurements, and laboratory determination of strength and deformation properties as well as time-dependent behaviour are reported. Design of the tunnel, in particular provisions for "rock squeeze," is described in detail.To verify the design approach adopted and the provisions made, field instrumentation was performed during excavation of the tunnel. The results of field measurements of stresses and displacements were compared with premonitoring analysis. Postmonitoring analyses were also performed using the as-constructed condition. It is shown that the performance of the tunnel is in general agreement with the predicted behaviour in both short and long term conditions. Keywords: stress, displacement, time-dependent deformation, stressmeter, tunnel, rock mechanics, rock squeeze.

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