Determination of silica in soaps and soap flakes. Perchloric acid method

1947 ◽  
Vol 24 (1) ◽  
pp. 13-14 ◽  
Author(s):  
Louis Silverman
Keyword(s):  
Perchloric Acid ◽  
Acid Method

Determination of Sulfur in Coal by Perchloric Acid Method

1932 ◽  
Vol 4 (2) ◽  
pp. 227-229 ◽  
Author(s):  
G. Frederick Smith ◽  
A. Garrell Deem
Keyword(s):  
Perchloric Acid ◽  
Acid Method ◽  
Sulfur In Coal

Spectrophotometric Determination of Aluminum, Iron, Manganese, Phosphorus, and Titanium in Liming Materials

1964 ◽  
Vol 47 (4) ◽  
pp. 620-626
Author(s):  
P Chichilo
Keyword(s):  
Spectrophotometric Determination ◽  
Perchloric Acid ◽  
Acid Method ◽  
Aluminum Iron ◽  
Iron Manganese

Abstract Methods have been developed for the determination of aluminum with ammonium aurintricarboxylate (Aluminon); iron with 2,4,6-tripyridyl-s-triazine (TPTZ); manganese by oxidation to permanganate with KI04; phosphorus by a heteropoly blue method; and titanium with disodium-1,2-dihydroxybenzene-3,5-disulfonate (Tiron), Detertested are carried out on the filtrate obtained in the AOAC perchloric acid method for silicon. Adequacy of the directions was established by “ruggedness tests,” and the procedures were used to analyze carbonate and silicate liming materials. It is recommended that the methods be studied collaboratively.

Deproteinizing methods evaluated for determination of uric acid in serum by reversed-phase liquid chromatography with ultraviolet detection.

1987 ◽  
Vol 33 (8) ◽  
pp. 1427-1430 ◽  
Author(s):  
R Sakuma ◽  
T Nishina ◽  
M Kitamura
Keyword(s):  
Uric Acid ◽  
Liquid Chromatography ◽  
Perchloric Acid ◽  
High Performance ◽  
Reversed Phase ◽  
Precipitation Method ◽  
Zinc Hydroxide ◽  
Good Precision ◽  
Ultraviolet Detection

Abstract We evaluated six deproteinizing methods for determination of uric acid in serum by "high-performance" liquid chromatography with ultraviolet detection: those involving zinc hydroxide, sodium tungstate, trichloroacetic acid, perchloric acid, acetonitrile, and centrifugal ultrafiltration (with Amicon MPS-1 devices). We used a Toyosoda ODS-120A reversed-phase column. The mobile phase was sodium phosphate buffer (40 mmol/L, pH 2.2) containing 20 mL of methanol per liter. Absorbance of the eluate was monitored at 284 nm. The precipitation method with perchloric acid gave high recoveries of uric acid and good precision, and results agreed with those by the uricase-catalase method of Kageyama (Clin Chim Acta 1971;31:421-6).

Comparison of several methods for semiquantitative determination of urinary protein.

1977 ◽  
Vol 23 (5) ◽  
pp. 876-879 ◽  
Author(s):  
W L Gyure
Keyword(s):  
Serum Albumin ◽  
Salt Concentration ◽  
Urine Samples ◽  
Urine Protein ◽  
Sulfosalicylic Acid ◽  
Green Method ◽  
Semiquantitative Determination ◽  
Acid Method ◽  
Bromcresol Green

Abstract Two types of urine protein dipsticks and the sulfosalicylic acid method were compared for their accuracy and specificity, with use of urine samples supplemented with various proteins. Dipsticks yield accurate results when the protein under consideration is restricted to albumin; the sulfosalicylic acid method accurately determines many kinds of proteins in addition to albumin. Detergents affect each of the methods, but changes in salt concentration only affect results by dipstick procedures. Dipsticks, which are based on the protein-error principle for indicators, are subject to some of the conditions that apply to the bromcresol green method for serum albumin determination.

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