Alternative spectrophotometric method for standardization of chlorite aqueous solutions

2007 ◽  
Vol 585 (2) ◽  
pp. 361-365 ◽  
Author(s):  
Marilia Philippi ◽  
Heldiane S. dos Santos ◽  
Aline O. Martins ◽  
Carla M.N. Azevedo ◽  
Marçal Pires
Keyword(s):  
Aqueous Solutions ◽  
Spectrophotometric Method

scholarly journals A New Spectrophotometric Method for Analysis of Allopurinol in Aqueous Solutions and Pharmaceutical Preparations

2009 ◽  
Vol 6 (2) ◽  
pp. 309-314
Author(s):  
Baghdad Science Journal
Keyword(s):  
Absorption Spectrum ◽  
Aqueous Solutions ◽  
Spectrophotometric Method ◽  
Calibration Curve ◽  
Pharmaceutical Preparations ◽  
High Sensitivity ◽  
Good Stability ◽  
Optimum Conditions ◽  
Wide Range

A new method for determination of allopurinol in microgram level depending on its ability to reduce the yellow absorption spectrum of (I-3) at maximum wavelength ( ?max 350nm) . The optimum conditions such as "concentration of reactant materials , time of sitting and order of addition were studied to get a high sensitivity ( ? = 27229 l.mole-1.cm-1) sandal sensitivity : 0.0053 µg cm-2 ,with wide range of calibration curve ( 1 – 9 µg.ml-1 ) good stability (more then24 hr.) and repeatability ( RSD % : 2.1 -2.6 % ) , the Recovery % : ( 98.17 – 100.5 % ) , the Erel % ( 0.50 -1.83 % ) and the interference's of Xanthine , Cystein , Creatinine , Urea and the Glucose in 20 , 40 , 60 fold of analyate were also studied .

A Kinetics Study of the Chemical Stability of Ketoconazole in Aqueous Solutions by Spectrophotometric Method

2011 ◽  
Vol 1 (5-6) ◽  
pp. 370-374 ◽  
Author(s):  
Reza Enayatifard ◽  
Noman Khalili ◽  
Mohammad Rahimizadeh ◽  
Jafar Akbari
Keyword(s):  
Aqueous Solutions ◽  
Chemical Stability ◽  
Spectrophotometric Method ◽  
Kinetics Study

Spectrophotometric study of the complex equilibria of cadmium(II) ions with 4-(2-pyridylazo)resorcine (PAR) using the SQUAD-G program and the method of determining Cd(II) ions with PAR

1982 ◽  
Vol 47 (4) ◽  
pp. 1086-1099 ◽  
Author(s):  
Sylva Vlčková ◽  
Luděk Jančář ◽  
Vlastimil Kubáň ◽  
Josef Havel
Keyword(s):  
Aqueous Solutions ◽  
Spectrophotometric Method ◽  
Calibration Curve ◽  
Linear Part ◽  
Spectrophotometric Study ◽  
Statistical Parameters ◽  
Cadmium Ions ◽  
Graphical Interpretation ◽  
Basic Parameters ◽  
The Individual

The existence of the red-orange CdLH+ complex (λmax = 406 nm, εmax = 1.78.104 mmol-1.cm2, log *β111 = -1.66+0.04) and CdL complex (λmax = 495 nm, εmax = 3.2.104 mmol-1. cm2, log *β112 = -8.25+0.05) was demonstrated in aqueous solutions of PAR with a concentration excess of Cd(II) ions. It was shown that a 10% v/v acetone medium containing Cd(II) in a concentration excess of PAR contains the following complexes: CdL2H2 (λmax = 507 nm, εmax = 1.4 . 104 mmol-1 cm(2), log*β122 = -2.85+0.04), CdL2H- (λmax = 495 nm, εmax = 6.25 . 104 mmol-1 cm2, log *β123 = -9.58 + 0.04) and CdL2-2 (λmax = 495 nm, εmax = 9.16 . 104 mmol-1 cm2, log *β124 = -17.33 + 0.06). The basic parameters of the individual complexes were determined by graphical interpretation using slope-intercept transformations and by numerical interpretation using the generalized SQUAD-G program. The statistical parameters of the spectrophotometric method of determining cadmium ions were evaluated from the linear part of the calibration curve using the STAT program.

Ultrathin frozen sections of yeast without aldehyde prefixation

1978 ◽  
Vol 36 (2) ◽  
pp. 58-59
Author(s):  
K. J. Böhm ◽  
a. E. Unger
Keyword(s):  
Aqueous Solutions ◽  
Biological Material ◽  
Yeast Cells ◽  
Frozen Sections ◽  
Good Preservation ◽  
Ultrathin Frozen Sections

During the last years it was shown that also by means of cryo-ultra-microtomy a good preservation of substructural details of biological material was possible. However the specimen generally was prefixed in these cases with aldehydes.Preparing ultrathin frozen sections of chemically non-prefixed material commonly was linked up to considerable technical and manual expense and the results were not always satisfying. Furthermore, it seems to be impossible to carry out cytochemical investigations by means of treating sections of unfixed biological material with aqueous solutions.We therefore tried to overcome these difficulties by preparing yeast cells (S. cerevisiae) in the following manner:

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