Development of preparation method to control silica sol–gel synthesis with rheological and morphological measurements

2014 ◽  
Vol 25 (2) ◽  
pp. 773-779 ◽  
Author(s):  
Aya Kaide ◽  
Takashi Saeki
Keyword(s):  
Preparation Method ◽  
Sol Gel ◽  
Silica Sol ◽  
Sol Gel Synthesis

Sol–gel synthesis of photoactive kaolinite-titania: Effect of the preparation method and their photocatalytic properties

2015 ◽  
Vol 331 ◽  
pp. 98-107 ◽  
Author(s):  
Godlisten N. Shao ◽  
Marion Engole ◽  
S.M. Imran ◽  
Sun Jeong Jeon ◽  
Hee Taik Kim
Keyword(s):  
Preparation Method ◽  
Sol Gel ◽  
Photocatalytic Properties ◽  
Sol Gel Synthesis

Non-cytotoxic hybrid bioscaffolds of chitosan-silica: Sol-gel synthesis, characterization and proposed application

2017 ◽  
Vol 178 ◽  
pp. 190-199 ◽  
Author(s):  
Athit Pipattanawarothai ◽  
Chomchai Suksai ◽  
Klaokwan Srisook ◽  
Thanida Trakulsujaritchok
Keyword(s):  
Sol Gel ◽  
Silica Sol ◽  
Sol Gel Synthesis

Progress in Developing Nerve Agent Sensors Using Combinatorial Techniques

2003 ◽  
Vol 787 ◽  
Author(s):  
John C. DiCesare ◽  
Jennifer Parker ◽  
Starr N. Horne ◽  
Justin Kita ◽  
Raghu Earni ◽  
...  
Keyword(s):  
Molecular Imprinting ◽  
Sol Gel ◽  
Hydrolysis Product ◽  
Three Dimensional ◽  
Nerve Agents ◽  
Nerve Agent ◽  
Silica Sol ◽  
Sol Gel Synthesis ◽  
Selection Of

ABSTRACTDevelopment of a sensor capable of selective detection of specific nerve agents is imperative in today’s atmosphere of terrorism. The sensor needs to be inexpensive, portable, reliable, absent of false positives and available to all military and first responders. By utilizing the techniques of molecular imprinting, combinatorial chemistry, silica sol-gel synthesis and lanthanide luminescence, a sensor for the detection of the hydrolysis product of the nerve agent soman is being developed. There are many parameters that require investigation in order for the sensor to become a reality. These parameters include 1) the selection of a chelate that can bind to the lanthanide and anchor the nerve agent simulant during the formation of the molecularly imprinted polymer, 2) the determination of the environment best suited for this complex formation, 3) the formation, as well as modification of the silica sol-gel for molecular imprinting to take place, and 4) the proper quantity and ratios of monomers used to create the three dimensional imprint. Key to the success of optimizing these parameters is the development of a combinatorial assay that allows for the synthesis and testing of tens of thousands of combinations of parameters. Work on the development of the combinatorial assay has lead to a method of preparing thin film polymers capable of analyzing the presence of nerve agent simulants. Current work is underway to validate the combinatorial assay and to synthesize and evaluate a library of sensor materials selective for nerve agents.

Inorganic-organic Hybrid Materials for Real 3-D Sub-νm Lithography

2003 ◽  
Vol 780 ◽  
Author(s):  
R. Houbertz ◽  
J. Schulz ◽  
L. Fröhlich ◽  
G. Domann ◽  
M. Popall ◽  
...  
Keyword(s):  
Femtosecond Laser ◽  
Sol Gel ◽  
Laser Pulses ◽  
Femtosecond Laser Pulses ◽  
Hybrid Polymer ◽  
Organic Hybrid ◽  
Two Photon ◽  
Applied Technology ◽  
Scale Structures ◽  
Sol Gel Synthesis

AbstractReal 3-D sub-νm lithography was performed with two-photon polymerization (2PP) using inorganic-organic hybrid polymer (ORMOCER®) resins. The hybrid polymers were synthesized by hydrolysis/polycondensation reactions (modified sol-gel synthesis) which allows one to tailor their material properties towards the respective applications, i.e., dielectrics, optics or passivation. Due to their photosensitive organic functionalities, ORMOCER®s can be patterned by conventional photo-lithography as well as by femtosecond laser pulses at 780 nm. This results in polymerized (solid) structures where the non-polymerized parts can be removed by conventional developers.ORMOCER® structures as small as 200 nm or even below were generated by 2PP of the resins using femtosecond laser pulses. It is demonstrated that ORMOCER®s have the potential to be used in components or devices built up by nm-scale structures such as, e.g., photonic crystals. Aspects of the materials in conjunction to the applied technology are discussed.

Sol-Gel Synthesis, Structure and Optical Properties of Nickel-Manganese Ferrites

2019 ◽  
Vol 11 (3) ◽  
pp. 03021-1-03021-5
Author(s):  
V. S. Bushkova ◽  
◽  
I. P. Yaremiy ◽  
B. K. Ostafiychuk ◽  
N. I. Riznychuk ◽  
...  
Keyword(s):  
Optical Properties ◽  
Sol Gel ◽  
Sol Gel Synthesis ◽  
Nickel Manganese

Sol-Gel Synthesis of Nano-Scale, End-Member Albite Feldspar (NaAlSi3O8)

2021 ◽  
Author(s):  
L.M. Anovitz ◽  
A. Affolter ◽  
M.C. Cheshire ◽  
A.J. Rondinone ◽  
Lawrence F. Allard
Keyword(s):  
Sol Gel ◽  
Nano Scale ◽  
Sol Gel Synthesis

scholarly journals A simple approach to prepare fluorescent molecularly imprinted nanoparticles

RSC Advances ◽  
2021 ◽  
Vol 11 (13) ◽  
pp. 7732-7737
Author(s):  
Fenying Wang ◽  
Dan Wang ◽  
Tingting Wang ◽  
Yu Jin ◽  
Baoping Ling ◽  
...  
Keyword(s):  
High Performance ◽  
Low Cost ◽  
Sol Gel ◽  
Silica Sol ◽  
Simple Approach ◽  
Imprinted Polymer ◽  
Molecularly Imprinted ◽  
Low Toxicity ◽  
Good Biocompatibility ◽  
Molecularly Imprinted Nanoparticles

Fluorescent molecularly imprinted polymer (FMIP) gains great attention in many fields due to their low cost, good biocompatibility and low toxicity. Here, a high-performance FMIP was prepared based on the autocatalytic silica sol–gel reaction.

scholarly journals Aqueous Sol-Gel Synthesis of Different Iron Ferrites: From 3D to 2D

Materials ◽  
2021 ◽  
Vol 14 (6) ◽  
pp. 1554
Author(s):  
Justinas Januskevicius ◽  
Zivile Stankeviciute ◽  
Dalis Baltrunas ◽  
Kęstutis Mažeika ◽  
Aldona Beganskiene ◽  
...  
Keyword(s):  
Magnetic Measurements ◽  
Substrate Surface ◽  
Sol Gel ◽  
Synthesis Method ◽  
Xrd Analysis ◽  
Dip Coating ◽  
Yttrium Iron ◽  
Iron Garnet ◽  
Dip Coating Technique ◽  
Sol Gel Synthesis

In this study, an aqueous sol-gel synthesis method and subsequent dip-coating technique were applied for the preparation of yttrium iron garnet (YIG), yttrium iron perovskite (YIP), and terbium iron perovskite (TIP) bulk and thin films. The monophasic highly crystalline different iron ferrite powders have been synthesized using this simple aqueous sol-gel process displaying the suitability of the method. In the next step, the same sol-gel solution was used for the fabrication of coatings on monocrystalline silicon (100) using a dip-coating procedure. This resulted, likely due to substrate surface influence, in all coatings having mixed phases of both garnet and perovskite. Thermogravimetric (TG) analysis of the precursor gels was carried out. All the samples were investigated by X-ray powder diffraction (XRD) analysis. The coatings were also investigated by scanning electron microscopy (SEM), atomic force microscopy (AFM) and Mössbauer spectroscopy. Magnetic measurements were also carried out.

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