scholarly journals An ultrasound-assisted digestion method for the determination of toxic element concentrations in ash samples by inductively coupled plasma optical emission spectrometry

2007 ◽  
Vol 602 (2) ◽  
pp. 195-201 ◽  
Author(s):  
Aki Ilander ◽  
Ari Väisänen
Keyword(s):  
Inductively Coupled Plasma ◽  
Optical Emission ◽  
Toxic Element ◽  
Emission Spectrometry ◽  
Digestion Method ◽  
Inductively Coupled ◽  
Element Concentrations ◽  
Plasma Optical Emission Spectrometry ◽  
Ultrasound Assisted

Evaluation of ICP-OES Method for Heavy Metal and Metalloids Determination in Sterile Dump Material

2018 ◽  
Vol 273 ◽  
pp. 159-166 ◽  
Author(s):  
Darya Ilieva ◽  
Andriana Surleva ◽  
Manuela Murariu ◽  
Gabi Drochioiu ◽  
Mohd Mustafa Al Bakri Abdullah
Keyword(s):  
Inductively Coupled Plasma ◽  
Optical Emission ◽  
Emission Spectrometry ◽  
Icp Oes ◽  
Digestion Method ◽  
Inductively Coupled ◽  
Wet Digestion ◽  
Accuracy And Precision ◽  
Plasma Optical Emission Spectrometry

This study is aimed at development of an analytical method for the determination of heavy metals and arsenicin waste material from barite recovery by dual view inductively coupled plasma optical emission spectrometry (ICP-OES) after wet digestion. Aquaregia open digestion method was used for sample preparation. A soil certified reference material was used to study the efficiency of wet digestion procedure applied to sterile dump material. The sensitivity, accuracy, and precision of the method were determined. The achieved detection limits are: Arsenic (As) 0.80; Copper (Cu) 0.29; Lead (Pb) 0.29; Zink (Zn) 0.30; Cadmium (Cd) 0.11; Chromium (Cr) 0.09; Nickel (Ni) 0.02, mg.kg-1.The developed method is applied for the determination of hazardous metals and arsenic in sterile dump material from closed barite mine in the region of Tarnita-Suceava, Romania.

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