Direct electrochemical reduction of graphene oxide on ionic liquid doped screen-printed electrode and its electrochemical biosensing application

2011 ◽  
Vol 28 (1) ◽  
pp. 204-209 ◽  
Author(s):  
Jianfeng Ping ◽  
Yixian Wang ◽  
Kai Fan ◽  
Jian Wu ◽  
Yibin Ying
Author(s):  
Abolfazl Darroudi ◽  
Saeid Nazari ◽  
Seyed Ali Marashi ◽  
Mahdi Karimi-Nazarabad

Abstract An accurate, rapid, simple, and novel technique was developed to determine simvastatin (SMV). In this research, a screen-printed electrode (SPE) was deposited with graphene oxide (GO) and sodium dodecyl sulfate (SDS), respectively. For the first time, the handmade modified SPE measured the SMV by differential pulse voltammetry (DPV) with high sensitivity and selectivity. The results of cyclic voltammetry indicated the oxidation irreversible process of SMV. Various parameters (pH, concentration, scan rate, support electrolyte) were performed to optimize the conditions for the determination of SMV. Under the optimum experiment condition of 0.1 M KNO3 as support electrolyte and pH 7.0, the linear range was achieved for SMV concentration from 1.8 to 36.6 µM with a limit of detection (LOD), and a limit of quantitation (LOQ) of 0.06 and 1.8 µM, respectively. The proposed method was successfully utilized to determine SMV in tablets and urine samples with a satisfactory recovery in the range of 96.2 to 103.3%.


2020 ◽  
Vol 8 (33) ◽  
pp. 7539-7547
Author(s):  
Xinrui Liu ◽  
Rajalakshmi Sakthivel ◽  
Yu-Cheng Chen ◽  
Ning Chang ◽  
Udesh Dhawan ◽  
...  

We have developed an electrochemical sensor based on integrated 2D materials including SnS2, graphene oxide, and β-cyclodextrin forming a ternary nanocomposite decorated on a screen-printed electrode for the electrochemical detection of melatonin.


2019 ◽  
Vol 19 ◽  
pp. 1183-1188
Author(s):  
Suhaili Sabdin ◽  
Mohd Azraie Mohd Azmi ◽  
Nurul Azurin Badruzaman ◽  
Fatihatul Zuriati Makmon ◽  
Azman Abd Aziz ◽  
...  

Author(s):  
Hamed Tashakkorian ◽  
Behnaz Aflatoonian ◽  
Peyman Mohammadzadeh Jahani ◽  
Mohammad Reza Aflatoonian

A simple strategy for determination of hydroxylamine based on Fe3O4 nanoparticles function­nalized by [2-(4-((3-(trimethoxysilyl)propylthio)methyl)1-H1,2,3-triazol-1-yl)acetic­acid] (FNPs) and graphene oxide (GO) modified screen-printed electrode (SPE), denoted as (Fe3O4 FNPs/GO/SPE), is reported. The electrochemical behavior of hydroxylamine was investigated at Fe3O4FNPs/GO/SPE by cyclic voltammetry (CV), differential pulse voltammetry (DPV) and chro­noamperometry (CHA) techniques in phosphate buffer solution (pH 7.0). Fe3O4 FNPs/GO/SPE as a novel electrochemical sensor exhibited catalytic activity toward the oxidation of hydroxyl­ami­ne. The potential of hydroxylamine oxidation was shifted to more negative potentials, and its oxidation peak current increased on the modified electrode, also indicating that under these conditions, the electrochemical process is irreversible. The electrocatalytic current of hydroxyl­amine showed a good relationship in the concentration range of 0.05–700.0 μM, with a detection limit of 10.0 nM. The proposed electrode was applied for the determination of hydroxyl­amine in water samples, too.


2021 ◽  
Author(s):  
Gizem Turkkan ◽  
Salih Zeki Bas ◽  
Keziban Atacan ◽  
Mustafa Ozmen

In this study, we report the fabrication of nanocomposite consisting of Co3O4 nanoparticles (Co3O4 NPs) and electrochemically reduced graphene oxide (ERGO) on the screen-printed electrode (SPE) and its sensing performance...


Sign in / Sign up

Export Citation Format

Share Document