3-D microstructural characterization: Methods, analysis, and applications

JOM ◽  
2006 ◽  
Vol 58 (12) ◽  
pp. 24-24 ◽  
Author(s):  
Michael D. Uchic
Keyword(s):  
Microstructural Characterization ◽  
Characterization Methods

Microstructural Characterization Methods for Magnetic Thin Films

1999 ◽  
Vol 562 ◽  
Author(s):  
J. E. Wittig ◽  
J. Bentley ◽  
T. P. Nolan
Keyword(s):  
Thin Films ◽  
High Resolution ◽  
Microstructural Characterization ◽  
Magnetic Thin Films ◽  
Complete Analysis ◽  
Structure Property ◽  
Characterization Methods ◽  
Transmission Electron ◽  
High Resolution Tem ◽  
20 Nm

ABSTRACTMicrostructural characterization is key to determining the structure-property-processing relationships required to optimize the performance of magnetic thin films for longitudinal magnetic recording. Since the grain size of modem recording media is on the order of 10 to 20 nm, only high-resolution characterization methods such as transmission electron microscopy (TEM) can accurately describe the microstructure. Complete analysis requires a combination of conventional and high-resolution TEM imaging with analytical methods such as energy dispersivespectroscopy and energy-filtered TEM imaging. This paper provides examples from CoCr(Pt,Ta) alloys that reveal the strengths and limitations of these characterization methods as they apply to microstructural characterization of magnetic thin films.

scholarly journals Micromechanical behaviors related to confined deformation in pure titanium

2020 ◽  
Vol 321 ◽  
pp. 12018
Author(s):  
Runguang Li ◽  
Youkang Wang ◽  
Xiaojing Liu ◽  
Shilei Li ◽  
Qing Tan ◽  
...  
Keyword(s):  
Shear Banding ◽  
Pure Titanium ◽  
Microstructural Characterization ◽  
High Energy ◽  
Mechanical Twinning ◽  
Uniaxial Tensile ◽  
Good Resolution ◽  
Stress Concentrations ◽  
Complex Deformation ◽  
Characterization Methods

Confined deformation, e.g. mechanical twinning, shear banding, and Lüders banding, etc. was extensively observed in metals and alloys with low stacking-fault energies, especially under complex loadings, governing the mechanical properties. It is often accompanied with gradient microstructures to accommodate the stress concentrations. Understanding the micromechanical behaviors of structural materials having confined deformation is important for evaluating the structural stabilities of engineering components. Synchrotron-based techniques provide powerful tools for multiscale microstructural characterization owing to their good resolution in real/reciprocal space, fast data collection/processing and flexible application scenarios. In this paper, the synchrotron-based high-energy X-ray diffraction (HE-XRD) and microdiffraction (μXRD) techniques in combination with traditional characterization methods are used to reveal the deformational gradient structures/stresses under different loading modes in multiscale. The structure/stress gradients induced by laser shot peening treatment and the deformation twins generated during uniaxial tensile loading in pure titanium were systematically studied by HE-XRD and μXRD, in order to elucidate the accommodating role of the deformational structures subjected to various confined scenarios. The new finding regarding the micromechanical behaviors related to confined deformation contributes to the in-depth understanding of related complex deformation behaviors.

scholarly journals Construction of MoO3/MoSe2 nanocomposite based gas sensor for low detection limit trimethylamine sensing at room temperature

2021 ◽  
Author(s):  
Lanjuan Zhou ◽  
Qian Mi ◽  
Yingbo Jin ◽  
Tingting Li ◽  
Dongzhi Zhang
Keyword(s):  
Detection Limit ◽  
Gas Sensor ◽  
Room Temperature ◽  
Gas Sensing ◽  
Microstructural Characterization ◽  
Honeycomb Structure ◽  
Gas Sensitivity ◽  
Characterization Methods ◽  
Low Detection Limit ◽  
Sensing Performance

Abstract In this paper, MoO3/MoSe2 n-n heterostructure was constructed for fabricating trimethylamine (TMA) gas sensor by an improved hydrothermal and spin-coating method. The surface morphology and microstructure of the prepared materials were analyzed by XRD, XPS, SEM and TEM characterization methods. The microstructural characterization results demonstrated that the MoO3/MoSe2 heterostructure had been successfully synthesized, in which the MoSe2 had a flower-shaped structure, and MoO3 had a rod-shaped structure. At the same time, the MoSe2 surface exhibited periodic honeycomb structure. The gas-sensitivity experimental results showed that the proposed MoO3/MoSe2 sensor had excellent TMA sensing performance at room temperature, including high response capability, low detection limit (20 ppb), short response/recovery time (12 s/19 s), long-term stability, good repeatability and outstanding selectivity. The heterostructure of MoO3/MoSe2 had made outstanding contributions to the enhanced TMA gas sensing performance at room temperature.

The Influence of Deformation on Microstructure Evolution of Low Alloy TRIP Steel

2010 ◽  
Vol 638-642 ◽  
pp. 3531-3536
Author(s):  
Lucia Suarez ◽  
Josep Antonio Benito ◽  
Pablo Rodriguez-Calvillo ◽  
Daniel Casellas ◽  
Yvan Houbaert ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Electron Backscatter Diffraction ◽  
Physical And Mechanical Properties ◽  
Microstructural Characterization ◽  
Ferrite Matrix ◽  
Characterization Methods ◽  
Steel Microstructure ◽  
Trip Steels ◽  
Multiphase Microstructure

Low alloy transformation-induced plasticity aided (TRIP) steels have attracted much interest over the last years. TRIP steels were initially developed for automotive applications as they offer an excellent combination of strength and ductility at reasonable costs. These excellent mechanical properties mainly arise from a complex multiphase microstructure of a ferrite matrix and a dispersion of multiphase grains of bainite, martensite and metastable retained austenite. The relevant influence of microstructure on physical and mechanical properties makes metallographic study essential for an appropriate understanding and improvement of the mechanical behavior. An accurate microstructural characterization and quantification of the amount of the different constituents is indispensable to know how the stresses and strains are distributed within the different microstructural constituents. Among the different characterization methods commonly used electron backscatter diffraction (EBSD) appears to be the unique technique able to observe retained austenite grains often no larger than 1 μm. The present work shows the evolution of retained austenite while straining. Microstructural and textural evolution after different strains was examined by optical microscopy OM, EBSD and XRD techniques on TRIP800 steel. EBSD technique appears as a powerful tool for characterizing the complex multiphase steel microstructure and provides an accurate evaluation of the local crystallographic texture. It allows to measure orientation gradients within individual grains of each different phase. The distinction between some phases is observed.

Microstructural characterization of CoPtCr/Cr thin film disks by cross-section TEM and elongated probe micro-diffraction

1991 ◽  
Vol 49 ◽  
pp. 762-763
Author(s):  
M.A. Parker ◽  
K.E. Johnson ◽  
C. Hwang ◽  
A. Bermea
Keyword(s):  
Magnetic Recording ◽  
Electron Probe ◽  
Microstructural Characterization ◽  
Crystallographic Structure ◽  
Recording Media ◽  
Layer By Layer ◽  
Cross Sectional ◽  
New Techniques ◽  
Polished Side

We have reported the dependence of the magnetic and recording properties of CoPtCr recording media on the thickness of the Cr underlayer. It was inferred from XRD data that grain-to-grain epitaxy of the Cr with the CoPtCr was responsible for the interaction observed between these layers. However, no cross-sectional TEM (XTEM) work was performed to confirm this inference. In this paper, we report the application of new techniques for preparing XTEM specimens from actual magnetic recording disks, and for layer-by-layer micro-diffraction with an electron probe elongated parallel to the surface of the deposited structure which elucidate the effect of the crystallographic structure of the Cr on that of the CoPtCr.XTEM specimens were prepared from magnetic recording disks by modifying a technique used to prepare semiconductor specimens. After 3mm disks were prepared per the standard XTEM procedure, these disks were then lapped using a tripod polishing device. A grid with a single 1mmx2mm hole was then glued with M-bond 610 to the polished side of the disk.

TEM examination of 2014-SiC metal matrix composite

1988 ◽  
Vol 46 ◽  
pp. 726-727
Author(s):  
M. G. Burke ◽  
M. N. Gungor ◽  
P. K. Liaw
Keyword(s):  
Metal Matrix Composite ◽  
Metal Matrix Composites ◽  
Matrix Composite ◽  
Metal Matrix ◽  
Tensile Deformation ◽  
Microstructural Characterization ◽  
Thin Foil ◽  
Matrix Alloy ◽  
Matrix Composites ◽  
Ion Milling

Aluminum-based metal matrix composites offer unique combinations of high specific strength and high stiffness. The improvement in strength and stiffness is related to the particulate reinforcement and the particular matrix alloy chosen. In this way, the metal matrix composite can be tailored for specific materials applications. The microstructural characterization of metal matrix composites is thus important in the development of these materials. In this study, the structure of a p/m 2014-SiC particulate metal matrix composite has been examined after extrusion and tensile deformation.Thin-foil specimens of the 2014-20 vol.% SiCp metal matrix composite were prepared by dimpling to approximately 35 μm prior to ion-milling using a Gatan Dual Ion Mill equipped with a cold stage. These samples were then examined in a Philips 400T TEM/STEM operated at 120 kV. Two material conditions were evaluated: after extrusion (80:1); and after tensile deformation at 250°C.

Microstructural characterization of laser-melted/roller-quenched dicalcium silicate

1988 ◽  
Vol 46 ◽  
pp. 582-583
Author(s):  
C. J. Chan ◽  
K. R. Venkatachari ◽  
W. M. Kriven ◽  
J. F. Young
Keyword(s):  
Particle Size ◽  
Raw Materials ◽  
Shape Change ◽  
Microstructural Characterization ◽  
Particle Size Effect ◽  
Dicalcium Silicate ◽  
Laser Melting ◽  
Uniform Size ◽  
Cell Shape Change ◽  
Wide Range

Dicalcium silicate (Ca2SiO4) is a major component of Portland cement. It has also been investigated as a potential transformation toughener alternative to zirconia. It has five polymorphs: α, α'H, α'L, β and γ. Of interest is the β-to-γ transformation on cooling at about 490°C. This transformation, accompanied by a 12% volume increase and a 4.6° unit cell shape change, is analogous to the tetragonal-to-monoclinic transformation in zirconia. Due to the processing methods used, previous studies into the particle size effect were limited by a wide range of particle size distribution. In an attempt to obtain a more uniform size, a fast quench rate involving a laser-melting/roller-quenching technique was investigated.The laser-melting/roller-quenching experiment used precompacted bars of stoichiometric γ-Ca2SiO4 powder, which were synthesized from AR grade CaCO3 and SiO2xH2O. The raw materials were mixed by conventional ceramic processing techniques, and sintered at 1450°C. The dusted γ-Ca2SiO4 powder was uniaxially pressed into 0.4 cm x 0.4 cm x 4 cm bars under 34 MPa and cold isostatically pressed under 172 MPa. The γ-Ca2SiO4 bars were melted by a 10 KW-CO2 laser.

Sign in / Sign up

Export Citation Format

Share Document