Structure switch between α-Fe2O3, γ-Fe2O3 and Fe3O4 during the large scale and low temperature sol–gel synthesis of nearly monodispersed iron oxide nanoparticles

2013 ◽  
Vol 24 (1) ◽  
pp. 93-97 ◽  
Author(s):  
Hongtao Cui ◽  
Yan Liu ◽  
Wanzhong Ren
2009 ◽  
Vol 404 (20) ◽  
pp. 3666-3670 ◽  
Author(s):  
Zhijun Zhang ◽  
Liviu Clime ◽  
Boguslaw Tomanek ◽  
Garnette Sutherland ◽  
Teodor Veres

Langmuir ◽  
2017 ◽  
Vol 33 (7) ◽  
pp. 1662-1669 ◽  
Author(s):  
Jing Cai ◽  
Yu Qing Miao ◽  
Bao Zhi Yu ◽  
Pei Ma ◽  
Li Li ◽  
...  

2020 ◽  
Vol 20 (10) ◽  
pp. 6525-6531
Author(s):  
Majid Mostaghelchi ◽  
Jani Kotakoski ◽  
Christian Rentenberger ◽  
Christian L. Lengauer

The wide range of actual and potential applications of nanoparticles, highlight the necessity of a reliable production method for both quality and quantity of the products. Mechanical attrition is one of the first well-known techniques used to produce nanoparticles. However, these approaches have been restricted to produce uniform particles below the critical size of 15 nm because of the attrition balance limit. This paper introduces the magnetite–silicate raw material of a Kiruna-type ore deposit as a novel precursor, which enables the production of small iron oxide nanoparticles below the critical size by mechanical attrition. X-ray fluorescence (XRF), powder X-ray diffractometry (pXRD), dynamic light scattering (DLS) and transmission electron microscopy (TEM) were used for characterization of the precursor and obtained nanoparticles. The results indicate that the particles with a mean diameter of 10.7(2.7) nm consist of mainly less than one crystallite. The significant size reduction below the attrition balance limit can be attributed to the quartz content of the raw material, which operated as supporting micro-balls for transferring the energy during the milling process.


2016 ◽  
Vol 180 ◽  
pp. 272-278 ◽  
Author(s):  
Vilém Bartůněk ◽  
David Průcha ◽  
Marie Švecová ◽  
Pavel Ulbrich ◽  
Štěpán Huber ◽  
...  

2013 ◽  
Vol 25 (14) ◽  
pp. 2803-2811 ◽  
Author(s):  
Nilantha P. Wickramaratne ◽  
Vindya S. Perera ◽  
Byung-Wook Park ◽  
Min Gao ◽  
Grant W. McGimpsey ◽  
...  

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