Effect of cationic precursor pH on optical and transport properties of SILAR deposited nano crystalline PbS thin films

2012 ◽  
Vol 12 (1) ◽  
pp. 53-59 ◽  
Author(s):  
K.C. Preetha ◽  
K.V. Murali ◽  
A.J. Ragina ◽  
K. Deepa ◽  
T.L. Remadevi
2007 ◽  
Vol 313 (1) ◽  
pp. 115-121 ◽  
Author(s):  
Ajay Singh ◽  
D.K. Aswal ◽  
P. Chowdhury ◽  
N. Padma ◽  
C.S. Viswanadham ◽  
...  

RSC Advances ◽  
2021 ◽  
Vol 11 (42) ◽  
pp. 26218-26227
Author(s):  
R. Panda ◽  
S. A. Khan ◽  
U. P. Singh ◽  
R. Naik ◽  
N. C. Mishra

Swift heavy ion (SHI) irradiation in thin films significantly modifies the structure and related properties in a controlled manner.


2018 ◽  
Vol 2 (11) ◽  
Author(s):  
W. C. Yang ◽  
Y. T. Xie ◽  
X. Sun ◽  
X. H. Zhang ◽  
K. Park ◽  
...  

2018 ◽  
Vol 165 ◽  
pp. 04011
Author(s):  
Keisuke Tanaka ◽  
Yuta Murase ◽  
Hirohisa Kimachi

The effect of micro-notches on the fatigue strength of nickel thin films was studied. Two types of thin films with 10 μm thickness were produced by electrodeposition using sulfamate solution without and with brightener: ultra-fine grained film (UFG) with the grain size of 384 nm and nano-crystalline grained film (NCG) with that of 17 nm. Micro-sized notches introduced by FIB had the width of 2 μm and various depths from 8 to 150μm. Fatigue tests were conducted under the stress ratio of 0.1. The fatigue strength decreased with increasing depth of notches. NCG had much higher strength than UFG compared at the same notch depth. Notches as small as 8μm did reduce the fatigue strength of both UFG and NCG. The fatigue limit was controlled by the initiation of cracks and no non-propagating crack was observed in specimens fatigued below the fatigue limit. A model of fictitious crack successfully predicted the reduction of the fatigue limit due to micro-notches. The characteristic crack length of NCG was much smaller than the UFG, while the fatigue strength of defect-free NCG was larger than that of UFG. SEM observation of fracture surfaces was conducted to reveal micromechanisms of fatigue crack initiation.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Aziz Ahmed ◽  
Seungwoo Han

AbstractN-type bismuth telluride (Bi2Te3) thin films were prepared on an aluminum nitride (AlN)-coated stainless steel foil substrate to obtain optimal thermoelectric performance. The thermal co-evaporation method was adopted so that we could vary the thin film composition, enabling us to investigate the relationship between the film composition, microstructure, crystal preferred orientation and thermoelectric properties. The influence of the substrate temperature was also investigated by synthesizing two sets of thin film samples; in one set the substrate was kept at room temperature (RT) while in the other set the substrate was maintained at a high temperature, of 300 °C, during deposition. The samples deposited at RT were amorphous in the as-deposited state and therefore were annealed at 280 °C to promote crystallization and phase development. The electrical resistivity and Seebeck coefficient were measured and the results were interpreted. Both the transport properties and crystal structure were observed to be strongly affected by non-stoichiometry and the choice of substrate temperature. We observed columnar microstructures with hexagonal grains and a multi-oriented crystal structure for the thin films deposited at high substrate temperatures, whereas highly (00 l) textured thin films with columns consisting of in-plane layers were fabricated from the stoichiometric annealed thin film samples originally synthesized at RT. Special emphasis was placed on examining the nature of tellurium (Te) atom based structural defects and their influence on thin film properties. We report maximum power factor (PF) of 1.35 mW/m K2 for near-stoichiometric film deposited at high substrate temperature, which was the highest among all studied cases.


2005 ◽  
Vol 97 (10) ◽  
pp. 10D319 ◽  
Author(s):  
Zhenjun Wang ◽  
Jinke Tang ◽  
Leonard Spinu

2017 ◽  
Vol 50 (27) ◽  
pp. 275004 ◽  
Author(s):  
A E Stanciu ◽  
A Kuncser ◽  
G Schinteie ◽  
P Palade ◽  
A Leca ◽  
...  

2020 ◽  
Vol 0 (0) ◽  
Author(s):  
Kooliyankal Naseema ◽  
Kaniyamkandy Ribin ◽  
Nidiyanga Navya ◽  
Prasoon Prasannan

AbstractNano crystalline zinc sulfide thin films were deposited onto glass substrates by chemical bath deposition method. One of the samples was annealed at 300 °C for 2 h in air using a muffle furnace. The prepared thin films were investigated by X-ray diffraction (XRD), UV–visible spectroscopy (UV–vis), photoluminescence spectroscopy (PL), scanning electron microscopy (SEM) and Raman spectroscopy (FT-R) studies before and after annealing. The analysis confirmed the thermal-induced anion substitution and conversion of ZnS crystal to ZnO wurtzite crystal. XRD pattern showed that these films were phase pure and polycrystalline in nature. Optical band gap was found to be 3.86 eV for ZnS and 3.21 eV for ZnO. The films prepared by this simple, low-cost technique are suitable for photovoltaic and optoelectronic applications.


1994 ◽  
Vol 235-240 ◽  
pp. 597-598 ◽  
Author(s):  
J. Azoulay ◽  
A. Verdyan ◽  
I. Lapsker

Sign in / Sign up

Export Citation Format

Share Document