Synthesis and crystal structure of [Nb2(S1.72Se2.28)(S2CNEt2)4]—A solid solution based on [Nb2(μ2, η2-X2)2(S2CNEt2)4], where X2=S2, SSe, and Se2. New model of structure refinement of [Nb2(S2)2(S2CNEt2)4], where X2=S2, SSe, and Se2. New model of structure refinement of [Nb2(S2)2(S2CNEt2)4]

1996 ◽  
Vol 37 (3) ◽  
pp. 458-463
Author(s):  
A. V. Virovets ◽  
M. N. Sokolov ◽  
N. V. Podberezskaya ◽  
V. E. Fedorov
Keyword(s):  
Crystal Structure ◽  
Solid Solution ◽  
Structure Refinement ◽  
Synthesis And Crystal Structure ◽  
New Model

Water-based sol–gel synthesis and crystal structure refinement of lanthanum silicate apatite

2008 ◽  
Vol 179 (38) ◽  
pp. 2209-2215 ◽  
Author(s):  
K KOBAYASHI ◽  
Y MATSUSHITA ◽  
N IGAWA ◽  
F IZUMI ◽  
C NISHIMURA ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Structure Refinement ◽  
Sol Gel ◽  
Crystal Structure Refinement ◽  
Synthesis And Crystal Structure ◽  
Water Based ◽  
Sol Gel Synthesis ◽  
Lanthanum Silicate

scholarly journals Synthesis and Crystal Structure of Nb0.84N

2011 ◽  
Vol 66 (1) ◽  
pp. 1-6 ◽  
Author(s):  
Nancy Frenzel ◽  
Elisabeth Irran ◽  
Martin Lerch ◽  
Alexandra Buchsteiner
Keyword(s):  
Crystal Structure ◽  
Rietveld Method ◽  
Structure Refinement ◽  
Close Packing ◽  
Powder Diffraction Data ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
Layer Sequence ◽  
Neutron Powder Diffraction Data ◽  
Metal Layers

A new compound of the composition Nb0.84N was prepared by ammonolysis of NbO2 at 1100 °C. The crystal structure refinement was performed by the Rietveld method using X-ray and neutron powder diffraction data. Nb0.84N crystallizes in the trigonal space group R3m (no. 166) with the lattice parameters a = 298.5(2) and c = 2384.3(4) pm. The niobium atoms form a close packing with a layer sequence which can be described by the Jagodzinski symbol hhc. The nitrogen atoms fill all octahedral voids. Along [001] a sequence of two layers of trigonal NbN6 prisms and one layer of NbN6 octahedra is formed. The nitrogen positions are fully occupied, the niobium positions only partially. Nb0.84N is part of a family of crystal structures between the anti-NiAs and the NaCl type consisting of close-packed metal layers with varying stacking sequences

Synthesis and Crystal Structure of Hollandite-Related Vanadium-Deficient Solid Solution BaV10-xO17 (0.10 ≤ x ≤ 0.65)

1994 ◽  
Vol 113 (1) ◽  
pp. 125-131 ◽  
Author(s):  
Yasushi Kanke ◽  
Eiji Takayama-Muromachi ◽  
Katsuo Kato ◽  
Kousuke Kosuda
Keyword(s):  
Crystal Structure ◽  
Solid Solution ◽  
Synthesis And Crystal Structure
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